ASTM E753-80(1999)
(Specification)Specification for Municipal Aluminum Scrap (MAS) (Withdrawn 2001)
Specification for Municipal Aluminum Scrap (MAS) (Withdrawn 2001)
SCOPE
1.1 This specification covers municipal-refuse originated aluminum alloy scrap (MAS), not source-separated, that is recovered from industrial, commercial, or household wastes destined for disposal facilities.
1.2 Municipal aluminum scrap (MAS) covered by this specification is suitable for use by the following industries:
1.2.1 Secondary aluminum smelters,
1.2.2 Primary aluminum producers,
1.2.3 Aluminum scrap dealers,
1.2.4 Iron and steel industry,
1.2.5 Foundries,
1.2.6 Nonintegrated aluminum producers, and
1.2.7 Independent aluminum fabricators.
1.3 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. The hazard statement applies only to the test method sections in the annexes of this specification.
General Information
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Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
Designation: E 753 – 80 (Reapproved 1999)
Standard Specification for
Municipal Aluminum Scrap (MAS)
This standard is issued under the fixed designation E 753; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope E 227 Test Method for Optical Emission Spectrometric
Analysis of Aluminum and Aluminum Alloys by the
1.1 This specification covers municipal-refuse originated
Point-to-Plane Technique
aluminum alloy scrap (MAS), not source-separated, that is
E 276 Test Method for Particle Size or Screen Analysis at
recovered from industrial, commercial, or household wastes
No. 4 (4.75-mm) Sieve and Finer for Metal Bearing Ores
destined for disposal facilities.
and Related Materials
1.2 Municipal aluminum scrap (MAS) covered by this
specification is suitable for use by the following industries:
3. Terminology
1.2.1 Secondary aluminum smelters,
3.1 Definitions of Terms Specific to This Standard:
1.2.2 Primary aluminum producers,
3.1.1 combustible material (organic)—material that is mea-
1.2.3 Aluminum scrap dealers,
sured by weight loss of a dried sample input after heating to red
1.2.4 Iron and steel industry,
heat in an open crucible in a vented furnace. Combustibles
1.2.5 Foundries,
include both loose organics and organic coatings.
1.2.6 Nonintegrated aluminum producers, and
3.1.2 loose combustible material (organic)—loose combus-
1.2.7 Independent aluminum fabricators.
tible organics (LCO) that consist of, but are not limited to,
1.3 The values stated in inch-pound units are to be regarded
nonmetallic materials such as paper, rags, plastic, rubber,
as the standard. The values given in parentheses are for
wood, food wastes, and yard or lawn wastes, etc., which are not
information only.
permanently attached to noncombustible objects. The LCOs
1.4 This standard does not purport to address all of the
are defined as material larger than 12 mesh (U.S. Standard
safety concerns, if any, associated with its use. It is the
Sieve). A determination of LCOs is best done by sampling the
responsibility of the user of this standard to establish appro-
material and handpicking, handcleaning, and visually identify-
priate safety and health practices and determine the applica-
ing the materials described previously.
bility of regulatory limitations prior to use. The hazard
3.1.3 moisture percent—liquid content, as determined by
statement applies only to the test method sections in the
weight loss when sample material is dried to a constant weight
annexes of this specification.
at 110° 6 5°C.
2. Referenced Documents 3.1.4 recovery—the percent material recovered after an
assay using the procedures prescribed in this specification.
2.1 ASTM Standards:
D 2013 Test Method for Preparing Coal Samples for Analy-
4. Classification
sis
4.1 This specification covers two classes based on fines
E 11 Specification for Wire-Cloth Sieves for Testing Pur-
3 content (7.2) and six grades based on chemical composition of
poses
MAS material, as listed in Table 1 (see also 7.2).
E 34 Test Methods for Chemical Analysis of Aluminum and
Aluminum Alloys
5. Ordering Information
E 101 Test Method for Spectrographic Analysis of Alumi-
5.1 It is recognized that variations in the MAS may occur
num and Aluminum Alloys by the Point-to-Plane Tech-
4 due to the heterogeneous nature of the solid waste stream. The
nique
grades indicated are intended as a means for the purchaser and
E 122 Practice for Choice of Sample Size to Estimate a
3 the seller to establish the value and quality of the MAS.
Measure of Quality for a Lot or Process
5.2 MAS shall be considered to be of a particular grade if
the value for each element specified, as obtained by the test
This specification is under the jurisdiction of ASTM Committee D-34 on Waste method agreed upon between the purchaser and seller, does not
Disposal and is the direct responsibility of Subcommittee D 34.06 on Recovery and
exceed any of the limits for that grade.
Reuse.
Current edition approved Sept. 2, 1980. Published November 1980.
6. Chemical Composition
Annual Book of ASTM Standards, Vol 05.05.
Annual Book of ASTM Standards, Vol 14.02.
6.1 The MAS shall conform to the requirements as to
Annual Book of ASTM Standards, Vol 03.05.
Copyright © ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States.
E 753
TABLE 1 Chemical Requirements
Composition, Maximum % Allowable
A
Element
Grade 1 Grade 2 Grade 3 Grade 4 Grade 5 Grade 6
Silicon 0.30 0.30 0.50 1.00 9.00 9.00
Iron 0.60 0.70 1.00 1.00 0.80 1.00
Copper 0.25 0.40 1.00 2.00 3.00 4.00
Manganese 1.25 1.50 1.50 1.50 0.60 0.80
Magnesium 2.00 2.00 2.00 2.00 2.00 2.00
Chromium 0.05 0.10 0.30 0.30 0.30 0.30
Nickel 0.04 0.04 0.30 0.30 0.30 0.30
Zinc 0.25 0.25 1.00 2.00 1.00 3.00
Lead 0.02 0.04 0.30 0.50 0.10 0.25
Tin 0.02 0.04 0.30 0.30 0.10 0.25
Bismuth 0.02 0.04 0.30 0.30 0.10 0.25
Titanium 0.05 0.05 0.05 0.05 0.10 0.25
Others (each) 0.04 0.05 0.05 0.08 0.10 0.10
Others (total) 0.12 0.15 0.15 0.20 0.30 0.30
Aluminum balance balance balance balance balance balance
A
By agreement between the purchaser and the seller, analysis may be required, and limits established for elements or compounds not specified in this table.
chemical composition prescribed in Table 1 (see Test Methods 8.1.1 Annex A1 covers sampling at the point of origin.
E 34, E 101, and E 227). 8.1.2 Annex A2 covers sampling at the point of receipt.
7. Physical Properties
9. Test Methods
7.1 Density—The density for MAS is not specified and shall
9.1 Determine the properties enumerated in this specifica-
be agreed upon between the purchaser and the seller.
tion in accordance with the following:
7.2 Fineness—MAS shall contain not more than the amount
9.1.1 Fineness—Annex A3.
of minus 12-mesh (U.S. Standard Sieve) (see Specification
9.1.2 Moisture—Annex A3.
E 11) material, described in 7.2.1 and 7.2.2.
9.1.3 Metal Recovery—Annex A3.
7.2.1 Class A material shall contain not more than 1
weight % fines.
10. Rejection and Rehearing
7.2.2 Class B material shall contain not more than 3
10.1 Material that fails to conform to the requirements of
weight % fines.
this specification may be rejected. Rejection should be reported
7.3 Loose Combustibles—MAS shall contain not more than
to the producer or supplier promptly and in writing. In case of
2.0 weight % of loose combustible material.
dissatisfaction with the results of the test, the producer or
7.4 Moisture—MAS shall contain not more than 0.5
supplier may make claim for a rehearing.
weight % of moisture.
7.5 Metal Recovery— A minimum metal recovery of 85 %
11. Shipping
is required.
11.1 MAS shall be shipped in rail cars, trailers, or other
7.6 Magnetics—The presence of free magnetic material is
containers as agreed upon between the purchaser and the seller.
not specified and shall be as agreed upon between the pur-
The shipping equipment shall be sufficiently watertight to
chaser and seller as part of the purchase contract.
prevent the MAS from becoming wet during shipment.
8. Sampling
12. Keywords
8.1 Sampling shall be in accordance with the procedures
described in Annex A1 or Annex A2. Either procedure may be 12.1 assay; chemical composition; classification system;
used, as determined by agreement between the purchaser and gross sample; municipal aluminum scrap; physical properties;
the seller. sampling; test methods; user industries
E 753
ANNEXES
(Mandatory Information)
A1. TEST METHOD FOR COLLECTION OF A SAMPLE OF ALUMINUM SCRAP, RECOVERED FROM
MUNICIPAL SOLID WASTE, AND ITS PREPARATION FOR ANALYSIS
A1.1 Scope concerning possible variation is available. This information
should be gathered with practice. Due to the heterogeneity in
A1.1.1 This test method describes procedures for collection
size and type of material comprising municipal solid waste, the
of a sample of shredded aluminum metal scrap recovered from
choice of a large sample is desirable.
municipal refuse, and the shredding, mixing, and secondary
sampling of the metal for analysis.
A1.5 Taking a Gross Sample
A1.2 Summary of Test Method A1.5.1 In order to obtain complete representation of mate-
rials in a gross sample, it is desirable that the sample incre-
A1.2.1 A selected size, gross sample of shredded, nonfer-
ments be withdrawn from the full cross section of the stream.
rous metal scrap is taken from the metal recovery system
The best possible increment is either a full cross section
conveyor belt in increments. Sample increments are taken at
removed from a stopped conveyor belt or the total flow at the
timed intervals from a full cross section of the conveyor while
discharge of the moving conveyor taken during a suitable
it is stopped or by briefly taking the total flow at the discharge
interval of time.
of the conveyor while it is moving.
A1.5.2 The choice of sample size can be estimated using
A1.2.2 The quantity of gross sample may be further reduced
Practice E 122. It is imperative for a given degree of precision
by mixing, cone-and-quarter sampling, and riffling.
that not less than the minimum size and number of sample
A1.3 Hazards
increments be collected from a lot (see Table A1.1).
A1.5.3 Number of Gross Samples—For quantities up to
A1.3.1 In solids sampling, each step must be designed to
approximately 20 tons (18 000 kg), it is recommended that one
eliminate accidental classification by size or gravity. Different
gross sample represent the lot. Take this sample in accordance
sizes usually have different analyses.
with the requirements prescribed in Table A1.1.
A1.3.2 The increments obtained during the sampling period
A1.5.4 Distribution of Increments—It is essential that the
shall be protected from changes in composition due to expo-
increments be distributed throughout the lot to be sampled. The
sure to the weather.
taking of increments shall be at regularly spaced intervals.
A1.3.3 Plan the sampling arrangement to avoid contamina-
tion of the increments with foreign material.
A1.6 Sample Preparation
A1.3.4 A satisfactory sampling arrangement is one that
A1.6.1 Cone and quarter the sample until approximately 2
takes an unbiased sample at the desired degree of precision of
ft (0.06 m ) remains. Pile the material to be sampled into a
the constituent for which the sample is to be analyzed. The
conical heap and then spread out into a circular cake. Divide
weight or volume of the collected sample is compared with that
the cake into quarters, take two of the diagonally opposite
of the total lot to assure a constant sampling ratio.
quarte
...
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