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ASTM E539-02

(Test Method)

Standard Test Method for X-Ray Emission Spectrometric Analysis of 6AI-4V Titanium Alloy

Standard Test Method for X-Ray Emission Spectrometric Analysis of 6AI-4V Titanium Alloy

SCOPE
1.1 This test method covers the X-ray emission analysis of 6Al-4V titanium alloy for the following elements in the ranges indicated (Note 1): ElementConcentration Range, %Aluminum4.6 to 7.2Vanadium2.6 to 5.4Iron0.1 to 0.3
Note 1—The concentration ranges can be extended by use of suitable reference materials. The ranges for aluminum and vanadium represent the actual concentration ranges of the NIST Standard Reference Materials used when this method was tested. The maximum concentrations of the unknowns used in the cooperative test program were all lower than the reference materials. The iron concentration range was determined by in-house reference materials used by the cooperating laboratories.
1.2 This test method is designed for control analysis in the production of titanium alloys and for inspection testing of the product shipped to the consumer. It is applicable for analyzing cast or wrought samples having a diameter of approximately 32 mm and a thickness of approximately 25 mm.
Note 2—Samples of greater or lesser size than the size designed may be used with specially designed sample holders.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.

General Information

Status
Historical
Publication Date
09-Mar-2002
ICS
71.040.50 - Physicochemical methods of analysis
77.120.50 - Titanium and titanium alloys
Technical Committee
E01 - Analytical Chemistry for Metals, Ores, and Related Materials
Drafting Committee
E01.06 - Ti, Zr, W, Mo, Ta, Nb, Hf, Re
Current Stage
Ref Project

Relations

Replaces
ASTM E539-90(1996)e1 - Standard Test Method for X-Ray Emission Spectrometric Analysis of 6AI-4V Titanium Alloy
Effective Date
10-Mar-2002
Replaced By
ASTM E539-06 - Standard Test Method for X-Ray Emission Spectrometric Analysis of 6Al-4V Titanium Alloy
Effective Date
01-Dec-2006
Referred By
ASTM B863-19 - Standard Specification for Titanium and Titanium Alloy Wire
Effective Date
10-Mar-2002
Referred By
ASTM B862-19 - Standard Specification for Titanium and Titanium Alloy Welded Pipe
Effective Date
10-Mar-2002
Referred By
ASTM F1472-23 - Standard Specification for Wrought Titanium-6Aluminum-4Vanadium Alloy for Surgical Implant Applications (UNS R56400)
Effective Date
10-Mar-2002
Referred By
ASTM F2924-14(2021) - Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium with Powder Bed Fusion
Effective Date
10-Mar-2002
Referred By
ASTM B265-20a - Standard Specification for Titanium and Titanium Alloy Strip, Sheet, and Plate
Effective Date
10-Mar-2002
Referred By
ASTM B381-21 - Standard Specification for Titanium and Titanium Alloy Forgings
Effective Date
10-Mar-2002
Referred By
ASTM F90-23 - Standard Specification for Wrought Cobalt-20Chromium-15Tungsten-10Nickel Alloy for Surgical Implant Applications (UNS R30605)
Effective Date
10-Mar-2002
Referred By
ASTM F2989-21 - Standard Specification for Metal Injection Molded Unalloyed Titanium Components for Surgical Implant Applications
Effective Date
10-Mar-2002
Referred By
ASTM F620-20 - Standard Specification for Titanium Alloy Forgings for Surgical Implants in the Alpha Plus Beta Condition
Effective Date
10-Mar-2002
Referred By
ASTM F3049-14(2021) - Standard Guide for Characterizing Properties of Metal Powders Used for Additive Manufacturing Processes
Effective Date
10-Mar-2002
Referred By
ASTM B348/B348M-21 - Standard Specification for Titanium and Titanium Alloy Bars and Billets
Effective Date
10-Mar-2002
Referred By
ASTM F3001-14(2021) - Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium ELI (Extra Low Interstitial) with Powder Bed Fusion
Effective Date
10-Mar-2002
Referred By
ASTM B861-19 - Standard Specification for Titanium and Titanium Alloy Seamless Pipe
Effective Date
10-Mar-2002

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ASTM E539-02 - Standard Test Method for X-Ray Emission Spectrometric Analysis of 6AI-4V Titanium AlloyASTM E539-02 - Standard Test Method for X-Ray Emission Spectrometric Analysis of 6AI-4V Titanium Alloy
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ASTM E539-02 - Standard Test Method for X-Ray Emission Spectrometric Analysis of 6AI-4V Titanium Alloy
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:E539–02
Standard Test Method for
X-Ray Emission Spectrometric Analysis of 6AI-4V Titanium
1
Alloy
This standard is issued under the fixed designation E 539; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
1.1 This test method covers the X-ray emission analysis of 2.1 ASTM Standards:
6Al-4V titanium alloy for the following elements in the ranges E 120 Test Methods for ChemicalAnalysis of Titanium and
3
indicated (Note 1): Titanium Alloys
E 135 Terminology Relating to Analytical Chemistry for
Element Concentration Range, %
3
Metals, Ores, and Related Materials
Aluminum 4.6 to 7.2
Vanadium 2.6 to 5.4
3. Terminology
Iron 0.1 to 0.3
3.1 Definitions:
NOTE 1—The concentration ranges can be extended by use of suitable
3.1.1 Refer to Terminology E 135.
reference materials. The ranges for aluminum and vanadium represent the
2
actual concentration ranges of the NIST Standard Reference Materialst
4. Summary of Test Method
used when this method was tested. The maximum concentrations of the
unknowns used in the cooperative test program were all lower than the
4.1 The sample is finished to a clean, uniform surface and
reference materials. The iron concentration range was determined by
then irradiated by an X-ray beam of high energy (short
in-house reference materials used by the cooperating laboratories.
wavelength). The secondary X rays produced are dispersed by
1.2 This test method is designed for control analysis in the means of crystals and the intensities measured by detectors at
production of titanium alloys and for inspection testing of the
selected wavelengths. The outputs of the detectors in voltage
product shipped to the consumer. It is applicable for analyzing pulses are integrated or counted. Data are collected using time
castorwroughtsampleshavingadiameterofapproximately32
requiredtoreachafixednumberofcountsorusingtotalcounts
mm and a thickness of approximately 25 mm. for a fixed time. Concentrations of the elements are determined
by relating the measured radiation of unknown samples to
NOTE 2—Samples of greater or lesser size than the size designed may
analytical curves or charts prepared from certified reference
be used with specially designed sample holders.
materials of known compositions.Afixed channel or polychro-
1.3 This standard does not purport to address all of the
mator system or a sequential system may be used to provide
safety concerns, if any, associated with its use. It is the
simultaneous or sequential determinations of elements.
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
5. Significance and Use
bility of regulatory limitations prior to use. Specific precau-
5.1 The chemical composition of 6A1-4V titanium alloy
tionary statements are given in Section 8.
must be accurately determined to ensure the desired metallur-
gical properties. This test method is suitable for manufacturing
control and inspection testing.
1
This test method is under the jurisdiction of ASTM Committee E01 on
Analytical Chemistry for Metals, Ores and Related Materials and is the direct 6. Apparatus
responsibility of Subcommittee E1.06 on Ti, Zr, W, Mo, Ta, Nb, Hf.
NOTE 3—It is not within the scope of this test method to prescribe all
Current edition approved March 10, 2002. Published March 2002. Originally
e1
published as E 539 – 75. Last previous edition E 539 – 90 (1996) . details of equipment to be used. Equipment varies between laboratories.
2
NIST Standard Reference Materialst used when this study include NIST
SRMt 653, 654, and 655 from NIST SRMt Program, 100 Bureau Drive, Mail Stop
3
2322, Building 202, Room 204, Gaithersburg, MP 20899–2322. Annual Book of ASTM Standards, Vol 03.05.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
E539–02
6.1 Sample Preparation Equipment: eter installations. It is also recommended that personnel follow
6.1.1 Surface Grinder, with 60 to 600-grit silicon carbide the guidelines of safe operating procedures given in the NIST
5
belts or disks capable of providing test specimens with a Handbook X-Ray Protection, HB76, the booklet Radiation
uniform flat finish. A wet belt or wet disk grinder is preferred Safety Recommendations for X-Ray Diffraction and Spectro-
6
to prevent work hardening of the sample. graphicEquipment,#MORP68-14,1968, byT.M.Mooreand
6.2 Excitation Source: D. J. McDonald, and the U. S. Government Handbook 93,
6.2.1 X-Ray G
...

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5.1 This test method for the chemical analysis of titanium and titanium alloys is primarily intended to test material for compliance with specifications of chemical composition such as those under the jurisdiction of ASTM Committee B10. It may also be used to test compliance with other specifications that are compatible with the test method.  
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1.1 This method describes the analysis of titanium and titanium alloys, such as specified by committee B10, by inductively coupled plasma atomic emission spectrometry (ICP-AES) and direct current plasma atomic emission spectrometry (DCP-AES) for the following elements:    
Element  
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Aluminum  
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Boron  
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Copper  
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Manganese  
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Molybdenum  
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5.1 This method is suitable for providing data on the chemical composition of titanium alloys having compositions within the scope of the standard. It is intended for routine production control and for determination of chemical composition for the purpose of certifying material specification compliance. Additionally, the analytical performance data included with this method may be used as a benchmark to determine if similar X-ray spectrometers provide equivalent precision and accuracy.  
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1.1 This test method2 covers the X-ray fluorescence analysis of titanium alloys for the following elements in the ranges indicated:    
Element  
Range, %  
Aluminum  
0.041 to 8.00  
Chromium  
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Copper  
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Iron  
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Nickel  
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Standard Specification for Semi-Rigid, Closed-Cell Polypropylene Foam, Preformed Expansion Joint Fillers for Concrete Paving and Structural Construction

SCOPE
1.1 This specification covers preformed expansion joint fillers made from closed-cell polypropylene foam materials having suitable compressibility, recovery from compression, nonextruding, and weather-resistant characteristics.  
1.1.1 Type I, closed-cell polypropylene foam.  
1.2 These joint fillers are intended for use in concrete pavements in full-depth joints. There are several variations in size with typical thicknesses of 1/2 in. (12.7 mm), 3/4 in. (19.05 mm), and 1 in. (25.4 mm); typical widths of 31/2 in. (88.9 mm), 4 in. (101.6 mm), 5 in. (127 mm), 6 in. (152.5 mm), 7 in. (177.8 mm), 8 in. (203.2 mm), or 48 in. (1.2 m) sheet; and typical lengths of 5 ft (1.52 m) and 10 ft (3.05 m).  
1.3 The values stated in inch-pound units are to be regarded as the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Technical specification
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  • Technical specification
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ASTM
ASTM F3337-23(Guide)
Standard Guide for Taking Property and Behavior Measurements on Weathered Fractions of Oil

SIGNIFICANCE AND USE
5.1 A standard procedure is necessary to establish property changes for spilled oils or petroleum products at different oil weathering stages.  
5.2 This procedure employs standardized equipment, and test procedures.  
5.3 This procedure should be performed at the stages of weathering corresponding to the spill conditions of interest.
SCOPE
1.1 This guide summarizes methods to fractionate oil by evaporative weathering and then measure the properties and behavior of the weathered oil. The results of this guide can provide oil behavior data for input into oil spill models and response method selection.  
1.2 This guide covers general procedures for oil weathering and behavior and does not cover all possible procedures which may be applicable to this topic.  
1.3 The results obtained using this guide are intended to provide baseline data for the behavior of oil and petroleum products when spilled and input to oil spill models.  
1.4 The results obtained using this guide can be used directly to predict certain facets of oil spill behavior or as input to oil spill models.  
1.5 The accuracy of the guide depends very much on the representative nature of the oil sample used. Certain oils can have different properties depending on their chemical contents at the moment a sample is taken.  
1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Guide
    4 pages
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  • Guide
    4 pages
    English language
    sale 15% off