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ASTM F2130-11

(Test Method)

Standard Test Method for Measuring Repellency, Retention, and Penetration of Liquid Pesticide Formulation Through Protective Clothing Materials

Standard Test Method for Measuring Repellency, Retention, and Penetration of Liquid Pesticide Formulation Through Protective Clothing Materials

SIGNIFICANCE AND USE
This test method can be used for laboratory screening of protective clothing material used to manufacture garments and accessories worn by pesticide workers.
This test method can be used for the development and evaluation of new protective clothing materials.
This test method can be used for the evaluation of protective clothing materials against new pesticide formulations.
SCOPE
1.1 This test method measures repellency, retention and penetration of a known volume of liquid pesticide when applied to protective clothing material. No external hydrostatic or mechanical pressure is applied to the test specimen during or after the application of the liquid pesticide.
1.2 This test method is designed to measure performance of protective clothing materials at two levels of contamination. Low level of contamination is achieved by applying 0.1-mL liquid formulation and high level by applying 0.2 mL.
1.3 This test method does not measure resistance to permeation or degradation.
1.4 This test method is suitable for field strength pesticide formulations. This test method may not be suitable for testing protective clothing materials against volatile pesticides.
1.5 The values stated in SI units are to be regarded as the standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
30-Nov-2011
ICS
13.340.10 - Protective clothing
Technical Committee
F23 - Personal Protective Clothing and Equipment
Drafting Committee
F23.30 - Chemicals
Current Stage
Ref Project

Relations

Replaces
ASTM F2130-09 - Standard Test Method for Measuring Repellency, Retention, and Penetration of Liquid Pesticide Formulation Through Protective Clothing Materials
Effective Date
01-Dec-2011
Replaced By
ASTM F2130-11(2018) - Standard Test Method for Measuring Repellency, Retention, and Penetration of Liquid Pesticide Formulation Through Protective Clothing Materials (Withdrawn 2023)
Effective Date
01-Jul-2018
Referred By
ASTM F2669-12(2018) - Standard Performance Specification for Protective Clothing Worn by Operators Applying Pesticides (Withdrawn 2023)
Effective Date
01-Dec-2011
Referred By
ASTM F1296-08(2023) - Standard Guide for Evaluating Chemical Protective Clothing
Effective Date
01-Dec-2011

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ASTM F2130-11 - Standard Test Method for Measuring Repellency, Retention, and Penetration of Liquid Pesticide Formulation Through Protective Clothing Materials
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REDLINE ASTM F2130-11 - Standard Test Method for Measuring Repellency, Retention, and Penetration of Liquid Pesticide Formulation Through Protective Clothing MaterialsREDLINE ASTM F2130-11 - Standard Test Method for Measuring Repellency, Retention, and Penetration of Liquid Pesticide Formulation Through Protective Clothing Materials
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: F2130 − 11
Standard Test Method for
Measuring Repellency, Retention, and Penetration of Liquid
Pesticide Formulation Through Protective Clothing
1
Materials
This standard is issued under the fixed designation F2130; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
The health and safety of agricultural workers involved in the mixing, loading and application of
liquidpesticidescanbeaffectedbydermalexposuretoliquidpesticideformulations.Useofprotective
clothingcanassistinminimizingthedangerofcontactwithpotentiallyharmfulpesticides.Nonporous
materials that provide excellent protection to the user are usually not suitable for many agricultural
environments in which there is a potential for heat stress. Therefore, garments made of porous
materials that can provide a balance between risk from pesticide exposure and user comfort can also
be used as personal protective equipment (PPE) for agricultural workers. The movement of liquid
pesticides through these materials is primarily a result of penetration through spaces between fibers
and interstices between yarns. As these materials provide protection either by repelling or retaining
liquid pesticide, the measurement of these properties is also important. This test method is used to
measure repellency, retention, and penetration of liquid pesticides through protective clothing
materials.
The degree of contamination depends on numerous factors such as type of exposure, application
technique, and pesticide formulation. Worker exposure to liquid pesticides can range from low
exposure caused by spray drift to high exposure as in the case of an accidental spill while mixing or
handling of concentrates.As the level of exposure can vary considerably, this test method is designed
to rate relative performance of PPE materials at two levels of contamination.
1. Scope 1.4 This test method is suitable for field strength pesticide
formulations. This test method may not be suitable for testing
1.1 This test method measures repellency, retention and
protective clothing materials against volatile pesticides.
penetration of a known volume of liquid pesticide when
appliedtoprotectiveclothingmaterial.Noexternalhydrostatic 1.5 The values stated in SI units are to be regarded as the
ormechanicalpressureisappliedtothetestspecimenduringor standard.
after the application of the liquid pesticide.
1.6 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
1.2 This test method is designed to measure performance of
responsibility of the user of this standard to establish appro-
protective clothing materials at two levels of contamination.
priate safety and health practices and determine the applica-
Low level of contamination is achieved by applying 0.1-mL
bility of regulatory limitations prior to use.
liquid formulation and high level by applying 0.2 mL.
1.3 This test method does not measure resistance to perme-
2. Referenced Documents
ation or degradation.
2
2.1 ASTM Standards:
D123Terminology Relating to Textiles
1
ThistestmethodisunderthejurisdictionofASTMCommitteeF23onPersonal
ProtectiveClothingandEquipmentandisthedirectresponsibilityofSubcommittee
2
F23.30 on Chemicals. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Dec. 1, 2011. Published December 2011. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 2001. Last previous edition approved in 2009 as F2130-09. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/F2130-11. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
F2130 − 11
E105Practice for Probability Sampling of Materials isopropyl alcohol, or petroleum distillate. Solid materials
F1494Terminology Relating to Protective Clothing (powders, granules, and so forth) may be dissolved or emulsi-
fiedtoformaliquidorsuspension.Theseformulationsmaybe
3. Terminology
ready to use or concentrates that require dilution to field
strength. In some ultra-low volume applications, concentrated
3.1 Definitions:
oil-based formulations are used without dilution; testing for
3.1.1 analytical technique, n—a procedure whereby the
this application is beyond the scope of this test method.
concentration of the test chemical in a collection medium is
quantitatively determined.
3.1.10 ForothertextileterminologyseeTerminologyD123.
3.1.1.1 Discussion—T
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:F2130–09 Designation:F2130–11
Standard Test Method for
Measuring Repellency, Retention, and Penetration of Liquid
Pesticide Formulation Through Protective Clothing
1
Materials
This standard is issued under the fixed designation F2130; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
The health and safety of agricultural workers involved in the mixing, loading and application of
liquidpesticidescanbeaffectedbydermalexposuretoliquidpesticideformulations.Useofprotective
clothingcanassistinminimizingthedangerofcontactwithpotentiallyharmfulpesticides.Nonporous
materials that provide excellent protection to the user are usually not suitable for many agricultural
environments in which there is a potential for heat stress. Therefore, garments made of porous
materials that can provide a balance between risk from pesticide exposure and user comfort can also
be used as personal protective equipment (PPE) for agricultural workers. The movement of liquid
pesticides through these materials is primarily a result of penetration through spaces between fibers
and interstices between yarns. As these materials provide protection either by repelling or retaining
liquid pesticide, the measurement of these properties is also important. This test method is used to
measure repellency, retention, and penetration of liquid pesticides through protective clothing
materials.
The degree of contamination depends on numerous factors such as type of exposure, application
technique, and pesticide formulation. Worker exposure to liquid pesticides can range from low
exposure caused by spray drift to high exposure as in the case of an accidental spill while mixing or
handling of concentrates.As the level of exposure can vary considerably, this test method is designed
to rate relative performance of PPE materials at two levels of contamination.
1. Scope
1.1 This test method measures repellency, retention and penetration of a known volume of liquid pesticide when applied to
protective clothing material. No external hydrostatic or mechanical pressure is applied to the test specimen during or after the
application of the liquid pesticide.
1.2 This test method is designed to measure performance of protective clothing materials at two levels of contamination. Low
level of contamination is achieved by applying 0.1-mL liquid formulation and high level by applying 0.2 mL.
1.3 This test method does not measure resistance to permeation or degradation.
1.4 This test method is suitable for field strength pesticide formulations. This test method may not be suitable for testing
protective clothing materials against volatile pesticides.
1.5 The values stated in SI units are to be regarded as the standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D123 Terminology Relating to Textiles
1
This test method is under the jurisdiction of ASTM Committee F23 on Personal Protective Clothing and Equipment and is the direct responsibility of Subcommittee
F23.30 on Chemicals.
Current edition approved Feb.Dec. 1, 2009.2011. Published February 2009.December 2011. Originally approved in 2001. Last previous edition approved in 20012009 as
F2130 - 019. DOI: 10.1520/F2130-09.10.1520/F2130-11.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
F2130–11
E105 Practice for Probability Sampling of Materials
F1494 Terminology Relating to Protective Clothing
3. Terminology
3.1 Definitions:
3.1.1 analytical technique, n—a procedure whereby the concentration of the challengetest chemical in a collection medium is
quantitatively determined.
3.1.1.1 Discussion—These techniques are often specific to individual chemical and collection medium c
...

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1.1 This test method measures cut resistance of garments and devices worn to protect the lower body (legs) when operating a chainsaw.  
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Standard Test Method for Thermal Resistance, Evaporative Resistance, and Total Heat Loss Measurements of Clothing Materials Using a Sweating Hot Plate

SIGNIFICANCE AND USE
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4.1.1 The thermal resistance, evaporative resistance, and total heat loss can be significantly affected by environmental conditions. Extreme care must be taken when using results measured under standard testing conditions to determine a material’s suitability for use in conditions outside the testing conditions.  
4.2 The thermal interchange between people and their environment is an extremely complicated subject that involves many factors in addition to the steady-state resistance values of fabrics, films, coatings, foams, and leathers, including multi-layer assemblies. Therefore, thermal resistance values, evaporative resistance values, and total heat loss measured on a hot plate may or may not indicate relative merit of a particular material or system for a given clothing application. While a possible indicator of clothing performance, measurements produced by the testing of fabrics have no proven correlation to the performance of clothing systems worn by people. Clothing weight, drape, tightness of fit, and so forth, can minimize or even neutralize the apparent differences between fabrics or fabric assemblies measured by this test method.  
4.3 The thermal resistance and evaporative resistance of clothing systems and items can be measured with a heated sweating manikin in an environmental chamber in accordance with Test Methods F1291, F2370, and F3426.
SCOPE
1.1 This test method covers the measurement of the thermal resistance, evaporative resistance, and total heat loss under steady-state conditions of fabrics, films, coatings, foams, and leathers, including multi-layer assemblies, for use in clothing systems.  
1.2 The range of this measurement technique for intrinsic thermal resistance is from 0.002 to 0.5 K·m2/W and for intrinsic evaporative resistance is from 0.0 to 1.0 kPa·m 2/W. The total heat loss range is from 0.0 to 1300 W/m2.  
1.3 The values in SI units shall be regarded as standard. Other units of measurement are provided in this standard but are not regarded as standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM F2992-23(Test Method)
Standard Test Method for Measuring Cut Resistance of Materials Used in Protective Clothing with Tomodynamometer Test Equipment

SIGNIFICANCE AND USE
5.1 This test method assesses the cut resistance of a material when exposed to a cutting edge under specified loads. Data obtained from this test method can be used to compare the cut resistance of different materials.  
5.2 This test method only addresses that range of cutting hazards that are related to a cutting action by a smooth sharp edge across the surface of the material. It is not representative of any other cutting hazard to which the material may be subjected, such as serrated edges, saw blades, or motorized cutting tools. Nor is it representative of puncture, tear, or other modes of fabric failure.
SCOPE
1.1 This test method covers the measurement of the cut resistance of a material when mounted on a specimen holder and subjected to a cutting edge under a specified load using a tomodynamometer.2  
1.1.1 This procedure is not valid for high-porosity materials which allow cutting edge contact with the mounting surface prior to cutting.  
1.1.2 Test apparatus may have limitations in testing materials with a thickness greater than 20 mm.  
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM F3628-23(Test Method)
Standard Test Method for Measuring the Cooling Energy Provided by Wicking Liquid Moisture and Evaporating It from Clothing Materials Using a Sweating Hot Plate

SIGNIFICANCE AND USE
4.1 A clothing material’s ability to assist in the evaporation of liquid sweat by managing liquid moisture is of considerable importance when trying to maximize cooling and comfort benefits to the wearer while active. Understanding how much energy is released back to the skin is critical in determining their suitability for use in fabricating protective clothing systems or athletic wear.  
4.1.1 The cooling energy released back to the wearer can be significantly affected by environmental conditions. Extreme care must be taken when using standard results measured under standard testing conditions to determine a material’s suitability for use in conditions outside the testing conditions.  
4.2 This test method accounts for a clothing material’s ability to assist in evaporating liquid water during a sweating phase, as well as its ability to dry after the cessation of sweating.  
4.2.1 A large amount of cooling energy released from clothing materials during active work (sweating) is often seen as a positive, as it would assist in keeping the body cooler.  
4.2.2 A large amount of cooling energy released from clothing materials after active work (no sweating) is often seen as a negative, as it known to cause a chilling effect to the wearer.  
4.2.3 The longer it takes for a clothing material to dry after becoming wet is perceived as a negative, as it increases the potential for chilling the wearer.  
4.3 The thermal interchange between people and their environment is, however, an extremely complicated subject that involves many factors in addition to the steady-state resistance values of fabrics, films, coatings, foams, and leathers, including multi-layer assemblies. Therefore, the cooling provided from liquid evaporation may or may not indicate relative merit of a particular material or system for a given clothing application. While a possible indicator of clothing performance, measurements produced by the testing of fabrics have no proven correlation to the perfo...
SCOPE
1.1 This test method covers the measurement of the cooling energy released back to the wearer’s skin by a clothing material’s ability to move and evaporate controlled dosages of water under controlled ambient conditions using a sweating hot plate.  
1.1.1 This test method establishes procedures for measuring the cooling energy during a simulated “sweating” phase and in a drying phase. Calculations are also provided to determine the drying time and how efficient the clothing material is at assisting in the evaporation of liquid water by comparing it to the maximum amount of energy that can be lost.  
1.2 This test method does not address all properties that affect a clothing material’s ability to lose heat from the body. Consider measuring properties such as air permeability, insulation, and evaporative resistance.  
1.3 The values in SI units shall be regarded as standard. No other units of measurement are included in the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM F3267-22(Specification)
Standard Specification for Protective Clothing for Use Against Liquid Chemotherapy and Other Liquid Hazardous Drugs

SCOPE
1.1 This specification establishes design, performance, documentation, and labeling requirements and provides test methods for protective clothing used in preventing exposure to liquid chemotherapy and other liquid hazardous drugs.  
1.1.1 The principal requirement of this specification is permeation resistance testing of the protective clothing barrier material and seams to a specified battery of seven chemotherapy drugs. Two levels of protective clothing barrier material and seam performance are established for complying with Part A labeling requirements specific to these seven liquid chemotherapy drugs.
1.1.1.1 Broad chemotherapy drug protection is based on the protective clothing barrier material and seams demonstrating breakthrough detection times of 30 min or more for the seven specified chemotherapy drugs.
1.1.1.2 Selective chemotherapy drug protection is based on the protective clothing barrier material and seams demonstrating breakthrough detection times of 30 min or more for at least five of the seven specified chemotherapy drugs.  
1.1.2 It is also possible to report permeation resistance test results for additional liquid chemotherapy and other liquid hazardous drugs of interest as determined by the manufacturer or end user organization using the same breakthrough detection criteria for individual drugs for complying with the Part B labeling requirements.  
1.1.3 Protective clothing meeting this specification is also required to meet minimum flammability requirements, and if used as a medical device, biocompatibility (if used for breached skin contact), and demonstrate sterility assurance, if sterilized prior to use.  
1.1.4 Physical properties that indicate the strength, durability, and breathability of the protective clothing are optionally reported.  
1.1.5 Additional requirements are established for the label and user information to be provided for protective clothing meeting this specification.  
1.1.6 This specification also requires products intended to be used as medical devices such as surgical gowns and isolation gowns to meet the respective requirements of AAMI PB70, Specification F2407/F2407M, and Specification F3352/F3352M, as applicable.  
1.2 This specification does not address all conditions of exposure for individuals who wear protective clothing in the manufacture, transport, compounding, preparation, and administration of liquid chemotherapy and other hazardous drugs in addition to patient care activities and spills where contaminated items with these drugs are encountered.  
1.3 This specification does not address chemotherapy drugs or hazardous drugs that may be encountered in the form of a vapor or aerosol and does not provide any criteria for respiratory protection.  
1.4 This specification does not address the selection, use, or care of protective clothing used for protection against liquid chemotherapy or other liquid hazardous drugs. While this specification does not specifically determine which barrier material to select, the results of the tests described in this specification are useful for selecting barrier materials by comparing the test results among different materials under consideration. See USP 800, Hazardous Drugs—Handling In Healthcare Settings, for specific guidelines on the selection, use, and care of personal protective equipment for protection of healthcare workers against chemotherapy or other hazardous drugs.  
1.5 This specification is intended to provide the basis for manufacturers or suppliers to make specific claims that protective clothing products provide protection against liquid chemotherapy and other liquid hazardous drugs.  
1.6 The values stated in SI units or in other units shall be regarded separately as standard. The values stated in each system must be used independently of the other, without combining values in any way.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its u...

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