Standard Test Method for Rust-Preventing Characteristics of Inhibited Mineral Oil in the Presence of Water

SCOPE
1.1 This test method is used to evaluate the ability of inhibited mineral oils, particularly steam-turbine oils, to aid in preventing the rusting of ferrous parts should water become mixed with the oil. This test method is also used for testing other oils, such as hydraulic oils and circulating oils. Provision is made in the procedure for testing heavier-than-water fluids.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
09-Dec-1999
Current Stage
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ASTM D665-99 - Standard Test Method for Rust-Preventing Characteristics of Inhibited Mineral Oil in the Presence of Water
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NOTICE: This standard has either been superseded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
An American National Standard
Designation: D 665 – 99
Designation: 135/93
Standard Test Method for
Rust-Preventing Characteristics of Inhibited Mineral Oil in
1
the Presence of Water
This standard is issued under the fixed designation D 665; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope D 1401 Test Method for Water Separability of Petroleum
4
Oils and Synthetic Fluids
1.1 This test method is used to evaluate the ability of
D 2422 Classification of Industrial Fluid Lubricants by
inhibited mineral oils, particularly steam-turbine oils, to aid in
4
Viscosity System
preventing the rusting of ferrous parts should water become
D 3603 Test Method for Rust-Preventing Characteristics of
mixed with the oil. This test method is also used for testing
Steam Turbine Oil in the Presence of Water (Horizontal
other oils, such as hydraulic oils and circulating oils. Provision
6
Disk Method)
is made in the procedure for testing heavier-than-water fluids.
D 4057 Practice for Manual Sampling of Petroleum and
NOTE 1—For synthetic fluids, such as phosphate ester types, the plastic 6
Petroleum Products
holder and beaker cover should be made of a chemically resistant material,
7
E 1 Specification for ASTM Thermometers
such as polytetrafluoroethylene (PTFE).
Motor Fuels, Section I, Annex A2, Reference Materials and
8
1.2 This standard does not purport to address all of the
Blending Accessories
safety concerns, if any, associated with its use. It is the
2.2 Other Documents:
9
responsibility of the user of this standard to establish appro-
Specifications-IP Standard Thermometers, Appendix A
priate safety and health practices and determine the applica-
Specifications for IP Standard Reference Liquids, Appen-
9
bility of regulatory limitations prior to use.
dix B
SAE Standard J 405 Chemical Composition of SAE
2. Referenced Documents
10
Wrought Stainless Steels
9
2.1 ASTM Standards:
BS 871 Specification for abrasive papers and cloths
A 108 Specification for Steel Bars, Carbon, Cold-Finished,
BS 970: Part 1: Carbon and Carbon Manganese Steels
2
9
Standard Quality
Including Free Cutting Steels
A 240/A 240M Specification for Heat-Resisting Chromium
and Chromium-Nickel Stainless Steel Plate, Sheet, and 3. Summary of Test Method
3
Strip for Pressure Vessels
3.1 A mixture of 300 mL of the oil under test is stirred with
D 91 Test Method for Precipitation Number of Lubricating
30 mL of distilled water or synthetic sea water, as required, at
4
Oils
a temperature of 60°C (140°F) with a cylindrical steel test rod
5
D 1193 Specification for Reagent Water
completely immersed therein. It is recommended to run the test
for 4 h; however, the test period may, at the discretion of the
contracting parties, be for a shorter or longer period. The test
1
This test method is under the jurisdiction of ASTM Committee D-2 on
rod is observed for signs of rusting and, if desired, degree of
Petroleum Products and Lubricantsand is the direct responsibility of Subcommittee
rusting.
DO2.C on Turbine Oils.
In the IP, this test method is under the jurisdiction of the Standardization
Committee. This test method was adopted as a joint ASTM – IP standard in 1964.
6
Current edition approved Dec. 10, 1999. Published January 2000. Originally Annual Book of ASTM Standards, Vol 05.02.
e1 7
published as D 665 – 42 T. Last previous edition D 665 – 98 . Annual Book of ASTM Standards, Vol 14.03.
2 8
Annual Book of ASTM Standards, Vol 01.05. Annual Book of ASTM Standards, Vol 05.05.
3 9
Annual Book of ASTM Standards, Vol 01.03. Annual Book of IP Standard Methods for Analysis and Testing of Petroleum and
4
Annual Book of ASTM Standards, Vol 05.01. Related Products, Vol 2.
5 10
Annual Book of ASTM Standards, Vol 11.01. 1995 SAE Handbook, Vol 1.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

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NOTICE: This standard has either been superseded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
D665–99
NOTE 2—Until 1999 it was customary to run the test for 24 h. A round
capable of maintaining the test sample at a temperature of 60
robin with comparisons of different test times showed that no statistically
6 1°C (140 6 2°F) (see Note 4). An oil having a viscosity of
significant differences in rating were found for any sample, between the 4
approximately ISO VG 32 (see Classification D 2422) is
11
and 24 h r
...

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