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ASTM G77-17(2022)

(Test Method)

Standard Test Method for Ranking Resistance of Materials to Sliding Wear Using Block-on-Ring Wear Test

Standard Test Method for Ranking Resistance of Materials to Sliding Wear Using Block-on-Ring Wear Test

SIGNIFICANCE AND USE
5.1 The significance of this test method in any overall measurement program directed toward a service application will depend on the relative match of test conditions to the conditions of the service application.  
5.2 This test method seeks only to prescribe the general test procedure and method of calculating and reporting data. The choice of test operating parameters is left to the user. A fixed amount of sliding distance must be used because wear is usually non-linear with distance in this test.
SCOPE
1.1 This test method covers laboratory procedures for determining the resistance of materials to sliding wear. The test utilizes a block-on-ring friction and wear testing machine to rank pairs of materials according to their sliding wear characteristics under various conditions.  
1.2 An important attribute of this test is that it is very flexible. Any material that can be fabricated into, or applied to, blocks and rings can be tested. Thus, the potential materials combinations are endless. However, the interlaboratory testing has been limited to metals. In addition, the test can be run with various lubricants, liquids, or gaseous atmospheres, as desired, to simulate service conditions. Rotational speed and load can also be varied to better correspond to service requirements.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only. Wear test results are reported as the volume loss in cubic millimetres for both the block and ring. Materials of higher wear resistance will have lower volume loss.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Oct-2022
ICS
77.040.10 - Mechanical testing of metals
Technical Committee
G02 - Wear and Erosion
Drafting Committee
G02.40 - Non-Abrasive Wear
Current Stage
Ref Project

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ASTM G77-17(2022) - Standard Test Method for Ranking Resistance of Materials to Sliding Wear Using Block-on-Ring Wear TestASTM G77-17(2022) - Standard Test Method for Ranking Resistance of Materials to Sliding Wear Using Block-on-Ring Wear Test
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ASTM G77-17(2022) - Standard Test Method for Ranking Resistance of Materials to Sliding Wear Using Block-on-Ring Wear Test
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: G77 − 17 (Reapproved 2022)
Standard Test Method for
Ranking Resistance of Materials to Sliding Wear Using
1
Block-on-Ring Wear Test
ThisstandardisissuedunderthefixeddesignationG77;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginal
adoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperscript
epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
2
2.1 ASTM Standards:
1.1 This test method covers laboratory procedures for de-
D2714Test Method for Calibration and Operation of the
termining the resistance of materials to sliding wear. The test
Falex Block-on-Ring Friction and Wear Testing Machine
utilizes a block-on-ring friction and wear testing machine to
E122PracticeforCalculatingSampleSizetoEstimate,With
rank pairs of materials according to their sliding wear charac-
Specified Precision, the Average for a Characteristic of a
teristics under various conditions.
Lot or Process
1.2 An important attribute of this test is that it is very E177Practice for Use of the Terms Precision and Bias in
flexible.Anymaterialthatcanbefabricatedinto,orappliedto, ASTM Test Methods
E691Practice for Conducting an Interlaboratory Study to
blocks and rings can be tested. Thus, the potential materials
Determine the Precision of a Test Method
combinations are endless. However, the interlaboratory testing
G40Terminology Relating to Wear and Erosion
hasbeenlimitedtometals.Inaddition,thetestcanberunwith
various lubricants, liquids, or gaseous atmospheres, as desired,
3. Terminology
to simulate service conditions. Rotational speed and load can
3.1 Definitions:
also be varied to better correspond to service requirements.
3.1.1 sliding wear, n—wearduetotherelativemotioninthe
1.3 The values stated in SI units are to be regarded as
tangential plane of contact between two solid bodies.
standard. The values given in parentheses are for information
3.1.2 wear—damage to a solid surface, generally involving
only.Wear test results are reported as the volume loss in cubic
progressive loss of material, due to relative motion between
millimetres for both the block and ring. Materials of higher
that surface and a contacting substance or substances.
wear resistance will have lower volume loss.
3.1.3 Foradditionaldefinitionspertinenttothistestmethod,
1.4 This standard does not purport to address all of the
see Terminology G40.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
4. Summary of Test Method
priate safety, health, and environmental practices and deter-
4.1 Atest block is loaded against a test ring that rotates at a
mine the applicability of regulatory limitations prior to use.
given speed for a given number of revolutions. Block scar
1.5 This international standard was developed in accor-
volume is calculated from the block scar width, and ring scar
dance with internationally recognized principles on standard-
volume is calculated from ring weight loss. The friction force
ization established in the Decision on Principles for the
required to keep the block in place is continuously measured
Development of International Standards, Guides and Recom-
during the test with a load cell. These data, combined with
mendations issued by the World Trade Organization Technical
normal force data, are converted to coefficient of friction
Barriers to Trade (TBT) Committee.
values and reported.
5. Significance and Use
5.1 The significance of this test method in any overall
measurement program directed toward a service application
1
This test method is under the jurisdiction of ASTM Committee G02 on Wear
2
and Erosion and is the direct responsibility of G02.40 on Non-Abrasive Wear. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Nov. 1, 2022. Published November 2022. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 1983. Last previous edition approved in 2017 as G77–17. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/G0077-17R22. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
G77 − 17 (2022)
0.203µm (4µin. to 8 µin.) CLA in the direction of motion is
recommended. However, other surface conditions may be
evaluated as desired.
6.4 Analytical Balance, capable of measuring to the nearest
0.1 mg.
6.5 Optical Device (or equivalent), with metric or inch-
pound
...

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5.1 Assuming the presence of a preexisting, sharp, fatigue crack, the material fracture toughness values identified by this test method characterize its resistance to: (1)  fracture of a stationary crack, (2) fracture after some stable tearing, (3) stable tearing onset, and (4) sustained stable tearing. This test method is particularly useful when the material response cannot be anticipated before the test. Application of procedures in Test Method E1921 is recommended for testing ferritic steels that undergo cleavage fracture in the ductile-to-brittle transition.  
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1.1 This test method covers procedures and guidelines for the determination of fracture toughness of metallic materials using the following parameters: K, J, and CTOD (δ). Toughness can be measured in the R-curve format or as a point value. The fracture toughness determined in accordance with this test method is for the opening mode (Mode I) of loading.
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1.1 This practice covers procedures for preparing and conducting the polythionic acid test at room temperature, 22 °C to 25 °C (72 °F to 77 °F), to determine the relative susceptibility of stainless steels or other related materials (nickel-chromium-iron alloys) to intergranular stress corrosion cracking.  
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1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For more specific precautionary statements, see Section 7.  
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5.1 The property KIc determined by this test method characterizes the resistance of a material to fracture in a neutral environment in the presence of a sharp crack under essentially linear-elastic stress and severe tensile constraint, such that (1) the state of stress near the crack front approaches tritensile plane strain, and (2) the crack-tip plastic zone is small compared to the crack size, specimen thickness, and ligament ahead of the crack.  
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1.1 This test method covers the determination of fracture toughness (KIc and optionally KIsi) of metallic materials under predominantly linear-elastic, plane-strain conditions using fatigue precracked specimens having a thickness of 1.6 mm (0.063 in.) or greater2 subjected to slowly, or in special (elective) cases rapidly, increasing crack-displacement force. Details of test apparatus, specimen configuration, and experimental procedure are given in the annexes. Two procedures are outlined for using the experimental data to calculate fracture toughness values:  
1.1.1 The KIc test procedure is described in the main body of this test standard and is a mandatory part of the testing and results reporting procedure for this test method. The KIc test procedure is based on crack growth of up to 2 % percent of the specimen width. This can lead to a specimen size dependent rising fracture toughness resistance curve, with larger specimens producing higher fracture toughness results.  
1.1.2 The KIsi test procedure is described in Appendix X1 and is an optional part of this test method. The KIsi test procedure is based on a fixed amount of crack extension of 0.5 mm, and as a result, KIsi is less sensitive to specimen size than KIc. This less size-sensitive fracture toughness, KIsi, is called size-insensitive throughout this test method. Appendix X1 contains an optional procedure for reinterpreting the force-displacement test record recorded as part of this test method to calculate the additional fracture toughness value, KIsi.
Note 1: Plane-strain fracture toughness tests of materials thinner than 1.6 mm (0.063 in.) that are sufficiently brittle (see 7.1) can be made using other types of specimens (1).3 There is no standard test method for such thin materials.  
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5.1 Fatigue crack growth rate expressed as a function of crack-tip stress-intensity factor range, da/dN versus ΔK, characterizes a material's resistance to stable crack extension under cyclic loading. Background information on the ration-ale for employing linear elastic fracture mechanics to analyze fatigue crack growth rate data is given in Refs (3) and (4).  
5.1.1 In innocuous (inert) environments fatigue crack growth rates are primarily a function of ΔK and force ratio, R, or Kmax and R (Note 1). Temperature and aggressive environments can significantly affect da/dN versus ΔK, and in many cases accentuate R-effects and introduce effects of other loading variables such as cycle frequency and waveform. Attention needs to be given to the proper selection and control of these variables in research studies and in the generation of design data.
Note 1: ΔK, Kmax, and R are not independent of each other. Specification of any two of these variables is sufficient to define the loading condition. It is customary to specify one of the stress-intensity parameters (ΔK or Kmax) along with the force ratio, R.  
5.1.2 Expressing da/dN as a function of ΔK provides results that are independent of planar geometry, thus enabling exchange and comparison of data obtained from a variety of specimen configurations and loading conditions. Moreover, this feature enables da/dN versus ΔK data to be utilized in the design and evaluation of engineering structures. The concept of similitude is assumed, which implies that cracks of differing lengths subjected to the same nominal ΔK will advance by equal increments of crack extension per cycle.  
5.1.3 Fatigue crack growth rate data are not always geometry-independent in the strict sense since thickness effects sometimes occur. However, data on the influence of thickness on fatigue crack growth rate are mixed. Fatigue crack growth rates over a wide range of ΔK have been reported to either increase, decrease, or remain unaffected as specimen...
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1.1 This test method2 covers the determination of fatigue crack growth rates from near-threshold (see region I in Fig. 1) to Kmax  controlled instability (see region III in Fig. 1.) Results are expressed in terms of the crack-tip stress-intensity factor range (ΔK), defined by the theory of linear elasticity.  
1.9 Special requirements for the various specimen configurations appear in the following order:
The Compact Specimen  
Annex A1  
The Middle Tension Specimen  
Annex A2  
The Eccentrically-Loaded Single Edge Crack Tension Specimen  
Annex A3  
1.10 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.11 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM E468/E468M-23(Practice)
Standard Practice for Presentation of Constant Amplitude Fatigue Test Results for Metallic Materials

SIGNIFICANCE AND USE
4.1 Fatigue test results may be significantly influenced by the properties and history of the parent material, the operations performed during the preparation of the fatigue specimens, and the testing machine and test procedures used during the generation of the data. The presentation of fatigue test results should include citation of basic information on the material, specimens, and testing to increase the utility of the results and to reduce to a minimum the possibility of misinterpretation or improper application of those results.
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1.1 This practice covers the desirable and minimum information to be communicated between the originator and the user of data derived from constant-force amplitude axial, bending, or torsion fatigue tests of metallic materials tested in air and at room temperature.  
Note 1: Practice E466, although not directly referenced in the text, is considered important enough to be listed in this standard.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM E561-23(Test Method)
Standard Test Method for KR Curve Determination

SIGNIFICANCE AND USE
5.1 The KR curve characterizes the resistance to fracture of materials during slow, stable crack extension and results from the growth of the plastic zone ahead of the crack as it extends from a fatigue precrack or sharp notch. It provides a record of the toughness development as a crack is driven stably under increasing applied stress intensity factor K. For a given material, KR curves are dependent upon specimen thickness, temperature, and strain rate. The amount of valid KR data generated in the test depends on the specimen type, size, method of loading, and, to a lesser extent, testing machine characteristics.  
5.2 For an untested geometry, the KR curve can be matched with the applied-K curves (crack driving curves) to estimate the degree of stable crack extension and the conditions necessary to cause unstable crack propagation (2). In making this estimate, KR curves are regarded as being independent of initial crack size ao and the specimen configuration in which they are developed. For a given material, material thickness, and test temperature, KR curves appear to be a function of only the effective crack extension Δae (3).  
5.2.1 To predict crack behavior and instability in a component, a family of applied-K curves is generated by calculating  K as a function of crack size for the component using a series of force, displacement, or combined loading conditions. The KR curve may be superimposed on the family of applied-K curves as shown in Fig. 1, with the origin of the KR curve coinciding with the assumed initial crack size ao. The intersection of the applied-K curves with the KR curve shows the expected effective stable crack extension for each loading condition. The applied-K curve that develops tangency with the KR curve defines the critical loading condition that will cause the onset of unstable fracture under the loading conditions used to develop the applied-K curves.
FIG. 1 Schematic Representation of KR curve and Applied K Curves to Predict Insta...
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1.1 This test method covers the determination of the resistance to fracture of metallic materials under Mode I loading at static rates using either of the following notched and precracked specimens: the middle-cracked tension M(T) specimen or the compact tension C(T) specimen. A KR curve is a continuous record of toughness development (resistance to crack extension) in terms of KR plotted against crack extension in the specimen as a crack is driven under an increasing stress intensity factor, K. (1)2  
1.2 Materials that can be tested for KR curve development are not limited by strength, thickness, or toughness, so long as specimens are of sufficient size to remain predominantly elastic to the effective crack extension value of interest.  
1.3 Specimens of standard proportions are required, but size is variable, to be adjusted for yield strength and toughness of the materials.  
1.4 Only two of the many possible specimen types that could be used to develop KR curves are covered in this method.  
1.5 The test is applicable to conditions where a material exhibits slow, stable crack extension under increasing crack driving force, which may exist in relatively tough materials under plane stress crack tip conditions.  
1.6 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Reco...

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