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ASTM D1960-86(1995)e1

(Test Method)

Standard Test Method for Loss on Heating of Drying Oils (Withdrawn 2003)

Standard Test Method for Loss on Heating of Drying Oils (Withdrawn 2003)

SCOPE
1.1 This test method covers the determination of moisture and any other material that is volatile under the conditions of the test. It is applicable to all natural drying oils.  Note 1-For solutions of drying oils in volatile organic solvents it is recommended that Test Methods D1259 or D1644 be used.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 5.
WITHDRAWN RATIONALE
This test method covers the determination of moisture and any other material that is volatile under the conditions of the test. It is applicable to all natural drying oils.
Formerly under the jurisdiction of Committee D01 on Paint and Related Coatings, Materials, and Applications, this test method was withdrawn in December 2003 in accordance with section 10.6.3.1 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.

General Information

Status
Withdrawn
Publication Date
31-Dec-1994
Withdrawal Date
14-Dec-2003
ICS
87.060.20 - Binders
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Current Stage
Ref Project

Relations

Referred By
ASTM D4140-07(2018) - Standard Guide for Determining Volatile and Nonvolatile Content of Driers, Drying Oils, Naval Stores, and Solvents
Effective Date
01-Jan-1995

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ASTM D1960-86(1995)e1 - Standard Test Method for Loss on Heating of Drying Oils (Withdrawn 2003)ASTM D1960-86(1995)e1 - Standard Test Method for Loss on Heating of Drying Oils (Withdrawn 2003)
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ASTM D1960-86(1995)e1 - Standard Test Method for Loss on Heating of Drying Oils (Withdrawn 2003)
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NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
e1
Designation: D 1960 – 86 (Reapproved 1995)
Standard Test Method for
Loss on Heating of Drying Oils
This standard is issued under the fixed designation D 1960; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
e NOTE—Keywords and an update statement on precision and bias were added editorially in May 1995.
1. Scope 4.3 Carbon Dioxide or Nitrogen Gas,(Warning—see 5.1)
under pressure in cylinders.
1.1 This test method covers the determination of moisture
and any other material that is volatile under the conditions of
5. Hazards
the test. It is applicable to all natural drying oils.
5.1 Carbon Dioxide and Nitrogen Gas—Gas supplied in
NOTE 1—For solutions of drying oils in volatile organic solvents it is
cylinders is dangerous because of its extremely high pressure.
recommended that Test Methods D 1259 or D 1644 be used.
Take care to prevent damage to cylinders, valves, and pressure
1.2 This standard does not purport to address all of the
regulators. Consult supplier’s Material Safety Data Sheet.
safety concerns, if any, associated with its use. It is the
6. Procedure
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
6.1 Weigh 10 g of sample to 0.1 mg, into a tared 50-mL
bility of regulatory limitations prior to use. Specific hazard flask. Heat in an air oven at 105 6 2°C for 30 min, while
statements are given in Section 5.
passing a gentle stream of carbon dioxide or nitrogen into the
neck of the flask.
2. Referenced Documents
NOTE 2—Care must be taken to keep the surface of the oil blanketed
2.1 ASTM Standards:
with inert gas throughout the test to prevent oxidation of the oil.
D 1259 Test Methods for Nonvolatile Content of Resin
6.2 Remove the flask from the oven, cool in a desiccator,
Solutions
2 and weigh to 0.1 mg.
D 1644 Test Methods for Nonvolatile Content of Varnishes
7. Calculation
3. Significance and Use
7.1 Calculate the percent loss on heating, L, as follows:
3.1 Drying oils may contain small amounts of residual
S 2 R
ext
...

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