ASTM D4504-94(2011)
(Specification)Standard Specification for Molded Polyethylene Open-Head-Pails for Industrial Shipping of Nonhazardous Goods
Standard Specification for Molded Polyethylene Open-Head-Pails for Industrial Shipping of Nonhazardous Goods
ABSTRACT
This specification establishes the performance requirements and test methods for molded polyethylene open-head, self-supporting, and nonreusable pails used in packaging and transporting nonhazardous goods. The products for packaging in the open-head pails may be in liquid, solid, past, granular, or powder form. Each pail is classified as either pails for liquids or pails for nonliquids. Materials for the manufacture of the pails should be compatible with the intended contents. Carbon black or other suitable pigments may be used for ultraviolet protection if needed. Each pail should conform to the required values of capacity, closure, drop strength, stacking strength, amount of column stack vibratioin, compatibility permeation, resistance to environmental stress cracking, and other special requirements.
SCOPE
1.1 This specification covers molded polyethylene, open-head, self-supporting, nonreusable pails intended for the packaging and transportation of nonhazardous goods. Pails are to have volume capacities between 1 and 7 gal (3.8 to 26.5 L).
1.2 Pails intended to contain hazardous goods (materials) shall be in accordance with and tested to United States Department of Transportation Code of Federal Regulations (CFR) Title 49, Parts (100–199).
1.3 The purpose of this specification is to establish performance requirements and test methods for molded open-head polyethylene pails.
1.4 Additives for the resin used and design of the pails are left to the discretion of the supplier, within the allowable limits of regulatory and performance requirements.
1.5 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.6 The following safety hazards caveat pertains to the test method portions, Section 10, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation:D4504 −94 (Reapproved 2011)
Standard Specification for
Molded Polyethylene Open-Head-Pails for Industrial
Shipping of Nonhazardous Goods
This standard is issued under the fixed designation D4504; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D996Terminology of Packaging and Distribution Environ-
ments
1.1 This specification covers molded polyethylene, open-
D999Test Methods for Vibration Testing of Shipping Con-
head, self-supporting, nonreusable pails intended for the pack-
tainers
aging and transportation of nonhazardous goods. Pails are to
D1972Practice for Generic Marking of Plastic Products
have volume capacities between 1 and 7 gal (3.8 to 26.5 L).
D1975Test Method for Environmental Stress Crack Resis-
1.2 Pails intended to contain hazardous goods (materials)
tance of Plastic Injection Molded Open Head Pails
shall be in accordance with and tested to United States
D4577Test Method for Compression Resistance of a Con-
Department of Transportation Code of Federal Regulations
tainer Under Constant Load
(CFR) Title 49, Parts (100–199).
D5276Test Method for Drop Test of Loaded Containers by
1.3 The purpose of this specification is to establish perfor- Free Fall
E4Practices for Force Verification of Testing Machines
mance requirements and test methods for molded open-head
polyethylene pails.
2.2 Other Documents:
National Motor Freight Classification (NMFC)
1.4 Additives for the resin used and design of the pails are
Uniform Freight Classification (UFC)
lefttothediscretionofthesupplier,withintheallowablelimits
Code of Federal Regulations Title 49 Parts 100–199 (CFR
of regulatory and performance requirements.
49)
1.5 The values stated in inch-pound units are to be regarded
as standard. The values given in parentheses are mathematical
3. Terminology
conversions to SI units that are provided for information only
3.1 Definitions—For definitions of terms used in this
and are not considered standard.
specification, see Terminology D996.
1.6 The following safety hazards caveat pertains to the test
3.2 Definitions of Terms Specific to This Standard:
methodportions,Section10,ofthisspecification:This standard
3.2.1 open-head pail—a pail with a full-diameter unre-
does not purport to address all of the safety concerns, if any,
stricted opening at the top, and designed to be carried by hand.
associated with its use. It is the responsibility of the user of this
The pail body is usually of a tapered design to provide for
standard to establish appropriate safety and health practices
nesting of pails during transportation and storage, prior to
and determine the applicability of regulatory limitations prior
filling of contents. After filling of contents, the pail lid is
to use.
applied to the pail body, providing a sealed container for
2. Referenced Documents
storage and shipment of the contents. The pail lid may also
2 have openings or fitments to allow for dispensing of contents
2.1 ASTM Standards:
without removing the lid. These openings are sealed with
D445Test Method for Kinematic Viscosity of Transparent
closures.
and Opaque Liquids (and Calculation of DynamicViscos-
3.2.1.1 Discussion—The definition for open-head pail for
ity)
hazardous materials differs (see Section 49 CFR Parts 100 to
199).
This specification is under the jurisdiction of ASTM Committee D10 on
Packaging and is the direct responsibility of Subcommittee D10.21 on Shipping
Containers and Systems - Application of Performance Test Methods.
Current edition approved Aug. 1, 2011. Published November 2011. Originally Available from National Motor Freight Traffic Association, Inc. (NMFTA),
´1
approved in 1985. Last previous edition approved in 2005 as D4504–94 (2005) . 1001 N. Fairfax St., Suite 600, Alexandria, VA 22314, http://www.nmfta.org.
DOI: 10.1520/D4504-94R11. Available from National Railroad Freight Committee, Suite 1120, 222 South
For referenced ASTM standards, visit the ASTM website, www.astm.org, or Riverside Plaza, Chicago, IL 60606.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM AvailablefromU.S.GovernmentPrintingOfficeSuperintendentofDocuments,
Standards volume information, refer to the standard’s Document Summary page on 732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401, http://
the ASTM website. www.access.gpo.gov.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D4504−94 (2011)
4. Classification 7.3 Closure—The closure for the pail (when used) shall be
in compliance with carrier regulatory requirements and shall
4.1 Products to be packaged in open-head pails may be
ensureprotectionofcontentsfromleakage,easeofclosure,and
liquid (Note 1), solid, paste, granular, or powder form.
removal.Gaskets,whenusedwiththeclosure,andtheclosure,
NOTE 1—For the purpose of establishing test requirements, a liquid is
shall be compatible with the intended contents.
heredefinedashavingaviscosityoflessthan5.0Pa.Satatemperatureof
7.4 Drop Strength— The pails shall show no evidence of
73.46 3.6°F (23 6 2°C), using the method described in Test Method
D445.
rupture, cracks, or leakage when tested in accordance with
10.2.1.
4.2 Molded polyethylene open-head pails are classified as
follows:
7.5 Stacking Strength—Two vertically stacked pails shall
4.2.1 Pails for liquids.
withstand testing without sidewall buckling sufficient to cause
4.2.2 Pails for nonliquids.
damage and shall have a total top-to-bottom deflection of both
pails of not more than 1 in. (25.4 mm), when tested in
5. Ordering Information
accordance with 10.2.2. In addition, there shall be no evidence
of leakage or sifting of contents from the pail when tested in
5.1 A summary of ordering requirements, detailed in other
accordance with 10.2.2.2.
sections of this specification include the following:
5.1.1 Materials of construction (see Section 6).
7.6 Vibration (Stack)—The pails shall show no evidence of
5.1.2 Ultraviolet protection (see 6.2).
rupture, cracks, or leakage when tested in accordance with
5.1.3 Other materials not specifically covered in this speci-
10.2.3.
fication (see 6.3 and 6.4).
7.7 Repetitive Shock Test (Optional)—The pails shall show
5.1.4 Pail capacity (see 7.2).
no evidence of rupture, cracks, or leakage when tested in
5.1.5 Closure requirements, including tamper evident fea-
accordance with 10.2.4.
ture (see 7.3).
7.8 Compatibility, Permeation—The pail shall perform sat-
5.1.6 Provisions for handling.
isfactorily when tested in accordance with 10.2.5.
5.1.7 Compatibility testing (see 7.8 and 7.9).
5.1.8 Inspection (see Section 11).
7.9 Resistance to Environmental Stress Cracking—The pail
5.1.9 Marking (see Section 13).
shall perform satisfactorily when tested in accordance with
5.1.10 Intended contents.
10.2.5.3.
5.1.11 Whether pressure testing is required.
7.10 Special Requirements—Pailrequirements,additionalto
those in 7.2 through 7.9, if needed by a purchaser, must be
6. Materials
specified in the procurement document and as agreed between
6.1 Materials for the construction of the pail shall be
purchaser and supplier.
compatible with the intended contents. Effects of impact,
vibration, temperature, warehouse stacking, and ultraviolet
8. Sampling
exposure should be considered.
8.1 Lotting—A lot shall consist of all pails of one size and
6.2 If ultraviolet protection is required, it shall be provided
design,producedfromthesamematerialsandunderessentially
bytheadditionofcarbonblackorothersuitablepigmentswith
the same manufacturing conditions and offered for delivery at
ultraviolet stabilizers and inhibitors.These additives should be
one time.
compatible with the contents and should retain their effective-
8.2 Sampling Pails— Select sample pails for test at random
ness during the life of the pail.
from a continuous production lot. As a minimum, the number
6.3 Materials for purposes other than ultraviolet protection
of pails required is 17 as outlined for design qualification tests
may be added, provided such additives permit the pail to meet
(see Section 10 and Supplementary Requirements).
the requirements of this specification.
6.4 Used materials, except regrind from the same concur- 9. Specimen Preparation
rent production process shall not be acceptable for manufac-
9.1 Prepare pail specimens in accordance with NMFC, item
turing new pails unless otherwise specified.
258 and UFC Rule 40, where applicable, and as agreed
between the pail purchaser and supplier.
7. Other Requirements
7.1 The pail shall show good workmanship such as absence 10. Methods of Testing Pails for Design Qualification
of flashing, dents, and scratched surfaces.
10.1 General—The test procedures described in this section
7.2 Capacity—Pails covered by this specification shall be are to be used to determine physical performance capability of
rangeinrated(marked)capacityfrom1to7gal(3.8to26.5L). aspecificdesignandthereby,toqualifysuchadesignunderthe
Minimum actual liquid capacity shall not be less than rated performance requirements of this specification. Additional
capacity plus 4%, and maximum actual capacity shall not be sampling and testing of these pails, as may be agreed upon
greaterthan4%aboveratedcapacityplusonequart,measured between purchaser and supplier, is not precluded by this
with cover attached and contents and pail at 73.4 6 5°F (23.8 section. Test methods to determine compatibility of the con-
6 3°C). tents (lading) with the pail will depend on the specific conten
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