ASTM D6749-24
(Test Method)Standard Test Method for Pour Point of Petroleum Products (Automatic Air Pressure Method)
Standard Test Method for Pour Point of Petroleum Products (Automatic Air Pressure Method)
SIGNIFICANCE AND USE
5.1 The pour point of a petroleum product is an index of the lowest temperature of its utility for certain applications. Flow characteristics, like pour point, can be critical for the correct operation of lubricating systems, fuel systems, and pipeline operations.
5.2 Petroleum blending operations require precise measurement of the pour point.
5.3 Test results from this test method can be determined at either 1 °C or 3 °C intervals.
5.4 This test method yields a pour point in a format similar to Test Method D97/IP 15 when the 3 °C interval results are reported. However, when specification requires Test Method D97/IP 15, do not substitute this test method.
Note 2: Since some users may wish to report their results in a format similar to Test Method D97/IP 15 (in 3 °C intervals), the precision data were derived for the 3 °C intervals. For statements on bias relative to Test Method D97/IP 15, see 13.3.1.
5.5 This test method has better repeatability and reproducibility relative to Test Method D97/IP 15 as measured in the 1998 interlaboratory test program (see Section 13).
SCOPE
1.1 This test method covers the determination of pour point of petroleum products by an automatic apparatus that applies a slightly positive air pressure onto the specimen surface while the specimen is being cooled.
1.2 This test method is designed to cover the range of temperatures from −57 °C to +51 °C; however, the range of temperatures included in the (1998) interlaboratory test program only covered the temperature range from −51 °C to −11 °C.
1.3 Test results from this test method can be determined at either 1 °C or 3 °C testing intervals.
1.4 This test method is not intended for use with crude oils.
Note 1: The applicability of this test method on residual fuel samples has not been verified. For further information on the applicability, refer to 13.4.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D6749 − 24
Standard Test Method for
Pour Point of Petroleum Products (Automatic Air Pressure
1
Method)
This standard is issued under the fixed designation D6749; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
This test method covers an alternative procedure for the determination of pour point of petroleum
products using an automatic apparatus.
1. Scope* 2. Referenced Documents
2
1.1 This test method covers the determination of pour point 2.1 ASTM Standards:
of petroleum products by an automatic apparatus that applies a D97 Test Method for Pour Point of Petroleum Products
slightly positive air pressure onto the specimen surface while D4057 Practice for Manual Sampling of Petroleum and
the specimen is being cooled. Petroleum Products
D4175 Terminology Relating to Petroleum Products, Liquid
1.2 This test method is designed to cover the range of
Fuels, and Lubricants
temperatures from −57 °C to +51 °C; however, the range of
D4177 Practice for Automatic Sampling of Petroleum and
temperatures included in the (1998) interlaboratory test pro-
Petroleum Products
gram only covered the temperature range from −51 °C to
2.2 Energy Institute Standard:
−11 °C.
3
IP 15 Test Method for Pour Point of Petroleum Products
1.3 Test results from this test method can be determined at
either 1 °C or 3 °C testing intervals.
3. Terminology
1.4 This test method is not intended for use with crude oils.
3.1 Definitions:
NOTE 1—The applicability of this test method on residual fuel samples
3.1.1 For definitions of terms used in this test method, refer
has not been verified. For further information on the applicability, refer to
to Terminology D4175.
13.4.
3.1.2 pour point, n—in petroleum products, lowest tempera-
1.5 The values stated in SI units are to be regarded as
ture at which movement of the test specimen is observed under
standard. No other units of measurement are included in this
prescribed conditions of test.
standard.
3.2 Definitions of Terms Specific to This Standard:
1.6 This standard does not purport to address all of the
3.2.1 air pressure, n—regulated slightly positive air pres-
safety concerns, if any, associated with its use. It is the
sure gently applied onto the specimen surface in the airtight
responsibility of the user of this standard to establish appro-
test jar that causes upward movement of the specimen in the
priate safety, health, and environmental practices and deter-
communicating tube, which has one end inserted into the test
mine the applicability of regulatory limitations prior to use.
specimen and the other end at atmospheric pressure.
1.7 This international standard was developed in accor-
3.2.2 no-flow point, n—in petroleum products, temperature
dance with internationally recognized principles on standard-
of the test specimen at which a wax crystal structure of the test
ization established in the Decision on Principles for the
specimen or viscosity increase, or both, impedes movement of
Development of International Standards, Guides and Recom-
the surface of the test specimen under the conditions of the test.
mendations issued by the World Trade Organization Technical
3.2.2.1 Discussion—The no-flow point occurs when, upon
Barriers to Trade (TBT) Committee.
1 2
This test method is under the jurisdiction of ASTM Committee D02 on For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Subcommittee D02.07 on Flow Properties. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved March 1, 2024. Published April 2024. Originally the ASTM website.
3
approved in 2002. Last previous edition approved in 2018 as D6749 – 02 (2018). Available from Energy Institute, 61 New Cavendish St., London, W1G 7AR,
DOI: 10.1520/D6749-24. U.K., http://www.energyinst.org.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D6749 − 24
cooling, the formation of wax crystal structures or viscosity 6. Apparatus
increase, or both, has progressed to the point where the applied 4,5
6.1 Automatic Apparatus —The automatic pour point ap-
observation
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D6749 − 02 (Reapproved 2018) D6749 − 24
Standard Test Method for
Pour Point of Petroleum Products (Automatic Air Pressure
1
Method)
This standard is issued under the fixed designation D6749; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
This test method covers an alternative procedure for the determination of pour point of petroleum
products using an automatic apparatus.
1. Scope Scope*
1.1 This test method covers the determination of pour point of petroleum products by an automatic apparatus that applies a slightly
positive air pressure onto the specimen surface while the specimen is being cooled.
1.2 This test method is designed to cover the range of temperatures from −57 °C to +51 °C; however, the range of temperatures
included in the (1998) interlaboratory test program only covered the temperature range from −51 °C to −11 °C.
1.3 Test results from this test method can be determined at either 1 °C or 3 °C testing intervals.
1.4 This test method is not intended for use with crude oils.
NOTE 1—The applicability of this test method on residual fuel samples has not been verified. For further information on the applicability, refer to 13.4.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of
regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D97 Test Method for Pour Point of Petroleum Products
1
This test method is under the jurisdiction of ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of Subcommittee
D02.07 on Flow Properties.
Current edition approved May 1, 2018March 1, 2024. Published June 2018April 2024. Originally approved in 2002. Last previous edition approved in 20122018 as
D6749 – 02 (2012).(2018). DOI: 10.1520/D6749-02R18.10.1520/D6749-24.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D6749 − 24
D4057 Practice for Manual Sampling of Petroleum and Petroleum Products
D4175 Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products
2.2 Energy Institute Standard:
3
IP 15 Test Method for Pour Point of Petroleum Products
3. Terminology
3.1 Definitions:
3.1.1 For definitions of terms used in this test method, refer to Terminology D4175.
3.1.2 pour point, n—in petroleum products, lowest temperature at which movement of the test specimen is observed under
prescribed conditions of test.
3.2 Definitions of Terms Specific to This Standard:
3.2.1 air pressure, n—regulated slightly positive air pressure gently applied onto the specimen surface in the airtight test jar that
causes upward movement of the specimen in the communicating tube, which has one end inserted into the test specimen and the
other end at atmospheric pressure.
3.2.2 no-flow point, n—in petroleum products, temperature of the test specimen at which a wax crystal structure of the test
specimen or viscosity increase, or both, impedes movement of the surface of the test specimen under the conditions of the test.
3.2.2.1 Discussion—
The no-flow point occurs when, upon cooling, the formation of wax crystal structures or viscosity increase, or both, has progressed
to the point where the appl
...
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