ASTM D36-95(2000)e1
(Test Method)Standard Test Method for Softening Point of Bitumen (Ring-and-Ball Apparatus)
Standard Test Method for Softening Point of Bitumen (Ring-and-Ball Apparatus)
SCOPE
1.1 This test method covers the determination of the softening point of bitumen in the range from 30 to 157°C (86 to 315°F) using the ring-and-ball apparatus immersed in distilled water (30 to 80°C), USP glycerin (above 80 to 157°C), or ethylene glycol (30 to 110°C).
1.2 The values stated in SI units are to be regarded as the standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
General Information
Relations
Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
e1
Designation:D36–95 (Reapproved 2000)
Standard Test Method for
Softening Point of Bitumen (Ring-and-Ball Apparatus)
ThisstandardisissuedunderthefixeddesignationD36;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginal
adoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperscript
epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
e NOTE—Editorially switched from English dominant to SI dominant.
1. Scope meanofthetemperaturesatwhichthetwodiskssoftenenough
to allow each ball, enveloped in bitumen, to fall a distance of
1.1 This test method covers the determination of the soft-
25 mm (1.0 in.).
ening point of bitumen in the range from 30 to 157°C (86 to
315°F) using the ring-and-ball apparatus immersed in distilled
4. Significance and Use
water (30 to 80°C), USP glycerin (above 80 to 157°C), or
4.1 Bitumens are viscoelastic materials without sharply
ethylene glycol (30 to 110°C).
defined melting points; they gradually become softer and less
1.2 The values stated in SI units are to be regarded as the
viscous as the temperature rises. For this reason, softening
standard.
points must be determined by an arbitrary and closely defined
1.3 This standard does not purport to address all of the
method if results are to be reproducible.
safety concerns, if any, associated with its use. It is the
4.2 The softening point is useful in the classification of
responsibility of the user of this standard to establish appro-
bitumens, as one element in establishing the uniformity of
priate safety and health practices and determine the applica-
shipments or sources of supply, and is indicative of the
bility of regulatory limitations prior to use.
tendency of the material to flow at elevated temperatures
2. Referenced Documents encountered in service.
2.1 ASTM Standards:
5. Apparatus
C670 Practice for Preparing Precision and Bias Statements
2 5.1 Rings—Two square-shouldered brass rings conforming
for Test Methods for Construction Materials
to the dimensions shown in Fig. 1(a).
D92 Test Method for Flash and Fire Points by Cleveland
3 5.2 Pouring Plate— A flat, smooth, brass plate approxi-
Open Cup
4 mately 50 by 75 mm (2 by 3 in.).
D140 Practice for Sampling Bituminous Materials
5.3 Balls—Twosteelballs,9.5mm( ⁄8in.)indiameter,each
D3461 Test Method for Softening Point of Asphalt and
5 having a mass of 3.50 6 0.05 g.
Pitch (Mettler Cup-and-Ball Method)
6 5.4 Ball-Centering Guides—Two brass guides for centering
E1 Specification for ASTM Thermometers
the steel balls, one for each ring, conforming to the general
3. Summary of Test Method shape and dimensions shown in Fig. 1 (b).
5.5 Bath—A glass vessel, capable of being heated, not less
3.1 Two horizontal disks of bitumen, cast in shouldered
than 85 mm in inside diameter and not less than 120 mm in
brassrings,areheatedatacontrolledrateinaliquidbathwhile
depth from the bottom of the flare.
eachsupportsasteelball.Thesofteningpointisreportedasthe
NOTE 1—An 800-mL, low-form Griffin beaker of heat-resistant glass
meets this requirement.
This test method is under the jurisdiction of ASTM Committee D08 on
5.6 Ring Holder andAssembly—Abrass holder designed to
Roofing,Waterproofing,andBituminousMaterialsandisthedirectresponsibilityof
Subcommittee D08.03 on Surfacing and Bituminous Materials for Membrane
support the two rings in a horizontal position, conforming to
Waterproofing and Builtup Roofing.
the shape and dimensions shown in Fig. 1 (c), supported in the
Current edition approved Oct. 10, 1995. Published December 1995. Originally
e1 assemblyillustratedinFig.1(d).Thebottomoftheshouldered
published as D36–62T. Last previous edition D36–86(1993) .
Annual Book of ASTM Standards, Vol 04.02. rings in the ring holder shall be 25 mm (1.0 in.) above the
Annual Book of ASTM Standards, Vol 05.01.
upper surface of the bottom plate, and the lower surface of the
Annual Book of ASTM Standards, Vol 04.03.
5 1
bottom plate shall be 1663mm( ⁄8 6 ⁄8 in.) from the bottom
Annual Book of ASTM Standards, Vol 04.04.
of the bath.
Annual Book of ASTM Standards, Vol 14.03.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D36
NOTE 1—All dimensions are in millimetres.
FIG. 1 Shouldered Ring, Ball-Centering Guide, Ring Holder, and Assembly of Apparatus Showing Two Rings
5.7 Thermometers: 6.1.2 USP Glycerin,or
5.7.1 AnASTM Low Softening PointThermometer, having
NOTE 3—Caution:Glycerin has a flash point of 160°C (320°F) in
a range from−2 to+80°C or 30 to 180°F, and conforming to
accordance with Test Method D92.
the requirements forThermometer 15C or 15F as prescribed in
6.1.3 EthyleneGlycol,withaboilingpointbetween195and
Specification E1.
197°C (383 and 387°F).
5.7.2 AnASTMHighSofteningPointThermometer,having
arangefrom30to200°Cor85to392°F,andconformingtothe
NOTE 4—Caution:Ethylene glycol is toxic when taken internally or
requirements for Thermometer 16C or 16F as prescribed in
inhaled as a vapor. Avoid prolonged or repeated skin contact and
inhalation of vapors. Its flash point is 115°C (239°F) in accordance with
Specification E1.
Test Method D92. When using this bath liquid, conduct the test in a
5.7.3 The appropriate thermometer shall be suspended in
vented laboratory hood with adequate exhaust fan capacity to ensure
the assembly as shown in Fig. 1 (d) so that the bottom of the
removal of toxic vapors.
bulb is level with the bottom of the rings and within 13 mm
(0.5 in.) of the rings, but not touching them or the ring holder. 6.2 Release Agents:
Substitution of other thermometers shall not be permittted. 6.2.1 To prevent adhesion of bitumen to the pouring plate
when casting disks, the surface of the brass pouring plate may
6. Reagents and Materials
be thinly coated just before use with silicone oil or grease
6.1 Bath Liquids:
(Note 5), a mixture of glycerin and dextrin, talc, or china clay.
6.1.1 Freshly Boiled Distilled Water.
NOTE 5—Caution:Isolate silicones from other bituminous testing
NOTE 2—The use of freshly boiled distilled water is essential to avoid equipment and samples to avoid contamination, and wear disposable
trapping air bubbles on the surface of the specimen which may affect the rubbergloveswheneverhandlingsiliconesorapparatuscoatedwiththem.
results. Siliconecontaminationcanproduceerroneousresultsinothertestssuchas
D36
1 1
those for penetration and flash point.
3mm(4 ⁄8 6 ⁄8 in.) with the apparatus in place. If using
ethylene glycol, make sure the hood exhaust fan is turned on
7. Sampling
and operating properly to remove toxic vapors. Using forceps,
7.1 Sample the material in accordance with Practice D140.
place the two steel balls in the bottom of the bath so they will
reachthesamestartingtemperatureastherestoftheassembly.
8. Test Specimens
9.3 Placethebathinicewater,ifnecessary,orgentlyheatto
8.1 Do not start unless it is planned to complete preparation establish and maintain the proper starting bath temperature for
and testing of all asphalt specimens within 6 h and all coal-tar 15 min with the apparatus in place. Take care not to contami-
pitch specimens within 4 ⁄2 h. Heat the bitumen sample with nate the bath liquid.
care, stirring frequently to prevent local overheating, until it
9.4 Again using forceps, place a ball from the bottom of the
has become sufficiently fluid to pour (Note 6). Stir carefully to
bath in each ball-centering guide.
avoid incorporation of air bubbles in the sample.
9.5 Heat the bath from below so that the temperature
indicated by the thermometer rises at a uniform rate of 5°C
NOTE 6—An electric hot plate having a minimum power to unit-
(9°F)/min (Note 7). Protect the bath from drafts, using shields
surface-area ratio of 37 kW/m has been found satisfactory for this
purpose. if necessary. Do not average the rate of temperature rise over
the test period. The maximum permissible variation for any
8.1.
...
Questions, Comments and Discussion
Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.