ASTM D8155-17
(Practice)Standard Practice for Shake Extraction of Solid Mining and Metallurgical Processing Waste with Water
Standard Practice for Shake Extraction of Solid Mining and Metallurgical Processing Waste with Water
SIGNIFICANCE AND USE
4.1 This practice is intended as a rapid means for obtaining an extract of solid waste. The extract may be used to estimate the release of constituents of the solid waste under the laboratory conditions described in this procedure.
4.1.1 This practice is not intended to be used as a kinetic test to simulate weathering of ore, metal mining, and metallurgical processing wastes. For kinetic testing of ore, metal mining, and metallurgical processing wastes, refer to Test Method D5744 to determine release rates for constituents of interest. For static testing of metal mining ore and metal mining or metallurgical processing waste materials, refer to Test Methods E1915 and D6234. If the conditions of this practice are not suitable for the test material, Test Method E2242 may be used, if applicable to the ore or waste.
4.2 This practice is not intended to provide an extract that is representative of the actual leachate produced from a solid waste in the field, or to produce extracts to be used as the sole basis of engineering design.
4.3 This practice is not intended to simulate site-specific leaching conditions. It has not been demonstrated to simulate actual disposal site leaching conditions.
4.4 The intent of this practice is that the final pH of the extract reflects the interaction of the extractant with the buffering capacity of the solid waste.
4.5 The intent of this practice is that the water extraction simulates conditions where the solid waste is the dominant factor in determining the pH of the extract.
4.6 The practice produces an extract that is amenable to the determination of both major and minor constituents. When minor constituents are being determined, it is especially important that precautions are taken in sample storage and handling to avoid possible contamination of the samples.
4.6.1 This practice has been tested to determine its applicability to certain inorganic components in metal mining and metallurgical processing wastes.
4....
SCOPE
1.1 This practice covers a procedure for leaching of solid waste to obtain an aqueous solution to be used to determine the constituents leached under the specified testing conditions.
1.1.1 This practice includes a procedure for the shake leaching of metal mining ore, waste rock, or metallurgical processing waste containing at least 80 % dry solids (≤20 % moisture) in order to generate a solution to be used to determine the inorganic constituents leached under the specified testing conditions and for regulatory jurisdictions requiring a water leach practice.
1.2 This practice provides for the shaking of a known mass of waste with water of specified composition and the separation of the aqueous phase for analysis.
1.2.1 This practice is intended to describe the procedure for performing single-batch extractions only. It does not describe all types of sampling, sample preservation, and analytical requirements that may be associated with its application.
1.3 The values stated in SI units are to be regarded as standard. Values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D8155 − 17
Standard Practice for
Shake Extraction of Solid Mining and Metallurgical
1
Processing Waste with Water
This standard is issued under the fixed designation D8155; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
2
2.1 ASTM Standards:
1.1 This practice covers a procedure for leaching of solid
C471M Test Methods for ChemicalAnalysis of Gypsum and
waste to obtain an aqueous solution to be used to determine the
Gypsum Products (Metric)
constituents leached under the specified testing conditions.
D75/D75M Practice for Sampling Aggregates
1.1.1 This practice includes a procedure for the shake
D420 Guide to Site Characterization for Engineering Design
leaching of metal mining ore, waste rock, or metallurgical
3
and Construction Purposes (Withdrawn 2011)
processing waste containing at least 80 % dry solids (≤20 %
D1193 Specification for Reagent Water
moisture) in order to generate a solution to be used to
D2216 Test Methods for Laboratory Determination of Water
determine the inorganic constituents leached under the speci-
(Moisture) Content of Soil and Rock by Mass
fiedtestingconditionsandforregulatoryjurisdictionsrequiring
D2234/D2234M Practice for Collection of a Gross Sample
a water leach practice.
of Coal
D3370 Practices for Sampling Water from Closed Conduits
1.2 This practice provides for the shaking of a known mass
D5681 Terminology for Waste and Waste Management
ofwastewithwaterofspecifiedcompositionandtheseparation
D5744 Test Method for Laboratory Weathering of Solid
of the aqueous phase for analysis.
Materials Using a Humidity Cell
1.2.1 This practice is intended to describe the procedure for
D6234 Test Method for Shake Extraction of Mining Waste
performing single-batch extractions only. It does not describe
by the Synthetic Precipitation Leaching Procedure
all types of sampling, sample preservation, and analytical
E122 Practice for Calculating Sample Size to Estimate,With
requirements that may be associated with its application.
Specified Precision, the Average for a Characteristic of a
Lot or Process
1.3 The values stated in SI units are to be regarded as
E877 Practice for Sampling and Sample Preparation of Iron
standard. Values given in parentheses are mathematical con-
Ores and Related Materials for Determination of Chemi-
versions to inch-pound units that are provided for information
cal Composition and Physical Properties
only and are not considered standard.
E1915 Test Methods forAnalysis of Metal Bearing Ores and
1.4 This standard does not purport to address all of the
Related Materials for Carbon, Sulfur, and Acid-Base
safety concerns, if any, associated with its use. It is the
Characteristics
responsibility of the user of this standard to establish appro-
E2242 Test Method for Column Percolation Extraction of
priate safety, health, and environmental practices and deter-
Mine Rock by the Meteoric Water Mobility Procedure
mine the applicability of regulatory limitations prior to use.
3. Terminology
1.5 This international standard was developed in accor-
dance with internationally recognized principles on standard-
3.1 For definitions of terms used in this practice, see
ization established in the Decision on Principles for the Terminology D5681.
Development of International Standards, Guides and Recom-
3.2 Definitions of Terms Specific to This Standard:
mendations issued by the World Trade Organization Technical
3.2.1 metal mining waste, n—overburden or waste rock
Barriers to Trade (TBT) Committee.
excavated and disposed of during mining operations.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
1
This practice is under the jurisdiction of ASTM Committee D34 on Waste contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Management and is the direct responsibility of Subcommittee D34.01.04 on Waste Standards volume information, refer to the standard’s Document Summary page on
Leaching Techniques. the ASTM website.
3
Current edition approved Dec. 15, 2017. Published December 2017. Originally The last approved version of this historical standard is referenced on
approved in 2017. DOI: 10.1520/D8155-17. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D8155 − 17
3.2.2 mineral processing waste, n—waste genera
...
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D8155 − 17
Standard Practice for
Shake Extraction of Solid Mining and Metallurgical
1
Processing Waste with Water
This standard is issued under the fixed designation D8155; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
2
2.1 ASTM Standards:
1.1 This practice covers a procedure for leaching of solid
C471M Test Methods for Chemical Analysis of Gypsum and
waste to obtain an aqueous solution to be used to determine the
Gypsum Products (Metric)
constituents leached under the specified testing conditions.
D75/D75M Practice for Sampling Aggregates
1.1.1 This practice includes a procedure for the shake
D420 Guide to Site Characterization for Engineering Design
leaching of metal mining ore, waste rock, or metallurgical
3
and Construction Purposes (Withdrawn 2011)
processing waste containing at least 80 % dry solids (≤20 %
D1193 Specification for Reagent Water
moisture) in order to generate a solution to be used to
D2216 Test Methods for Laboratory Determination of Water
determine the inorganic constituents leached under the speci-
(Moisture) Content of Soil and Rock by Mass
fied testing conditions and for regulatory jurisdictions requiring
D2234/D2234M Practice for Collection of a Gross Sample
a water leach practice.
of Coal
D3370 Practices for Sampling Water from Closed Conduits
1.2 This practice provides for the shaking of a known mass
D5681 Terminology for Waste and Waste Management
of waste with water of specified composition and the separation
D5744 Test Method for Laboratory Weathering of Solid
of the aqueous phase for analysis.
Materials Using a Humidity Cell
1.2.1 This practice is intended to describe the procedure for
D6234 Test Method for Shake Extraction of Mining Waste
performing single-batch extractions only. It does not describe
by the Synthetic Precipitation Leaching Procedure
all types of sampling, sample preservation, and analytical
E122 Practice for Calculating Sample Size to Estimate, With
requirements that may be associated with its application.
Specified Precision, the Average for a Characteristic of a
Lot or Process
1.3 The values stated in SI units are to be regarded as
E877 Practice for Sampling and Sample Preparation of Iron
standard. Values given in parentheses are mathematical con-
Ores and Related Materials for Determination of Chemi-
versions to inch-pound units that are provided for information
cal Composition and Physical Properties
only and are not considered standard.
E1915 Test Methods for Analysis of Metal Bearing Ores and
1.4 This standard does not purport to address all of the
Related Materials for Carbon, Sulfur, and Acid-Base
safety concerns, if any, associated with its use. It is the
Characteristics
responsibility of the user of this standard to establish appro-
E2242 Test Method for Column Percolation Extraction of
priate safety, health, and environmental practices and deter-
Mine Rock by the Meteoric Water Mobility Procedure
mine the applicability of regulatory limitations prior to use.
3. Terminology
1.5 This international standard was developed in accor-
dance with internationally recognized principles on standard-
3.1 For definitions of terms used in this practice, see
ization established in the Decision on Principles for the Terminology D5681.
Development of International Standards, Guides and Recom-
3.2 Definitions of Terms Specific to This Standard:
mendations issued by the World Trade Organization Technical
3.2.1 metal mining waste, n—overburden or waste rock
Barriers to Trade (TBT) Committee.
excavated and disposed of during mining operations.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
1
This practice is under the jurisdiction of ASTM Committee D34 on Waste contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Management and is the direct responsibility of Subcommittee D34.01.04 on Waste Standards volume information, refer to the standard’s Document Summary page on
Leaching Techniques. the ASTM website.
3
Current edition approved Dec. 15, 2017. Published December 2017. Originally The last approved version of this historical standard is referenced on
approved in 2017. DOI: 10.1520/D8155-17. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D8155 − 17
3.2.2 mineral processing waste, n—waste generated from sition suitable to the nature of the analyses to be performed and
ore processing metallurgical operation such as tailing
...
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