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ASTM D4806-07

(Specification)

Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel

Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel

SCOPE
1.1 This specification covers nominally anhydrous denatured fuel ethanol intended to be blended with unleaded or leaded gasolines at 1 to 10 volume % for use as a spark-ignition automotive engine fuel. The significance of this specification is shown in Appendix X1.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

General Information

Status
Historical
Publication Date
14-Jul-2007
ICS
75.160.20 - Liquid fuels
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.A0.02 - Oxygenated Fuels and Components
Current Stage
Ref Project

Relations

Replaces
ASTM D4806-06c - Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
Effective Date
15-Jul-2007
Replaced By
ASTM D4806-07a - Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
Effective Date
01-Dec-2007
Referred By
ASTM D4814-23 - Standard Specification for Automotive Spark-Ignition Engine Fuel
Effective Date
15-Jul-2007
Referred By
ASTM D7717-11(2021) - Standard Practice for Preparing Volumetric Blends of Denatured Fuel Ethanol and Gasoline Blendstocks for Laboratory Analysis
Effective Date
15-Jul-2007
Referred By
ASTM D8235-21 - Standard Specification for Ethyl Tertiary-Butyl Ether (ETBE) for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
Effective Date
15-Jul-2007
Referred By
ASTM D6423-20a - Standard Test Method for Determination of pHe of Denatured Fuel Ethanol and Ethanol Fuel Blends
Effective Date
15-Jul-2007
Referred By
ASTM D8076-21b - Standard Specification for 100 Research Octane Number Test Fuel for Automotive Spark-Ignition Engines
Effective Date
15-Jul-2007
Referred By
ASTM D8181-19 - Standard Specification for Microemulsion Blendstock for Preparing Microemulsion Test Fuel Oils
Effective Date
15-Jul-2007
Referred By
ASTM D5798-21 - Standard Specification for Ethanol Fuel Blends for Flexible-Fuel Automotive Spark-Ignition Engines
Effective Date
15-Jul-2007
Referred By
ASTM D7757-22 - Standard Test Method for Silicon in Gasoline and Related Products by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
Effective Date
15-Jul-2007
Referred By
ASTM D7875-20 - Standard Test Method for Determination of Butanol and Acetone Content of Butanol for Blending with Gasoline by Gas Chromatography
Effective Date
15-Jul-2007
Referred By
ASTM D8011-19 - Standard Specification for Natural Gasoline as a Blendstock in Ethanol Fuel Blends or as a Denaturant for Fuel Ethanol
Effective Date
15-Jul-2007
Referred By
ASTM D7794-21 - Standard Practice for Blending Mid-Level Ethanol Fuel Blends for Flexible-Fuel Vehicles with Automotive Spark-Ignition Engines
Effective Date
15-Jul-2007
Referred By
ASTM D7923-19 - Standard Test Method for Water in Ethanol and Hydrocarbon Blends by Karl Fischer Titration
Effective Date
15-Jul-2007
Referred By
ASTM D3120-08(2019) - Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
Effective Date
15-Jul-2007

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ASTM D4806-07 - Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine FuelASTM D4806-07 - Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
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ASTM D4806-07 - Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
An American National Standard
Designation: D 4806 – 07
Standard Specification for
Denatured Fuel Ethanol for Blending with Gasolines for Use
1
as Automotive Spark-Ignition Engine Fuel
This standard is issued under the fixed designation D 4806; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope* D 4057 Practice for Manual Sampling of Petroleum and
Petroleum Products
1.1 This specification covers nominally anhydrous dena-
D 4177 Practice for Automatic Sampling of Petroleum and
tured fuel ethanol intended to be blended with unleaded or
Petroleum Products
leaded gasolines at 1 to 10 volume % for use as a spark-
D 4306 Practice for Aviation Fuel Sample Containers for
ignition automotive engine fuel. The significance of this
Tests Affected by Trace Contamination
specification is shown in Appendix X1.
D 4814 SpecificationforAutomotiveSpark-IgnitionEngine
1.2 The values stated in SI units are to be regarded as the
Fuel
standard. The values given in parentheses are for information
D 5453 Test Method for Determination of Total Sulfur in
only.
Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel
2. Referenced Documents
Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
2
D 5501 Test Method for Determination of Ethanol Content
2.1 ASTM Standards:
of Denatured Fuel Ethanol by Gas Chromatography
D86 Test Method for Distillation of Petroleum Products at
D 5580 Test Method for Determination of Benzene, Tolu-
Atmospheric Pressure
ene, Ethylbenzene, p/m-Xylene, o-Xylene, C and Heavier
D 381 Test Method for Gum Content in Fuels by Jet 9
Aromatics, and Total Aromatics in Finished Gasoline by
Evaporation
Gas Chromatography
D 512 Test Methods for Chloride Ion In Water
D 5854 Practice for Mixing and Handling of Liquid
D 891 Test Methods for Specific Gravity, Apparent, of
Samples of Petroleum and Petroleum Products
Liquid Industrial Chemicals
D 6423 Test Method for Determination of pHe of Ethanol,
D 1152 Specification for Methanol (Methyl Alcohol)
Denatured Fuel Ethanol, and Fuel Ethanol (Ed75-Ed85)
D 1193 Specification for Reagent Water
D 6428 Test Method for Total Sulfur in Liquid Aromatic
D 1613 Test Method for Acidity in Volatile Solvents and
Hydrocarbons and Their Derivatives by Oxidative Com-
Chemical Intermediates Used in Paint, Varnish, Lacquer,
3
bustion and Electrochemical Detection
and Related Products
D 6550 Test Method for Determination of Olefin Content of
D 1688 Test Methods for Copper in Water
Gasolines by Supercritical-Fluid Chromatography
D 2622 Test Method for Sulfur in Petroleum Products by
D 7318 Test Method for Total Inorganic Sulfate in Ethanol
Wavelength Dispersive X-ray Fluorescence Spectrometry
by Potentiometric Titration
D 3120 Test Method for Trace Quantities of Sulfur in Light
D 7319 Test Method for Determination of Total and Poten-
Liquid Petroleum Hydrocarbons by Oxidative Microcou-
tial Sulfate and Inorganic Chloride in Fuel Ethanol by
lometry
Direct Injection Suppressed Ion Chromatography
D 3505 Test Method for Density or Relative Density of
D 7328 Test Method for Determination of Total and Poten-
Pure Liquid Chemicals
tial Inorganic Sulfate and Total Inorganic Chloride in Fuel
D 4052 Test Method for Density and Relative Density of
Ethanol by Ion Chromatography Using Aqueous Sample
Liquids by Digital Density Meter
Injection
E29 Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
1
This specification is under the jurisdiction of ASTM Committee D02 on
E 203 TestMethodforWaterUsingVolumetricKarlFischer
Petroleum Products and Lubricants and is the direct responsibility of Subcommittee
D02.A0.01 on Gasoline and Gasoline-Oxygenate Blends.
Titration
Current edition approved July 15, 2007. Published August 2007. Originally
E 300 Practice for Sampling Industrial Chemicals
approved in 1988. Last previous edition approved in 2006 as D 4806–06c.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
3
the ASTM website. Withdrawn.
*ASummary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D4806–07
E 1064 Test Method for Water in Organic Liquids by
Ethanol, volume %, min 92.1
Methanol, volume %, max 0.5
Coulometric Karl Fischer Titration
Solvent-washed gum, 5.0
2.2 Other Standards:
mg/100 mL, max
Water conten
...

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Section  
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Referenced Documents  
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4  
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5  
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6  
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Annexes  
Safety Precautions  
Annex A1  
Intake Air Aftercooler  
Annex A2  
The Cummins ISB Engine Build Parts Kit  
Annex A3  
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Annex A4  
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Annex A5  
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Annex A6  
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Annex A8  
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Annex A9  
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Petroleum Products  
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(approximate)  
A  
Light Distillates  
15–260 (60–500)  
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Gas Oils  
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C  
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510+ (950+ )  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. The preferred units are mass %.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Sections 7.2 and 7.4.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D8252-23(Test Method)
Standard Test Method for Vanadium and Nickel in Crude and Residual Oil by X-ray Spectrometry

SIGNIFICANCE AND USE
5.1 This test method provides a rapid and precise elemental measurement with simple sample preparation. Typical analysis times are approximately 4 min to 5 min per sample with a preparation time of approximately 1 min to 3 min per sample.  
5.2 The quality of crude oil is related to the amount of sulfur present. Knowledge of the vanadium and nickel concentration is necessary for processing purposes as well as contractual agreements.  
5.3 The presence of vanadium and nickel presents significant risks for contamination of the cracking catalysts in the refining process.  
5.4 This test method provides a means of determining whether the vanadium and nickel content of crude meets the operational limits of the refinery and whether the metal content will have a deleterious effect on the refining process or when used as a fuel.
SCOPE
1.1 This test method covers the quantitative determination of total vanadium and nickel in crude and residual oil in the concentration ranges shown in Table 1 using X-ray fluorescence (XRF) spectrometry.  
1.2 Sulfur is measured for analytical purposes only for the compensation of X-ray absorption matrix effects affecting the vanadium and nickel X-rays. For measurement of sulfur by standard test method use Test Methods D4294, D2622 or other suitable standard test method for sulfur in crude and residual oils.  
1.3 This test method is limited to the use of X-ray fluorescence (XRF) spectrometers employing an X-ray tube for excitation in conjunction with wavelength dispersive detection system or energy dispersive high resolution semiconductor detector with the ability to separate signals of adjacent and near-adjacent elements.  
1.4 This test method uses inter-element correction factors calculated from XRF theory, the fundamental parameters (FP) approach, or best fit regression.  
1.5 Samples containing higher concentrations than shown in Table 1 must be diluted to bring the elemental concentration of the diluted material within the scope of this test method.  
1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6.1 The preferred concentrations units are mg/kg for vanadium and nickel.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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