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ASTM D4806-02

(Specification)

Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel

Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel

SCOPE
1.1 This specification covers nominally anhydrous denatured fuel ethanol intended to be blended with unleaded or leaded gasolines at 1 to 10 volume % for use as a spark-ignition automotive engine fuel. The significance of this specification is shown in Appendix X1.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

General Information

Status
Historical
Publication Date
09-Nov-2002
ICS
75.160.20 - Liquid fuels
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.A0.02 - Oxygenated Fuels and Components
Current Stage
Ref Project

Relations

Replaces
ASTM D4806-01a - Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
Effective Date
10-Nov-2002
Replaced By
ASTM D4806-03 - Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
Effective Date
10-Jun-2003
Referred By
ASTM E3050-22 - Standard Specification for Denatured Ethanol for Use as Cooking and Appliance Fuel
Effective Date
10-Nov-2002
Referred By
ASTM D7757-22 - Standard Test Method for Silicon in Gasoline and Related Products by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
Effective Date
10-Nov-2002
Referred By
ASTM D7795-15(2022)e1 - Standard Test Method for Acidity in Ethanol and Ethanol Blends by Titration
Effective Date
10-Nov-2002
Referred By
ASTM D1613-17(2023) - Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
Effective Date
10-Nov-2002
Referred By
ASTM D8235-21 - Standard Specification for Ethyl Tertiary-Butyl Ether (ETBE) for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
Effective Date
10-Nov-2002
Referred By
ASTM D5798-21 - Standard Specification for Ethanol Fuel Blends for Flexible-Fuel Automotive Spark-Ignition Engines
Effective Date
10-Nov-2002
Referred By
ASTM D7577-12(2021) - Standard Test Method for Determining the Accelerated Iron Corrosion Rating of Denatured Fuel Ethanol and Ethanol Fuel Blends
Effective Date
10-Nov-2002
Referred By
ASTM D7794-21 - Standard Practice for Blending Mid-Level Ethanol Fuel Blends for Flexible-Fuel Vehicles with Automotive Spark-Ignition Engines
Effective Date
10-Nov-2002
Referred By
ASTM D7875-20 - Standard Test Method for Determination of Butanol and Acetone Content of Butanol for Blending with Gasoline by Gas Chromatography
Effective Date
10-Nov-2002
Referred By
ASTM D8181-19 - Standard Specification for Microemulsion Blendstock for Preparing Microemulsion Test Fuel Oils
Effective Date
10-Nov-2002
Referred By
ASTM D5501-20 - Standard Test Method for Determination of Ethanol and Methanol Content in Fuels Containing Greater than 20 % Ethanol by Gas Chromatography
Effective Date
10-Nov-2002
Referred By
ASTM D8076-21b - Standard Specification for 100 Research Octane Number Test Fuel for Automotive Spark-Ignition Engines
Effective Date
10-Nov-2002
Referred By
ASTM D7717-11(2021) - Standard Practice for Preparing Volumetric Blends of Denatured Fuel Ethanol and Gasoline Blendstocks for Laboratory Analysis
Effective Date
10-Nov-2002

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ASTM D4806-02 - Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine FuelASTM D4806-02 - Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
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ASTM D4806-02 - Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
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Standards Content (Sample)

NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
An American National Standard
Designation: D 4806 – 02
Standard Specification for
Denatured Fuel Ethanol for Blending with Gasolines for Use
1
as Automotive Spark-Ignition Engine Fuel
This standard is issued under the fixed designation D 4806; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope D 4814 Specification for Automotive Spark-Ignition Engine
7
Fuel
1.1 This specification covers nominally anhydrous dena-
D 5453 Test Method for Determination of Total Sulfur in
tured fuel ethanol intended to be blended with unleaded or
Light Hydrocarbons, Motor Fuels, and Oils by Ultraviolet
leaded gasolines at 1 to 10 volume % for use as a spark-ignition
8
Fluorescence
automotive engine fuel. The significance of this specification is
D 5501 Test Method for the Determination of Ethanol
shown in Appendix X1.
Content of Denatured Fuel Ethanol by Gas Chromatogra-
1.2 The values stated in SI units are to be regarded as the
8
phy
standard. The values given in parentheses are for information
D 5580 Test Method for Determination of Benzene, Tolu-
only.
ene, Ethylbenzene, p/m-Xylene, o-Xylene, C and Heavier
9
2. Referenced Documents Aromatics, and Total Aromatics in Finished Gasoline by
8
Gas Chromatography
2.1 ASTM Standards:
D 6423 Test Method for Determination of pHe of Ethanol,
D 86 Test Method for Distillation of Petroleum Products at
9
2
Denatured Fuel Ethanol, and Fuel Ethanol (Ed75–Ed85)
Atmospheric Pressure
D 6550 Test Method for Determination of Olefin Content of
D 381 Test Method for Gum Content in Fuels by Jet
9
2
Gasolines by Supercritical-Fluid Chromatography
Evaporation
3
E 203 Test Method for Water Using Volumetric Karl Fischer
D 512 Test Methods for Chloride Ion in Water
4
Titration
D 891 Test Methods for Specific Gravity, Apparent, of
4
4
E 300 Practice for Sampling Industrial Chemicals
Liquid Industrial Chemicals
5
E 1064 Test Method for Water in Organic Liquids by
D 1152 Specification for Methanol (Methyl Alcohol)
4
6
Coulometric Karl Fischer Titration
D 1193 Specification for Reagent Water
2.2 Other Standards:
D 1613 Test Method for Acidity in Volatile Solvents and
United States Code of Federal Regulations, Title 27, Parts
Chemical Intermediates Used in Paint, Varnish, Lacquer,
10
5
20 and 21
and Related Products
6
United States Federal Specification O-E-760b Ethyl Alco-
D 1688 Test Methods for Copper in Water
hol (Ethanol): Denatured Alcohol: and Proprietary Sol-
D 3505 Test Method for Density or Relative Density of
11
5
vent
Pure Liquid Chemicals
D 4052 Test Method for Density and Relative Density of
3. Terminology
7
Liquids by Digital Density Meter
3.1 Definitions:
D 4057 Practice for Manual Sampling of Petroleum and
7 3.1.1 ethanol, n—ethyl alcohol, the chemical compound
Petroleum Products
C H OH.
2 5
3.1.2 gasoline, n—a volatile mixture of liquid hydrocar-
1
This specification is under the jurisdiction of ASTM Committee D02 on
bons, generally containing small amounts of additives, suitable
Petroleum Products and Lubricantsand is the direct responsibility of Subcommittee
for use as a fuel in spark-ignition, internal combustion engines.
D02.A0on Gasoline and Oxygenated Fuels.
Current edition approved Nov. 10, 2002. Published February 2003. Originally
approved in 1988. Last previous edition approved in 2001 as D 4806–01a.
2 8
Annual Book of ASTM Standards, Vol 05.01. Annual Book of ASTM Standards, Vol 05.03.
3 9
1986 Annual Book of ASTM Standards, Vol 11.01. Annual Book of ASTM Standards, Vol 05.04.
4 10
Annual Book of ASTM Standards, Vol 15.05. Order as Code of Federal Regulations Title 27 Parts 200-End: from Superin-
5
Annual Book of ASTM Standards, Vol 06.04. tendent of Documents, U.S. Government Printing Office, Washington, DC 20402.
6 11
Annual Book of ASTM Standards, Vol 11.01. Order from Superintendent of Documents, U.S. Government Printing Office,
7
Annual Book of ASTM Standards, Vol 05.02. Washington, DC 20402.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
D4806–02
3.1.3 gasoline-ethanol blend, n—a fuel consisting primarily 5. Denaturants
of gasoline along with a substantial amount (more than 0.35
5.1 The only denaturants used for fuel ethanol shall be
mass % oxygen) of denatured fuel ethanol.
natural gasoline, gasoline components, or unleaded gasoline at
3.1.4 oxygenate, n—an oxygen-containi
...

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Standard Test Method for Boiling Range Distribution of Fatty Acid Methyl Esters (FAME) in the Boiling Range from 100 °C to 615 °C by Gas Chromatography

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5.1 The boiling range distribution of FAMES provides an insight into the composition of product related to the transesterification process. This gas chromatographic determination of boiling range can be used to replace conventional distillation methods for product specification testing with the mutual agreement of interested parties.  
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SCOPE
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ASTM
ASTM D7484-23a(Test Method)
Standard Test Method for Evaluation of Automotive Engine Oils for Valve-Train Wear Performance in Cummins ISB Medium-Duty Diesel Engine

SIGNIFICANCE AND USE
5.1 This test method was developed to assess the performance of a heavy-duty engine oil in controlling engine wear under operating conditions selected to accelerate soot production and valve-train wear in a turbocharged and aftercooled four-cycle diesel engine with sliding tappet followers equipped with exhaust gas recirculation hardware.  
5.2 The design of the engine used in this test method is representative of many, but not all, modern diesel engines. This factor, along with the accelerated operating conditions, shall be considered when extrapolating test results.
SCOPE
1.1 This test method, commonly referred to as the Cummins ISB Test, covers the utilization of a modern, 5.9 L, diesel engine equipped with exhaust gas recirculation and is used to evaluate oil performance with regard to valve-train wear.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Exceptions—SI units are provided for all parameters except where there is no direct equivalent such as the units for screw threads, National Pipe Threads/diameters, tubing size, or where there is a sole source of supply equipment specification.  
1.2.2 See also A7.1 for clarification; it does not supersede 1.2 and 1.2.1.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See Annex A1 for general safety precautions.  
1.4 Table of Contents:    
Section  
Scope  
1  
Referenced Documents  
2  
Terminology  
3  
Summary of Test Method  
4  
Significance and Use  
5  
Apparatus  
6  
Engine Fluids and Cleaning Solvents  
7  
Preparation of Apparatus  
8  
Engine/Stand Calibration and Non-Reference Oil Tests  
9  
Test Procedure  
10  
Calculations, Ratings, and Test Validity  
11  
Report  
12  
Precision and Bias  
13  
Annexes  
Safety Precautions  
Annex A1  
Intake Air Aftercooler  
Annex A2  
The Cummins ISB Engine Build Parts Kit  
Annex A3  
Sensor Locations and Special Hardware  
Annex A4  
External Oil System  
Annex A5  
Cummins Service Publications  
Annex A6  
Specified Units and Formats  
Annex A7  
Oil Analyses  
Annex A8  
Alternate Fuel Approval Process  
Annex A9  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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