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ASTM D4562-90(1995)e1

(Test Method)

Standard Test Method for Shear Strength of Adhesives Using Pin-and-Collar Specimen

Standard Test Method for Shear Strength of Adhesives Using Pin-and-Collar Specimen

SCOPE
1.1 This test method covers the determination of the shear strength of curing liquid adhesives used for retaining cylindrical assemblies or for locking and sealing threaded fasteners.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Dec-1994
ICS
83.180 - Adhesives
Technical Committee
D14 - Adhesives
Drafting Committee
D14.60 - Adhesive Material Classification System
Current Stage
Ref Project

Relations

Replaced By
ASTM D4562-01 - Standard Test Method for Shear Strength of Adhesives Using Pin-and-Collar Specimen
Effective Date
10-Mar-2001
Referred By
ASTM D6465-99(2016) - Standard Guide for Selecting Aerospace and General Purpose Adhesives and Sealants
Effective Date
01-Jan-1995
Referred By
ASTM D4800-94(2023) - Standard Guide for Classifying and Specifying Adhesives
Effective Date
01-Jan-1995
Referred By
ASTM D5363-16 - Standard Specification for Anaerobic Single-Component Adhesives (AN)
Effective Date
01-Jan-1995
Referred By
ASTM D4896-01(2016) - Standard Guide for Use of Adhesive-Bonded Single Lap-Joint Specimen Test Results
Effective Date
01-Jan-1995

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ASTM D4562-90(1995)e1 - Standard Test Method for Shear Strength of Adhesives Using Pin-and-Collar SpecimenASTM D4562-90(1995)e1 - Standard Test Method for Shear Strength of Adhesives Using Pin-and-Collar Specimen
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ASTM D4562-90(1995)e1 - Standard Test Method for Shear Strength of Adhesives Using Pin-and-Collar Specimen
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NOTICE: This standard has either been superseded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
e1
Designation: D 4562 – 90 (Reapproved 1995)
Standard Test Method for
Shear Strength of Adhesives Using Pin-and-Collar
Specimen
This standard is issued under the fixed designation D 4562; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
e NOTE—Section 11 was added editorially in May 1995.
1. Scope shearing forces. It may also be used to determine degree of
cure and the effect of environment on shear strength.
1.1 This test method covers the determination of the shear
strength of curing liquid adhesives used for retaining cylindri-
6. Apparatus
cal assemblies or for locking and sealing threaded fasteners.
6.1 Universal Test Machine, or equivalent, for applying
1.2 This standard does not purport to address all of the
force to the specimen. Details of the test specimen (pin-and-
safety concerns, if any, associated with its use. It is the
collar) are given in Fig. 1.
responsibility of the user of this standard to establish appro-
6.2 Specimen Curing Rack, as shown in Fig. 2, or equiva-
priate safety and health practices and determine the applica-
lent.
bility of regulatory limitations prior to use.
7. Preparation of Test Specimens
2. Referenced Documents
7.1 Assemble five specimens for each test as described in
2.1 ASTM Standards:
the following paragraphs:
A 108 Specification for Steel Bars, Carbon, Cold-Finished,
2 7.1.1 Each specimen shall be comprised of a pin 0.498 to
Standard Quality
3 0.499 in. (12.65 to 12.675 mm) in diameter and a slip collar
D 907 Terminology of Adhesives
0.500 to 0.501 in. (12.7 to 12.725 mm) inside diameter by
D 2651 Guide for Preparation of Metal Surfaces for Adhe-
0.435 to 0.439 in. (11.05 to 11.15 mm) wide, both components
sive Bonding
finished to 32 to 64 μin (0.8 to 1.6μ m) with 0.001 to 0.003 in.
E 177 Practice for Use of the Terms Precision and Bias in
(0.025 to 0.075 mm) diametral clearance between the pin and
ASTM Test Methods
collar (see Fig. 1). The pin and collar, by agreement, may be
E 691 Practice for Conducting an Interlaboratory Study to
made of any material (see Appendix X1), but the most common
Determine the Precision of a Test Method
material is steel, as specified in Specification A 108.
3. Terminology 7.1.2 Vapor degrease all pins and collars (refer to Practice
D 2651), store in an atmosphere of low humidity (20 % relative
3.1 Definitions—Many of the terms in this standard are
humidity), and keep them clean. Use degreased specimens
defined in Terminology D 907.
within four days or discard. (Oxidation affects the test results
4. Summary of Test Method after this time. Prior to vapor degreasing, it is permissible to
soak or wash hard-greased or waxed parts in solvent.) Do not
4.1 This test method consists of bonding a metal pin inside
prime or activate unless specified for the material to be tested.
a metal collar and determining the force required to shear the
7.1.3 To apply the adhesive, assemble the parts to be sure
adhesive joint.
that there are no nicks that will cause them to stick or drag.
5. Significance and Use
Disassemble the parts. Apply sufficient adhesive to the circum-
ference of the pin, beginning at one end, to completely cover an
5.1 This test method provides reasonably accurate informa-
area the width of the collar in its final position. Also apply
tion with regard to the ability of an adhesive to withstand
sufficient adhesive to completely cover the interior of the collar
360°. Slip the collar over the coated end of the pin with at least
This test method is under the jurisdiction of ASTM Committee D-14 on
180° of rotation as the collar travels over the adhesive. Repeat
Adhesives and is the direct responsibility of Subcommittee D14.80 on Metal
Bonding Adhesives. a back-and-forth rotation three times, or until the collar
Current edition approved Aug. 31, 1990. Published October 1990. Originally
exhibits a smooth, consistent resistance to rotation.
published as D 4562 – 86. Last previous edition D 4562 – 86.
7.1.4 Rack the assembly with the fillet up so that the collar
Annual Book of ASTM Standards, Vol 01.05.
does not slip out of the bond area. Take care that the rack is at
Annual Book of ASTM Standards, Vol 15.06.
Annual Book of ASTM Standards, Vol 14.02.
Copyright © ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States.
D 4562
information is available to the individual conducting the tests,
the manufacturer of the adhesive shall furnish numerical values
and other specific information for each of the following
variables:
7.1.6.1 Directions for mixing the adhesive, if necessary.
7.1.6.2 Instructions for preconditioning the test specimens
or adhesive, including desired temperature, relative humidity,
and length of time.
7.1.6.3 Procedure for conditioning before testing, including
the length of time, temperature, and relative humidity.
8. Procedure
8.1 After allowing for cure and any planned environmental
conditioning, determine the static shear strength as follows:
8.1.1 Place the pin and collar assembly on the universal test
machine as shown in Fig. 3. Load the specimen smoothly at
about 500 lb/s (2200 N/s) using a free crosshead speed of 0.05
in./min (1.3 mm/min). Record the maximum load in pounds
(Newtons). Calculate the static shear strength by dividing the
breakaway load by the bond area as follows:
Shear Strength 5 Maximum Load/Diameter 3 3.14 3 Width
9. Report
9.1 Report the following information:
FIG. 1 Pin-and-Collar Assembly
9.1.1 Complete identification of the adhesiv
...

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1.1.1 The performance of the adhesives is measured in the following tests:    
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ASTM D907-15(2023)(Terminology)
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SCOPE
1.1 This terminology standard is a compilation of definitions used in the science and technology of the adhesives industry. Terms that are generally understood or adequately defined in other readily available sources are not included.  
1.2 Any changes in this standard since 1988 are documented as follows:  
1.2.1 Appendix X1 gives a history of revisions made since 1988. Table X1.1 lists the terms that are affected as: (1) Terms Added, (2) Terms Revised, and (3) Terms Deleted.
1.2.1.1 In Table X1.1, the year of publication in Volume 15.06 is shown in parentheses following the term.  
1.2.2 In the text of the standard, the year of publication is shown following each definition. Also, the following codes are included after the year of publication to describe the type change that was made: (A) Addition, (R) Revision, or (E) Edited.  
1.2.3 Deletions are shown in Appendix X1, suitably footnoted. The deleted terms do not appear in the text of the standard.  
1.2.4 Any special circumstances not covered by 1.2.2 and 1.2.3 are documented in Table X1.1, suitably footnoted.  
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ASTM D7966/D7966M-16(2023)(Test Method)
Standard Test Method for Resistance to Creep of Adhesives in Static Shear by Compression Loading (Wood-to-Wood)

SIGNIFICANCE AND USE
5.1 This test method evaluates the performance of the adhesive in laminated wood as measured by resistance to creep under static load.  
5.2 Test results from the evaluation of adhesive creep resistance, under designated environmental conditions of the test, provide a measure of the adhesive’s ability to withstand constant loading over a relatively long period of time.  
5.3 Creep measured with this test method is normally used in conjunction with specifications such as, but not limited to Specification D2559 and CSA O112.9 to confirm suitability of an adhesive to resist creep under designed loads when subjected to specific levels of stress, load duration and environmental conditions.
SCOPE
1.1 This test method covers the determination of creep properties of structural adhesives in wood-to-wood bonds when a standardized specimen is subjected to shearing stresses at various levels of static load, constant temperature, and relative humidity. Apparatus and procedures are provided for shear deformation (creep) of adhesive bonds under static load. This test method is used under the indicated conditions to evaluate resistance to creep properties of a structural wood adhesive.  
1.2 The test method is used to evaluate creep performance of adhesives suitable for the bonding of wood, including treated wood, into structural wood products for general construction, marine use, or for other uses where a high-strength general construction, creep-resistant, durable adhesive bond is required. Individual block shear specimens are prepared from adhesively bonded laminations, subjected to a constant load under various combinations of temperature and relative humidity, and the amount of creep measured.  
1.3 Creep of structural wood adhesives as measured by this test method may not be comparative to other ASTM methods and is limited to the conditions of the test and procedures contained herein.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
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Standard Guide for Classifying and Specifying Adhesives

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4.1 The purpose of this classification system is to provide a method of identifying adhesives in order to give industry a system that can be used universally for materials. It further provides a means for specifying these materials by the use of the standards that are developed using this guide.  
4.2 This classification system was developed to permit the addition of future adhesives.
SCOPE
1.1 This guide provides a classification system for tabulating the properties of adhesives suitable for holding parts or assemblies together. The use of this guide also provides information necessary for the development of standard specifications for adhesives.  
Note 1: This classification system may serve many of the needs of industries using adhesives. This guide is subject to revision as the need requires; therefore, the latest revision should always be used.  
1.2 Limitations—This classification system is intended to be a means of identifying adhesives. It is not intended for the selection of materials. Material selection should be made by those having expertise in the adhesives field after careful consideration of the design and the performance required of the part, the environment to which it will be exposed, the attachment process to be employed, the inherent properties of the material not covered in this document, and the economic factors.  
1.3 This classification system is based on the premise that adhesives can be arranged into broad generic families using basic properties to arrange the materials into groups, classes, and grades.  
1.4 In all cases where the provisions of this classification system would conflict with the referenced ASTM specification for a particular material, the latter shall take precedence.  
1.5 The values stated in SI units, as detailed in IEEE/ASTM SI 10, are to be regarded as the standard.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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