Standard Test Method for Combustible Properties of Treated Wood by the Fire-Tube Apparatus

SIGNIFICANCE AND USE
The purpose of this test method is to provide a relative measurement of the combustibility of fire-retardant-treated wood specimens based on their percentage loss in weight under controlled fire exposure conditions (1).3 In addition, other possible data include rate of weight loss, time of flaming and afterglowing, increase in temperature, and maximum vertical flame progress.
This test method is not sufficiently large scale to evaluate the suitability of a given treated product for building construction, but it is a convenient method to use for purposes of development or as a quality-control test during manufacture.
This test method gives a procedure for sampling and preparation of test specimens from a lot of treated material in which complete penetration is a requirement. A procedure is also given for the sampling of charges at a treating plant for purposes of quality control of the treatment process.
This test method has proven useful for evaluating comparative fire performance effectiveness of fire-retardant chemicals and treatment formulations for wood and wood products (2-5).
In this test method, the specimens are subjected to one or more specific sets of laboratory test conditions. If different test conditions are substituted or the anticipated end-use conditions are changed, it may not be possible by or from this test method to predict changes in the fire-test-response characteristics measured. Therefore, the results are valid only for the fire test exposure conditions described in this procedure.
SCOPE
1.1 This test method covers fire-tube test procedures for fire tests for combustible properties of wood treated to reduce flammability. This test method relates to properties of treated wood, as such, rather than to the performance of a fabrication used as an element of construction. Performance under this test method shall be as prescribed in requirements applicable to materials intended for specific uses.
1.2 This test method is a fire-test-response standard.
1.3 The SI values given in parentheses are provided for information purposes only.
1.4 This standard should be used to measure and describe the properties of materials, products, or assemblies in response to heat and flame under controlled laboratory conditions and should not be used to describe or appraise the fire hazard or fire risk of materials, products, or assemblies under actual fire conditions. However, results of this test may be used as elements of a fire risk assessment which takes into account all of the factors which are pertinent to an assessment of the fire hazard of a particular end use. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
31-Mar-2007
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ASTM E69-02(2007) - Standard Test Method for Combustible Properties of Treated Wood by the Fire-Tube Apparatus
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: E69 − 02(Reapproved 2007)
Standard Test Method for
Combustible Properties of Treated Wood by the Fire-Tube
Apparatus
This standard is issued under the fixed designation E69; the number immediately following the designation indicates the year of original
adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.Asuperscript
epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3. Terminology
1.1 This test method covers fire-tube test procedures for fire 3.1 Definitions—For definitions of terms found in this test
tests for combustible properties of wood treated to reduce method, refer to Terminologies D9 and E176.
flammability. This test method relates to properties of treated
4. Significance and Use
wood, as such, rather than to the performance of a fabrication
used as an element of construction. Performance under this test
4.1 The purpose of this test method is to provide a relative
method shall be as prescribed in requirements applicable to
measurement of the combustibility of fire-retardant-treated
materials intended for specific uses.
woodspecimensbasedontheirpercentagelossinweightunder
controlled fire exposure conditions (1). In addition, other
1.2 This test method is a fire-test-response standard.
possible data include rate of weight loss, time of flaming and
1.3 The SI values given in parentheses are provided for
afterglowing, increase in temperature, and maximum vertical
information purposes only.
flame progress.
1.4 This standard should be used to measure and describe
4.2 This test method is not sufficiently large scale to
the properties of materials, products, or assemblies in response
evaluate the suitability of a given treated product for building
to heat and flame under controlled laboratory conditions and
construction, but it is a convenient method to use for purposes
should not be used to describe or appraise the fire hazard or
of development or as a quality-control test during manufacture.
fire risk of materials, products, or assemblies under actual fire
4.3 This test method gives a procedure for sampling and
conditions. However, results of this test may be used as
preparation of test specimens from a lot of treated material in
elements of a fire risk assessment which takes into account all
which complete penetration is a requirement. A procedure is
of the factors which are pertinent to an assessment of the fire
also given for the sampling of charges at a treating plant for
hazard of a particular end use.
purposes of quality control of the treatment process.
1.5 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the 4.4 This test method has proven useful for evaluating
responsibility of the user of this standard to establish appro- comparative fire performance effectiveness of fire-retardant
priate safety and health practices and determine the applica- chemicals and treatment formulations for wood and wood
bility of regulatory limitations prior to use. products (2-5).
4.5 In this test method, the specimens are subjected to one
2. Referenced Documents
or more specific sets of laboratory test conditions. If different
2.1 ASTM Standards: test conditions are substituted or the anticipated end-use
D9 Terminology Relating to Wood and Wood-Based Prod-
conditions are changed, it may not be possible by or from this
ucts test method to predict changes in the fire-test-response char-
E176 Terminology of Fire Standards
acteristics measured. Therefore, the results are valid only for
the fire test exposure conditions described in this procedure.
This test method is under the jurisdiction of ASTM Committee D07 on Wood 5. Apparatus
and is the direct responsibility of Subcommittee D07.07 on Fire Performance of
5.1 The apparatus for conducting the fire-tube test shall
Wood.
Current edition approved April 1, 2007. Published April 2007. Originally consist of the fire-tube assembly and accessory equipment as
approved in 1946. Last previous edition approved in 2002 as E69 – 02. DOI:
follows:
10.1520/E0069-02R07.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on The boldface numbers in parentheses refer to the list of references at the end of
the ASTM website. this test method.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
E69 − 02 (2007)
5.1.1 Fire-Tube Assembly—A specially constructed balance 5.1.6 Oven—Asuitable thermostatically controlled oven for
designed to indicate directly the percentage loss of weight moisture-content determinations.
suffered by the test specimen when exposed to a standardized
flame for a given duration. Essential construction details of the 6. Sampling and Test Specimens for Wood Impregnated
apparatus assembly are shown in Fig. 1 and Fig. 2.
Throughout Entire Section
5.1.2 Igniting Burner—The igniting burner is to be of the
6.1 Forinteriortrimorotherlumberrequiringpenetrationof
low-form (curved-stem) bunsen type, having an inside tube
treatingsolutionthroughoutthesection(butnotforwoodgiven
diameter of ⁄8 in. (9.5 mm) and attached to a ring-stand
incomplete penetration), the test specimens shall be prepared
support. The igniting burner shall be provided with a device to
as follows:
maintain a constant gas flow, as described in 5.1.2.1 and the
6.1.1 Atleastonesampleshallbetakenfromthelotforeach
flame calibration, as required by 9.4.
5000 bd ft or fraction thereof. Different species, and pieces of
5.1.2.1 Gas Flow Device—Typical devices utilized to con-
the same species with widely different thicknesses, shall be
trol gas flow are manometers, pressure regulators or gas
considered as separate lots and sampled accordingly. The
flowmeters with a rating of 0 to 5 SCFH (0 to 142 L/h).Agas
samples shall be selected so as to include material from
flowmeter is desirable since they are readily available, very
different sections of a finished unit or different lengths of
accurate, and inexpensive.
finished trim, or to include variations such as heartwood or
5.1.3 Temperature-Indicating Apparatus—A thermometer
sapwood, rate of growth, density, and other visible nonunifor-
or thermocouple equipment that will indicate temperatures up
mities. Samples shall be cut not closer than 2 ft (0.6 m) from
to 1000°F (538°C).
the ends of treated boards.
5.1.4 Timer—A timing device capable of being read to
minutes and seconds. 6.1.2 Not less than five tests shall be made from each
5.1.5 Balance—A balance with readability of 0.1 g and sample, except that where the quantity is less than 2000 bd ft
suitable for weighing test specimens and moisture-content the number of tests shall be left to the discretion of the testing
samples. authority but shall be not less than two.
FIG. 1 Construction Details of Fire-Tube Apparatus
Inch-Pound Units SI Units Inch-Pound Units SI Units
1 9
⁄8 in. 3 mm 4 ⁄16 in. 116 mm
1 3
⁄4 in. 6 mm 4 ⁄4 in. 121 mm
3 1
⁄8 in. 9.5 mm 5 ⁄2 in. 140 mm
⁄4 in. 19 mm 6 in. 152 mm
1 in. 25 mm 8 in. 203 mm
1 ⁄4 in. 31.7 mm 28 in. 711 mm
1 ⁄2 in. 38 mm 33 in. 838 mm
3 in. 76 mm 38 in. 965 mm
3 ⁄2 in. 89 mm 4 ft 6 in. 1.35 m
4 ⁄16 in. 113 mm
E69 − 02 (2007)
The weight of nails used shall be recorded for correction of the
weight of the specimen.
6.1.7 A composite specimen prepared from more than one
sample piece shall be taken so as to be representative of the
average quality of the materials to be tested.
7. Sampling and Test Specimens
7.1 Where arrangements are made for sampling of each
charge at the treating plant, the specimens shall be obtained as
follows:
7.1.1 No charge shall contain less than six sample pieces.
These sample pieces shall be of Douglas fir or of the same
species and commodity (lumber, plywood, and so forth) of
wood as the rest of the material in the charge. Each sample
shall bear an identification mark.
7.1.2 Placement of sample pieces in the material to be
treated on a tram shall be representative of the average
exposuretothetreatingsolutionandyetbeaccessibleforready
removal without seriously disturbing the loading.
3 3 1
7.1.3 Sample pieces shall be ⁄8 by ⁄4 6 ⁄32 in. (9.5 by 19 6
0.8mm)incrosssectionandbeatleast42in.(1.1m)inlength.
7.1.4 Fire-tube test specimens shall be cut from each se-
lected sample and shall be 40 in. (1.016 m) in length, within
6 ⁄32 in. (0.8 mm).The remainder of the sample 2-in. (51-mm)
or greater in length shall be cut off for moisture test specimens.
8. Conditioning
FIG. 2 Assembly of Fire-Tube Apparatus for Procedure A
8.1 The moisture content of the specimen when tested shall
be 7 6 3 weight % of the dry material. Make the moisture
3 3
determination for each specimen on a piece ⁄8 by ⁄4 in. (9.5 by
6.1.3 The standard specimens cut from the selected samples
3 3
19mm)incrosssectionand2to8in.(51to203mm)inlength,
shall be ⁄8 by ⁄4 in. (9.5 by 19 mm) in cross section by 40 in.
cut adjacent to one end of the specimens. Weigh the moisture
(1016 mm) in length, with surfaces smooth-sawed to dimen-
test specimen and the fire tube test specimen to the nearest 0.1
sions within 6 ⁄32 in. (0.8 mm). Each test specimen shall
g or less and record. Dry the moisture test specimen for 24 h at
consist of one piece sawed the full 40-in. length or shall be
212 6 3°F (100 6 1.7°C) or until a constant weight is
made up of several shorter pieces joined at squared ends with
achieved. Constant weight is achieved when readings are taken
six
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