Standard Test Method for Length Change of Hydraulic-Cement Mortars Exposed to a Sulfate Solution

SIGNIFICANCE AND USE
This test method provides a means of assessing the sulfate resistance of mortars made using portland cement, blends of portland cement with pozzolans or slags, and blended hydraulic cements. Method C452 is suitable for evaluating portland cements but not blended cements or blends of portland cement with pozzolans or slags.
The standard exposure solution used in this test method, unless otherwise directed, contains 352 moles of Na2SO4 per m3 (50 g/L). Other sulfate concentrations or other sulfates such as MgSO4 may be used to simulate the environmental exposure of interest. Further discussion of these and other technical issues is given in the Appendix.
SCOPE
1.1 This test method covers the determination of length change of mortar bars immersed in a sulfate solution. Mortar bars made using mortar described in Test Method C109/C109M are cured until they attain a compressive strength of 20.0 ± 1.0 MPa [3000 ± 150 psi], as measured using cubes made of the same mortar, before the bars are immersed.
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. Within the text, the inch-pound units are shown in brackets. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
31-Mar-2012
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C1012/C1012M − 12
StandardTest Method for
Length Change of Hydraulic-Cement Mortars Exposed to a
1
Sulfate Solution
This standard is issued under the fixed designation C1012/C1012M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* C305 Practice for Mechanical Mixing of Hydraulic Cement
Pastes and Mortars of Plastic Consistency
1.1 This test method covers the determination of length
C348 Test Method for Flexural Strength of Hydraulic-
change of mortar bars immersed in a sulfate solution. Mortar
Cement Mortars
bars made using mortar described in Test Method C109/
C349 Test Method for Compressive Strength of Hydraulic-
C109M are cured until they attain a compressive strength of
Cement Mortars (Using Portions of Prisms Broken in
20.0 6 1.0 MPa [3000 6 150 psi], as measured using cubes
Flexure)
made of the same mortar, before the bars are immersed.
C452 Test Method for Potential Expansion of Portland-
1.2 The values stated in either SI units or inch-pound units
Cement Mortars Exposed to Sulfate
are to be regarded separately as standard. Within the text, the
C490 Practice for Use ofApparatus for the Determination of
inch-pound units are shown in brackets. The values stated in
Length Change of Hardened Cement Paste, Mortar, and
each system may not be exact equivalents; therefore, each
Concrete
system shall be used independently of the other. Combining
C511 Specification for Mixing Rooms, Moist Cabinets,
values from the two systems may result in non-conformance
Moist Rooms, and Water Storage Tanks Used in the
with the standard.
Testing of Hydraulic Cements and Concretes
1.3 This standard does not purport to address all of the C595 Specification for Blended Hydraulic Cements
safety concerns, if any, associated with its use. It is the
C597 Test Method for Pulse Velocity Through Concrete
responsibility of the user of this standard to establish appro- C618 Specification for Coal Fly Ash and Raw or Calcined
priate safety and health practices and determine the applica-
Natural Pozzolan for Use in Concrete
bility of regulatory limitations prior to use. C684 Test Method for Making, Accelerated Curing, and
Testing Concrete Compression Test Specimens (With-
3
2. Referenced Documents
drawn 2012)
2
C778 Specification for Sand
2.1 ASTM Standards:
C917 Test Method for Evaluation of Cement Strength Uni-
C109/C109M Test Method for Compressive Strength of
formity From a Single Source
Hydraulic Cement Mortars (Using 2-in. or [50-mm] Cube
C989 Specification for Slag Cement for Use in Concrete and
Specimens)
Mortars
C114 Test Methods for Chemical Analysis of Hydraulic
D1193 Specification for Reagent Water
Cement
E18 Test Methods for Rockwell Hardness of Metallic Ma-
C150 Specification for Portland Cement
terials
C157/C157M Test Method for Length Change of Hardened
Hydraulic-Cement Mortar and Concrete 2.2 American Concrete Institute Reports:
4
ACI C201-2R-01 Guide to Durable Concrete
C215 Test Method for Fundamental Transverse,
Longitudinal, and Torsional Resonant Frequencies of
3. Significance and Use
Concrete Specimens
3.1 This test method provides a means of assessing the
sulfate resistance of mortars made using portland cement,
1
This test method is under the jurisdiction ofASTM Committee C01 on Cement
blendsofportlandcementwithpozzolansorslags,andblended
and is the direct responsibility of Subcommittee C01.29 on Sulfate Resistance.
hydraulic cements. Method C452 is suitable for evaluating
Current edition approved April 1, 2012. Published May 2012. Originally
approved in 1984. Last previous edition approved in 2010 as C1012/C1012M–10.
DOI: 10.1520/C1012_C1012M-12.
2 3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or The last approved version of this historical standard is referenced on
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM www.astm.org.
4
Standards volume information, refer to the standard’s Document Summary page on Available fromAmerican Concrete Institute (ACI), P.O. Box 9094, Farmington
the ASTM website. Hills, MI 48333-9094, http://www.concrete.org.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1012/C1012M − 12
portlandcementsbutnotblendedcementsorblendsofportland and store at 23.0 6 2.0 °C [73.5 6 3.5 °F]. Determine the pH
cement with pozzolans or slags. of the solution before use; reject the solution if the pH range is
outside 6.0 to 8.0. Maintain the
...

This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:C1012/C1012M–10 Designation:C1012/C1012M–12
Standard Test Method for
Length Change of Hydraulic-Cement Mortars Exposed to a
1
Sulfate Solution
This standard is issued under the fixed designation C1012/C1012M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope*
1.1 This test method covers the determination of length change of mortar bars immersed in a sulfate solution. Mortar bars made
using mortar described in Test Method C109/C109M are cured until they attain a compressive strength of 20.0 6 1.0 MPa [3000
6 150 psi], as measured using cubes made of the same mortar, before the bars are immersed.
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. Within the text, the
inch-poundunitsareshowninbrackets.Thevaluesstatedineachsystemmaynotbeexactequivalents;therefore,eachsystemshall
be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
C109/C109M Test Method for Compressive Strength of Hydraulic Cement Mortars (Using 2-in. or [50-mm] Cube Specimens)
C114 Test Methods for Chemical Analysis of Hydraulic Cement
C150 Specification for Portland Cement
C157/C157M Test Method for Length Change of Hardened Hydraulic-Cement Mortar and Concrete
C215 Test Method for Fundamental Transverse, Longitudinal, and Torsional Resonant Frequencies of Concrete Specimens
C305 Practice for Mechanical Mixing of Hydraulic Cement Pastes and Mortars of Plastic Consistency
C348 Test Method for Flexural Strength of Hydraulic-Cement Mortars
C349 Test Method for Compressive Strength of Hydraulic-Cement Mortars (Using Portions of Prisms Broken in Flexure)
C452 Test Method for Potential Expansion of Portland-Cement Mortars Exposed to Sulfate
C490 Practice for Use ofApparatus for the Determination of Length Change of Hardened Cement Paste, Mortar, and Concrete
C511 Specification for Mixing Rooms, Moist Cabinets, Moist Rooms, and Water Storage Tanks Used in the Testing of
Hydraulic Cements and Concretes
C595 Specification for Blended Hydraulic Cements
C597 Test Method for Pulse Velocity Through Concrete
C618 Specification for Coal Fly Ash and Raw or Calcined Natural Pozzolan for Use in Concrete
C684 Test Method for Making, Accelerated Curing, and Testing Concrete Compression Test Specimens
C778 Specification for Sand
C917 Test Method for Evaluation of Cement Strength Uniformity From a Single Source
C989 Specification for Slag Cement for Use in Concrete and Mortars
D1193 Specification for Reagent Water
E18 Test Methods for Rockwell Hardness of Metallic Materials
2.2 American Concrete Institute Reports:
3
ACI C201-2R-01 Guide to Durable Concrete
1
This test method is under the jurisdiction of ASTM Committee C01 on Cement and is the direct responsibility of Subcommittee C01.29 on Sulfate Resistance.
Current edition approved Dec. 15, 2010. Published January 2011. Originally approved in 1984. Last previous edition approved in 2009 as C1012/C1012M–09. DOI:
10.1520/C1012_C1012M-10.
Current edition approved April 1, 2012. Published May 2012. Originally approved in 1984. Last previous edition approved in 2010 as C1012/C1012M–10. DOI:
10.1520/C1012_C1012M-12.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from American Concrete Institute (ACI), P.O. Box 9094, Farmington Hills, MI 48333-9094, http://www.concrete.org.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
C1012/C1012M–12
3. Significance and Use
3.1 This test method provides a means of assessing the sulfate resistance of mortars made using portland cement, blends of
port
...

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