Standard Test Method for Monotonic Equibiaxial Flexural Strength of Advanced Ceramics at Ambient Temperature

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1.1 This standard test method covers the determination of the equibiaxial strength of advanced ceramics at ambient temperature via concentric ring configurations under monotonic uniaxial loading. In addition, test specimen fabrication methods, testing modes, testing rates, allowable deflection, and data collection and reporting procedures are addressed. Two types of test specimens are considered: machined specimens and as-fired specimens exhibiting a limited degree of warpage. Strength as used in this test method refers to the maximum strength obtained under monotonic application of load. Monotonic loading refers to a test conducted at a constant rate in a continuous fashion, with no reversals from test initiation to final fracture.
1.2 This test method is intended primarily for use with advanced ceramics that macroscopically exhibit isotropic, homogeneous, continuous behavior. While this test method is intended for use on monolithic advanced ceramics, certain whisker- or particle-reinforced composite ceramics as well as certain discontinuous fiber-reinforced composite ceramics may also meet these macroscopic behavior assumptions. Generally, continuous fiber ceramic composites do not macroscopically exhibit isotropic, homogeneous, continuous behavior, and the application of this test method to these materials is not recommended.
1.3 Values expressed in this test method are in accordance with the International System of Units (SI) and Practice E 380.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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09-Oct-2002
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ASTM C1499-02 - Standard Test Method for Monotonic Equibiaxial Flexural Strength of Advanced Ceramics at Ambient Temperature
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NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
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Designation: C 1499 – 02
Standard Test Method for
Monotonic Equibiaxial Flexural Strength of Advanced
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Ceramics at Ambient Temperature
This standard is issued under the fixed designation C 1499; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope C 1239 Reporting Uniaxial Strength Data and Estimating
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Weibull Distribution Parameters for Advanced Ceramics
1.1 This standard test method covers the determination of
C 1259 Test Method for Dynamic Young’s Modulus, Shear
the equibiaxial strength of advanced ceramics at ambient
Modulus and Poisson’s Ratio for Advanced Ceramics by
temperature via concentric ring configurations under mono-
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Impulse Excitation of Vibration
tonic uniaxial loading. In addition, test specimen fabrication
C 1322 Practice for Fractography and Characterization of
methods, testing modes, testing rates, allowable deflection, and
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Fracture Origins in Advanced Ceramics
data collection and reporting procedures are addressed. Two
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E 4 Practices for Load Verification of Testing Machines
types of test specimens are considered: machined specimens
E 6 Terminology Relating to Methods of Mechanical Test-
and as-fired specimens exhibiting a limited degree of warpage.
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ing
Strength as used in this test method refers to the maximum
E 83 Practice for Verification and Classification of Exten-
strength obtained under monotonic application of load. Mono-
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someters
tonic loading refers to a test conducted at a constant rate in a
E 337 Test Method for Measured Humidity with Psychrom-
continuous fashion, with no reversals from test initiation to
eter (The Measurement of Wet-and Dry-Bulb Tempera-
final fracture.
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tures)
1.2 This test method is intended primarily for use with
E 380 Practice for Use of International System of Units (SI)
advanced ceramics that macroscopically exhibit isotropic,
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(the Modernized Metric System)
homogeneous, continuous behavior. While this test method is
F 394 Test Method for Biaxial Flexure Strength of Ceramic
intended for use on monolithic advanced ceramics, certain
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Substrates
whisker- or particle-reinforced composite ceramics as well as
certain discontinuous fiber-reinforced composite ceramics may
3. Terminology
also meet these macroscopic behavior assumptions. Generally,
3.1 Definitions—The definitions of terms relating to biaxial
continuous fiber ceramic composites do not macroscopically
testing appearing in Terminology E 6 and Terminology C 1145
exhibit isotropic, homogeneous, continuous behavior, and the
may apply to the terms used in this test method. Pertinent
application of this test method to these materials is not
definitions are listed below with the appropriate source given in
recommended.
parentheses. Additional terms used in conjunction with this test
1.3 Values expressed in this test method are in accordance
method are defined in the following section.
with the International System of Units (SI) and Practice E 380.
3.1.1 advanced ceramic, n—a highly engineered, high per-
1.4 This standard does not purport to address all of the
formance predominately non- metallic, inorganic, ceramic
safety concerns, if any, associated with its use. It is the
material having specific functional attributes. C 1145
responsibility of the user of this standard to establish appro-
3.1.2 breaking load, [F], n—the load at which fracture
priate safety and health practices and determine the applica-
occurs. E6
bility of regulatory limitations prior to use.
3.1.3 equibiaxial flexural strength, [F/L ], n—the maximum
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2. Referenced Documents stress that a material is capable of sustaining when subjected to
flexure between two concentric rings. This mode of flexure is
2.1 ASTM Standards:
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a cupping of the circular plate caused by loading at the inner
C 1145 Terminology on Advanced Ceramics
load ring and outer support ring. The equibiaxial flexural
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This test method is under the jurisdiction of ASTM Committee C28 on
Advanced Ceramics and is the direct responsibility of Subcommittee C28.01 on
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Properties and Performance. Annual Book of ASTM Standards, Vol 03.01.
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Current edition approved October 10, 2002. Published January 2003. Originally Annual Book of ASTM Standards, Vol 07.01, 11.03, 15.09.
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published in 2001. Last previous edition approved in 2001 as C 1499–01. Annual Book of ASTM Standards, Vol 14.02.
2 6
Annual Book of ASTM Standards, Vol 15.01. Annual Book of ASTM Standards, Vol 15.02.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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