ASTM E2823-17
(Test Method)Standard Test Method for Analysis of Nickel Alloys by Inductively Coupled Plasma Mass Spectrometry (Performance-Based)
Standard Test Method for Analysis of Nickel Alloys by Inductively Coupled Plasma Mass Spectrometry (Performance-Based)
SIGNIFICANCE AND USE
5.1 This test method for the chemical analysis of nickel and nickel alloys is primarily intended to test material for compliance with specifications such as those under jurisdiction of ASTM committee B02. It may also be used to test compliance with other specifications that are compatible with the test method.
5.2 It is assumed that all who use this method will be trained analysts capable of performing common laboratory procedures skillfully and safely, and that the work will be performed in a properly equipped laboratory.
5.3 This is a performance-based method that relies more on the demonstrated quality of the test result than on strict adherence to specific procedural steps. It is expected that laboratories using this method will prepare their own work instructions. These work instructions will include detailed operating instructions for the specific laboratory, the specific reference materials employed, and performance acceptance criteria. It is also expected that, when applicable, each laboratory will participate in proficiency test programs, such as described in Practice E2027, and that the results from the participating laboratory will be satisfactory.
SCOPE
1.1 This test method describes the inductively coupled plasma mass spectrometric analysis of nickel and nickel allys, as specified by Committee B02, and having chemical compositions within the following limits:
Element
Application Range (Mass Fraction %)
Aluminum
0. 01–6.00
Boron
0. 01–0.10
Carbon
0. 01–0.15
Chromium
0. 01–33.00
Copper
0.01–35.00
Cobalt
0. 01–20.00
Iron
0.05–50.00
Magnesium
0. 01–0.020
Molybdenum
0. 01–30.0
Niobium
0. 01–6.0
Nickel
25.00–100.0
Phosphorous
0.001–0.025
Silicon
0.01–1.50
Sulfur
0.0001–0.01
Titanium
0.0001–6.0
Tungsten
0.01–5.0
Vanadium
0.0005–1.0
1.2 The following elements may be determined using this method.
Element
Quantification Range (μg/g)
Antimony
0.5–50
Bismuth
0.1–11
Gallium
2.9–54
Lead
0.4–21
Silver
1–35
Tin
2.2–97
Thallium
0.5–3.0
1.3 This method has only been interlaboratory tested for the elements and ranges specified. It may be possible to extend this method to other elements or different composition ranges provided that method validation that includes evaluation of method sensitivity, precision, and bias as described in this document is performed. Additionally, the validation study must evaluate the acceptability of sample preparation methodology using reference materials and/or spike recoveries. The user is cautioned to carefully evaluate the validation data as to the intended purpose of the analytical results. Guide E2857 provides additional guidance on method validation.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific safety hazard statements are given in Section 9.
General Information
Relations
Buy Standard
Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E2823 − 17
Standard Test Method for
Analysis of Nickel Alloys by Inductively Coupled Plasma
1
Mass Spectrometry (Performance-Based)
This standard is issued under the fixed designation E2823; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope using reference materials and/or spike recoveries. The user is
cautioned to carefully evaluate the validation data as to the
1.1 This test method describes the inductively coupled
intended purpose of the analytical results. Guide E2857 pro-
plasma mass spectrometric analysis of nickel and nickel allys,
vides additional guidance on method validation.
as specified by Committee B02, and having chemical compo-
1.4 This standard does not purport to address all of the
sitions within the following limits:
safety concerns, if any, associated with its use. It is the
Element Application Range (Mass
Fraction %) responsibility of the user of this standard to establish appro-
Aluminum 0. 01–6.00
priate safety and health practices and determine the applica-
Boron 0. 01–0.10
bility of regulatory limitations prior to use. Specific safety
Carbon 0. 01–0.15
Chromium 0. 01–33.00 hazard statements are given in Section 9.
Copper 0.01–35.00
Cobalt 0. 01–20.00
2. Referenced Documents
Iron 0.05–50.00
Magnesium 0. 01–0.020 2
2.1 ASTM Standards:
Molybdenum 0. 01–30.0
D1193 Specification for Reagent Water
Niobium 0. 01–6.0
Nickel 25.00–100.0
E29 Practice for Using Significant Digits in Test Data to
Phosphorous 0.001–0.025
Determine Conformance with Specifications
Silicon 0.01–1.50
E50 Practices for Apparatus, Reagents, and Safety Consid-
Sulfur 0.0001–0.01
Titanium 0.0001–6.0
erations for Chemical Analysis of Metals, Ores, and
Tungsten 0.01–5.0
Related Materials
Vanadium 0.0005–1.0
E55 Practice for Sampling Wrought Nonferrous Metals and
1.2 The following elements may be determined using this
Alloys for Determination of Chemical Composition
method.
E88 Practice for Sampling Nonferrous Metals andAlloys in
Element Quantification Range (µg/g)
Cast Form for Determination of Chemical Composition
Antimony 0.5–50
E135 Terminology Relating to Analytical Chemistry for
Bismuth 0.1–11
Gallium 2.9–54 Metals, Ores, and Related Materials
Lead 0.4–21
E177 Practice for Use of the Terms Precision and Bias in
Silver 1–35
ASTM Test Methods
Tin 2.2–97
Thallium 0.5–3.0 E691 Practice for Conducting an Interlaboratory Study to
Determine the Precision of a Test Method
1.3 This method has only been interlaboratory tested for the
E1329 Practice for Verification and Use of Control Charts in
elementsandrangesspecified.Itmaybepossibletoextendthis
Spectrochemical Analysis
method to other elements or different composition ranges
E1479 Practice for Describing and Specifying Inductively
provided that method validation that includes evaluation of
Coupled Plasma Atomic Emission Spectrometers
method sensitivity, precision, and bias as described in this
E1601 Practice for Conducting an Interlaboratory Study to
documentisperformed.Additionally,thevalidationstudymust
Evaluate the Performance of an Analytical Method
evaluate the acceptability of sample preparation methodology
E2027 Practice for Conducting Proficiency Tests in the
ChemicalAnalysis of Metals, Ores, and Related Materials
1
This test method is under the jurisdiction of ASTM Committee E01 on
Analytical Chemistry for Metals, Ores, and Related Materials and is the direct
2
responsibility of Subcommittee E01.08 on Ni and Co and HighTemperatureAlloys. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Jan. 1, 2017. Published February 2017. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 2011. Last previous edition approved in 2011 as E2823–11. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/E2823-17. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
E2823 − 17
E2165 Practice for Establishing an Uncertainty Budget for 6.2 The use of an internal standard may compensate for the
the Chemical Analysis of Metals, Ores, and Related physical interferences resulting from variations in sample and
3
Materials (Withdrawn 2007) calibrationsolutionaerosoltransportrates.Theusermaychose
E2857 Guide for Validating Analytical Methods to add the
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E2823 − 11 E2823 − 17
Standard Test Method for
Analysis of Nickel Alloys by Inductively Coupled Plasma
Mass Spectrometry (Performance-Based
1
Method)(Performance-Based)
This standard is issued under the fixed designation E2823; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method describes the inductively coupled plasma mass spectrometric analysis of nickel, nickel and nickel allys,
as specified by Committee B02, and having chemical compositions within the following limits:
Element Application Range (Wt. (Mass
Fraction %)
Aluminum 0. 01–6.00
Boron 0. 01–0.10
Carbon 0. 01–0.15
Chromium 0. 01–33.00
Copper 0.01–35.00
Cobalt 0. 01–20.00
Iron 0.05–50.00
Magnesium 0. 01–0.020
Molybdenum 0. 01–30.0
Niobium 0. 01–6.0
Nickel 25.00–100.0
Phosphorous 0.001–0.025
Silicon 0.01–1.50
Sulfur 0.0001–0.01
Titanium 0.0001–6.0
Tungsten 0.01–5.0
Vanadium 0.0005–1.0
1.2 The following elements may be determined using this method.
Element Quantification Range (μg/g)
Antimony 0.5–50
Bismuth 0.1–11
Gallium 2.9–54
Lead 0.4–21
Silver 1–35
Tin 2.2–97
Thallium 0.5–3.0
1.3 This method has only been interlaboratory tested for the elements and ranges specified. It may be possible to extend this
method to other elements or different composition ranges provided that method validation that includes evaluation of method
sensitivity, precision, and bias as described in this document is performed. Additionally, the validation study must evaluate the
acceptability of sample preparation methodology using reference materials and/or spike recoveries. The user is cautioned to
carefully evaluate the validation data as to the intended purpose of the analytical results. Guide E2857 provides additional guidance
on method validation.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use. Specific safety hazard statements are given in Section 9.
1
This test method is under the jurisdiction of ASTM Committee E01 on Analytical Chemistry for Metals, Ores, and Related Materials and is the direct responsibility of
Subcommittee E01.08 on Ni and Co and High Temperature Alloys.
Current edition approved May 1, 2011Jan. 1, 2017. Published July 2011February 2017. Originally approved in 2011. Last previous edition approved in 2011 as E2823–11.
DOI: 10.1520/E2823-11.10.1520/E2823-17.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
E2823 − 17
2. Referenced Documents
2
2.1 ASTM Standards:
D1193 Specification for Reagent Water
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E50 Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
E55 Practice for Sampling Wrought Nonferrous Metals and Alloys for Determination of Chemical Composition
E88 Practice for Sampling Nonferrous Metals and Alloys in Cast Form for Determination of Chemical Composition
E135 Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
E1329 Practice for Verification and Use of Control Charts in Spectrochemical Analysis
E1479 Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers
E1601 Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
E2027 Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials
E2165 Practice for Establishing an Uncertainty Budget for the Chemical Analysis of Metals, Ores, and Related Materials
3
(Withdrawn 2007)
E2857 Guide for Validating Analytical Methods
E2972 Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other
Related Materials
4
2.2 ISO Standards:
ISOISO/IEC 17025 General Requirements for the Competence of
...
Questions, Comments and Discussion
Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.