Standard Test Method for Measuring Non-Fibrous Content of Man-Made Rock and Slag Mineral Fiber Insulation

SIGNIFICANCE AND USE
Inorganic fibrous thermal insulation can contain varying amounts of non-fibrous material. Non-fibrous material does not contribute to the insulating value of the insulation and therefore a procedure for determining that amount is desirable. Several specifications refer to shot content and percent (%) retained on various screen sizes determined by this test method.
SCOPE
1.1 This test method covers a procedure for determining the non-fibrous content (shot) of man-made rock and slag mineral fiber insulation. The procedure covers a dry sieve analysis method to distinguish between fiberized and non-fiberized (shot) portions of a specimen of man-made rock and slag mineral fiber insulation specimen.
1.2 This test method does not apply to rock or slag materials containing any components other than rock and slag mineral fiber and organic thermal setting binders. Products containing other types of fibers, inorganic binders, or refractory clays are excluded.
1.3 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
30-Nov-2004
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ASTM C1335-04 - Standard Test Method for Measuring Non-Fibrous Content of Man-Made Rock and Slag Mineral Fiber Insulation
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
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Designation:C1335–04
Standard Test Method for
Measuring Non-Fibrous Content of Man-Made Rock and
1
Slag Mineral Fiber Insulation
This standard is issued under the fixed designation C 1335; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 3. Terminology
1.1 This test method covers a procedure for determining the 3.1 Definitions—Terminology C 168 shall be considered as
non-fibrous content (shot) of man-made rock and slag mineral applying to the terms used in this test method.
fiber insulation. The procedure covers a dry sieve analysis 3.2 Definition of Term Specific to This Standard:
method to distinguish between fiberized and non-fiberized 3.2.1 shot—materialthatcannotbebrushedormechanically
(shot) portions of a specimen of man-made rock and slag shaken through a No. 100 (150 µm) sieve.
mineral fiber insulation specimen.
4. Significance and Use
1.2 This test method does not apply to rock or slag materials
4.1 Inorganic fibrous thermal insulation can contain varying
containing any components other than rock and slag mineral
fiber and organic thermal setting binders. Products containing amountsofnon-fibrousmaterial.Non-fibrousmaterialdoesnot
contributetotheinsulatingvalueoftheinsulationandtherefore
other types of fibers, inorganic binders, or refractory clays are
excluded. a procedure for determining that amount is desirable. Several
specifications refer to shot content and percent (%) retained on
1.3 The values stated in inch-pound units are to be regarded
as the standard. The values given in parentheses are for various screen sizes determined by this test method.
information only.
5. Apparatus
1.4 This standard does not purport to address all of the
5.1 Furnace, capable of maintaining 1100 6 10°F (593 6
safety concerns, if any, associated with its use. It is the
5.6°C) for rock and slag wool.
responsibility of the user of this standard to establish appro-
5.2 U.S.A. Standard Sieve Shaker Machine.
priate safety and health practices and determine the applica-
5.3 Balance Scale, capable of weighing to an accuracy of
bility of regulatory limitations prior to use.
0.00035 oz (0.01 g).
2. Referenced Documents
5.4 Sieves—Three8in.(203mm)diameterU.S.A.Standard
2
Sieves. Nos. 20 (850 µm), 50 (300 µm), and 100 (150 µm)
2.1 ASTM Standards:
C 168 Terminology Relating to Thermal Insulation nested in order with bottom receiver pan. All sieve design and
construction shall be in accordance with SpecificationE11.
C 390 Practice for Sampling and Acceptance of Preformed
Thermal Insulation Lots 5.5 Brush—Approximately 1 in. (25 mm) diameter plastic
bristle brush, and approximately 1 in. (25 mm) wide soft paint
E 11 Specification for Wire-Cloth Sieves for Testing Pur-
poses brush.
5.6 Crucible Weighing Dish, tared.
E 178 Practice for Dealing with Outlying Observations
E 691 Practice for Conducting an Interlaboratory Study to 5.7 Stoppers, rubber, No. 12 or 13.
5.8 Cork Borer, approximately 0.8 in. (20 mm) diameter.
Determine the Precision of a Test Method
6. Sampling and Preparation of Test Specimen
1
ThistestmethodisunderthejurisdictionofASTMCommitteeC16onThermal
6.1 For the purposes of standard tests, sampling shall be in
Insulation and is the direct responsibility of Subcommittee C16.32 on Mechanical
accordance with Practice C 390 and Practice E 178 with a
Properties.
Current edition approved Dec. 1, 2004. Published December 2004. Originally minimum of three specimens per lot to be tested.
approved in 1996. Last previous edition approved in 2002 as C 1335 – 96 (2002).
6.1.1 Specimen—This test method requires approximately a
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
0.35 oz (10 g) specimen.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
6.2 Specimen Preparation:
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

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C1335–04
6.2.1 Obtainarepresentativespecimenutilizinga0.8in.(20 8.2 Adding the total percentages of all WC (s) (minimum of
mm) cork borer for blanket or board and random specimens for three specimens/tests) and dividing by the number of WC (s)
loosefill.Firethespecimeninatareddishat1100 610°F(593
equals the average total percent of shot (shot content).
6 5.6°C) for 15 min. Remove tared dish with specimen and
allow to cool for approximately 20 min.
9. Report
6.2.2 Weigh the crucible weighing dish and fiber on balance
9.1 Report the following in
...

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