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ASTM D803-12

(Test Method)

Standard Test Methods for Testing Tall Oil

Standard Test Methods for Testing Tall Oil

SIGNIFICANCE AND USE
3.1 Tall oil, both crude and refined, is an important by-product of the alkaline (kraft) pulping of pine wood. It consists primarily of fatty acids, resin acids, and neutral materials; the levels of these various components depend on factors such as the species of pine tree, geographic location, climate, etc.  
3.1.1 Tall oil is used primarily as a commercial source of fatty acids and rosin, and, therefore, reliable methods for the analysis of these components is necessary.
SCOPE
1.1 These test methods cover the test procedures to be applied to whole tall oils or refined tall oils. Previous editions of these test methods have described test procedures that are used to test tall oil fatty acid, rosin, and other tall oil-derived products as well as test crude and refined tall oil. Consequently, these test methods are widely cited in reference books and industry literature for the testing of tall oil-derived products.  
1.1.1 In this current revision, procedural details of some of the often-cited test methods have been removed and the test methods consolidated with other existing test methods. In such cases the consolidated methods, applicable to all tall oil-derived products.  
1.2 The procedures appear in the following order:    
Physical Tests  
Sections  
Viscosity:  
Brookfield Method (Preferred Method)  
7  
Bubble Time Method  
8  
Flash Point  
9  
Color  
10  
Moisture:  
11  
Insoluble Matter  
12  
Ash  
13  
Chemical Analysis  
Acid Number  
16  
Saponification Number  
17  
Rosin Acids  
18  
Unsaponifiable Matter  
19  
Fatty Acids  
20
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Oct-2012
ICS
87.060.20 - Binders
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.34 - Pine Chemicals and Hydrocarbon Resins
Current Stage
Ref Project

Relations

Replaces
ASTM D803-03(2008) - Standard Test Methods for Testing Tall Oil
Effective Date
01-Nov-2012
Referred By
ASTM D890-12(2022) - Standard Test Method for Water in Liquid Pine Chemicals
Effective Date
01-Nov-2012
Referred By
ASTM D465-15(2020) - Standard Test Methods for Acid Number of Pine Chemical Products Including Tall Oil and Other Related Products
Effective Date
01-Nov-2012
Referred By
ASTM D464-15(2020) - Standard Test Methods for Saponification Number of Pine Chemical Products Including Tall Oil and Other Related Products
Effective Date
01-Nov-2012
Referred By
ASTM E203-23 - Standard Test Method for Water Using Volumetric Karl Fischer Titration
Effective Date
01-Nov-2012
Referred By
ASTM D1065-18(2022) - Standard Test Method for Unsaponifiable Matter in Pine Chemicals, Including Rosin, Tall Oil, and Related Products
Effective Date
01-Nov-2012
Referred By
ASTM D1585-15(2020) - Standard Test Methods for Fatty Acids Content of Pine Chemicals, Including Rosin, Tall Oil, and Related Products
Effective Date
01-Nov-2012
Referred By
ASTM D802-02(2022) - Standard Test Methods for Sampling and Testing Pine Oils
Effective Date
01-Nov-2012

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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D803 − 12
StandardTest Methods for
1
Testing Tall Oil
This standard is issued under the fixed designation D803; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
2
2.1 ASTM Standards:
1.1 These test methods cover the test procedures to be
D92 Test Method for Flash and Fire Points by Cleveland
applied to whole tall oils or refined tall oils. Previous editions
Open Cup Tester
of these test methods have described test procedures that are
D93 Test Methods for Flash Point by Pensky-Martens
used to test tall oil fatty acid, rosin, and other tall oil-derived
Closed Cup Tester
productsaswellastestcrudeandrefinedtalloil.Consequently,
D269 Test Method for Insoluble Matter in Rosin and Rosin
these test methods are widely cited in reference books and
Derivatives
industry literature for the testing of tall oil-derived products.
D464 Test Methods for Saponification Number of Naval
1.1.1 In this current revision, procedural details of some of
Store Products Including Tall Oil and Other Related
the often-cited test methods have been removed and the test
Products
methods consolidated with other existing test methods. In such
D465 Test Methods for Acid Number of Naval Stores
cases the consolidated methods, applicable to all tall oil-
Products Including Tall Oil and Other Related Products
derived products.
D890 Test Method for Water in Liquid Naval Stores
1.2 The procedures appear in the following order:
D1065 Test Method for Unsaponifiable Matter in Naval
Physical Tests Sections
Stores, Including Rosin, Tall Oil, and Related Products
Viscosity:
D1240 Test Methods for Rosin Acids Content of Naval
Brookfield Method (Preferred Method) 7
Stores, Including Rosin, Tall Oil, and Related Products
Bubble Time Method 8
Flash Point 9
D1466 Test Method for Sampling Liquid Oils and Fatty
Color 10
Acids Commonly Used in Paints, Varnishes, and Related
Moisture: 11
3
Insoluble Matter 12 Materials (Withdrawn 2003)
Ash 13
D1544 Test Method for Color ofTransparent Liquids (Gard-
Chemical Analysis
ner Color Scale)
Acid Number 16
Saponification Number 17 D1545 Test Method for Viscosity of Transparent Liquids by
Rosin Acids 18
Bubble Time Method
Unsaponifiable Matter 19
D1585 Test Methods for Fatty Acids Content of Naval
Fatty Acids 20
Stores, Including Rosin, Tall Oil, and Related Products
1.3 The values stated in inch-pound units are to be regarded
D2196 Test Methods for Rheological Properties of Non-
as standard. The values given in parentheses are mathematical
Newtonian Materials by Rotational (Brookfield type)
conversions to SI units that are provided for information only
Viscometer
and are not considered standard.
D3278 Test Methods for Flash Point of Liquids by Small
1.4 This standard does not purport to address all of the
Scale Closed-Cup Apparatus
safety concerns, if any, associated with its use. It is the
D5974 Test Methods for Fatty and Rosin Acids in Tall Oil
responsibility of the user of this standard to establish appro-
Fractionation Products by Capillary Gas Chromatography
priate safety and health practices and determine the applica-
D6166 Test Method for Color of Pine Chemicals and Re-
bility of regulatory limitations prior to use.
lated Products (Instrumental Determination of Gardner
Color)
1
These test methods are under the jurisdiction of ASTM Committee D01 on
2
Paint and Related Coatings, Materials, and Applications and are the direct For referenced ASTM standards, visit the ASTM website, www.astm.org, or
responsibility of Subcommittee D01.34 on Pine Chemicals and Hydrocarbon contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Resins. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved Nov. 1, 2012. Published December 2012. Originally the ASTM website.
3
approved in 1944. Last previous edition approved in 2008 as D803 – 03 (2008). The last approved version of this historical standard is referenced on
DOI: 10.1520/D0803-12. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D803 − 12
E300 Practice for Sampling Industrial Chemicals VISCOSITY BY THE BROOKFIELD METHOD
(Preferred Method)
3. Significance and Use
7. Procedure
3.1 Tall oil, both crude and refined, is an important by-
7.1 Determinetheviscosityincentipoiseinaccordancewith
product of the alkaline (kraft) pulping of pine wood. It consists
Test Methods D2196. The testing temperature shall be 210°F
primarily of fatty acid
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D803 − 03 (Reapproved 2008) D803 − 12
Standard Test Methods for
1
Testing Tall Oil
This standard is issued under the fixed designation D803; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 These test methods cover the test procedures to be applied to whole tall oils or refined tall oils. Previous editions of these
test methods have described test procedures that are used to test tall oil fatty acid, rosin, and other tall oil-derived products as well
as test crude and refined tall oil. Consequently, these test methods are widely cited in reference books and industry literature for
the testing of tall oil-derived products.
1.1.1 In this current revision, procedural details of some of the often-cited test methods have been removed and the test methods
consolidated with other existing test methods. In such cases the consolidated methods, applicable to all tall oil-derived products,
are referenced.products.
1.2 The procedures appear in the following order:
Physical Tests Sections
Viscosity:
Brookfield Method (Preferred Method) 7
Bubble Time Method 8
Flash Point 9
Color 10
Moisture: 11
Insoluble Matter 12
Ash 13
Chemical Analysis
Acid Number 16
Saponification Number 17
Rosin Acids 18
Unsaponifiable Matter 19
Fatty Acids 20
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical
conversions to SI units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D92 Test Method for Flash and Fire Points by Cleveland Open Cup Tester
D93 Test Methods for Flash Point by Pensky-Martens Closed Cup Tester
D269 Test Method for Insoluble Matter in Rosin and Rosin Derivatives
D464 Test Methods for Saponification Number of Naval Store Products Including Tall Oil and Other Related Products
D465 Test Methods for Acid Number of Naval Stores Products Including Tall Oil and Other Related Products
D890 Test Method for Water in Liquid Naval Stores
D1065 Test Method for Unsaponifiable Matter in Naval Stores, Including Rosin, Tall Oil, and Related Products
D1240 Test Methods for Rosin Acids Content of Naval Stores, Including Rosin, Tall Oil, and Related Products
1
These test methods are under the jurisdiction of ASTM Committee D01 on Paint and Related Coatings, Materials, and Applications and are the direct responsibility of
Subcommittee D01.34 on Naval StoresPine Chemicals and Hydrocarbon Resins.
Current edition approved June 1, 2008Nov. 1, 2012. Published June 2008December 2012. Originally approved in 1944. Last previous edition approved in 20032008 as
D803 – 03.D803 – 03 (2008). DOI: 10.1520/D0803-03R08.10.1520/D0803-12.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D803 − 12
D1466 Test Method for Sampling Liquid Oils and Fatty Acids Commonly Used in Paints, Varnishes, and Related Materials
3
(Withdrawn 2003)
D1544 Test Method for Color of Transparent Liquids (Gardner Color Scale)
D1545 Test Method for Viscosity of Transparent Liquids by Bubble Time Method
D1585 Test Methods for Fatty Acids Content of Naval Stores, Including Rosin, Tall Oil, and Related Products
D2196 Test Methods for Rheological Properties of Non-Newtonian Materials by Rotational (Brookfield type) Viscometer
D3278 Test Methods for Flash Point of Liquids by Small Scale Closed-Cup Apparatus
D5974 Test Methods for Fatty and Rosin Acids in Tall Oil Fractionation Products by Capillary Gas Chromatography
D6166 Test Method for Color of Naval StoresPine Chemicals and Related Products (Instrumental Determination of Gardner
Color)
E300 Practice for Sampling Industrial Chemicals
3. Significance and Use
...

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1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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