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ASTM D7109-22e1

(Test Method)

Standard Test Method for Shear Stability of Polymer-Containing Fluids Using a European Diesel Injector Apparatus at 30 Cycles and 90 Cycles

Standard Test Method for Shear Stability of Polymer-Containing Fluids Using a European Diesel Injector Apparatus at 30 Cycles and 90 Cycles

SIGNIFICANCE AND USE
5.1 This test method evaluates the percent viscosity loss of fluids resulting from physical degradation in the high shear nozzle device. Thermal or oxidative effects are minimized.  
5.2 This test method may be used for quality control purposes by manufacturers of polymeric lubricant additives and their customers.  
5.3 This test method is not intended to predict viscosity loss in field service in different field equipment under widely varying operating conditions, which may cause lubricant viscosity to change due to thermal and oxidative changes, as well as by the mechanical shearing of polymer. However, when the field service conditions, primarily or exclusively, result in the degradation of polymer by mechanical shearing, there may be a correlation between the results from this test method and results from the field.
SCOPE
1.1 This test method covers the evaluation of the shear stability of polymer-containing fluids. The test method measures the viscosity loss, in mm2/s and percent, at 100 °C of polymer-containing fluids when evaluated by a diesel injector apparatus procedure that uses European diesel injector test equipment. The viscosity loss reflects polymer degradation due to shear at the nozzle. Viscosity loss is evaluated after both 30 cycles and 90 cycles of shearing.
Note 1: This test method evaluates the shear stability of oils after both 30 cycles and 90 cycles of shearing. For most oils, there is a correlation between results after 30 cycles and results after 90 cycles of shearing, but this is not universal.
Note 2: Test Method D6278 uses essentially the same procedure with 30 cycles but without the 90 cycles portion of the test. The correlation between results from this test method at 30 cycles and results from Test Method D6278 has been established and shown in Research Report RR:D02-1629 to be equivalent.
Note 3: Test Method D2603 has been used for similar evaluation of shear stability; limitations are as indicated in the significance statement. No detailed attempt has been undertaken to correlate the results of this test method with those of the sonic shear test method.
Note 4: This test method uses test apparatus as defined in CEC L-14-A-93. This test method differs from CEC-L-14-A-93 in the period of time required for calibration.
Note 5: Test Method D5275 also shears oils in a diesel injector apparatus but may give different results.
Note 6: This test method has different calibration and operational requirements than withdrawn Test Method D3945.  
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in Section 8.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
30-Apr-2022
ICS
17.060 - Measurement of volume, mass, density, viscosity
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.07 - Flow Properties
Current Stage
Ref Project

Relations

Refers
ASTM D2603-20 - Standard Test Method for Sonic Shear Stability of Polymer-Containing Oils
Effective Date
01-May-2020
Refers
ASTM D5275-20 - Standard Test Method for Fuel Injector Shear Stability Test (FISST) for Polymer Containing Fluids
Effective Date
01-May-2020
Refers
ASTM D6278-20 - Standard Test Method for Shear Stability of Polymer Containing Fluids Using a European Diesel Injector Apparatus
Effective Date
01-May-2020
Refers
ASTM D6278-20a - Standard Test Method for Shear Stability of Polymer Containing Fluids Using a European Diesel Injector Apparatus
Effective Date
01-Jun-2020

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ASTM D7109-22e1 - Standard Test Method for Shear Stability of Polymer-Containing Fluids Using a European Diesel Injector Apparatus at 30 Cycles and 90 CyclesASTM D7109-22e1 - Standard Test Method for Shear Stability of Polymer-Containing Fluids Using a European Diesel Injector Apparatus at 30 Cycles and 90 Cycles
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ASTM D7109-22e1 - Standard Test Method for Shear Stability of Polymer-Containing Fluids Using a European Diesel Injector Apparatus at 30 Cycles and 90 Cycles
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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
´1
Designation: D7109 − 22
Standard Test Method for
Shear Stability of Polymer-Containing Fluids Using a
European Diesel Injector Apparatus at 30 Cycles and 90
1
Cycles
This standard is issued under the fixed designation D7109; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1
ε NOTE—Editorially added Research Report RR:D02-2041 in December 2022.
1. Scope* mine the applicability of regulatory limitations prior to use.
Specific warning statements are given in Section 8.
1.1 This test method covers the evaluation of the shear
1.4 This international standard was developed in accor-
stability of polymer-containing fluids. The test method mea-
2 dance with internationally recognized principles on standard-
sures the viscosity loss, in mm /s and percent, at 100 °C of
ization established in the Decision on Principles for the
polymer-containing fluids when evaluated by a diesel injector
Development of International Standards, Guides and Recom-
apparatus procedure that uses European diesel injector test
mendations issued by the World Trade Organization Technical
equipment.The viscosity loss reflects polymer degradation due
Barriers to Trade (TBT) Committee.
to shear at the nozzle. Viscosity loss is evaluated after both
30 cycles and 90 cycles of shearing.
2. Referenced Documents
NOTE 1—This test method evaluates the shear stability of oils after both
2
30 cycles and 90 cycles of shearing. For most oils, there is a correlation
2.1 ASTM Standards:
between results after 30 cycles and results after 90 cycles of shearing, but
D445 Test Method for Kinematic Viscosity of Transparent
this is not universal.
and Opaque Liquids (and Calculation of Dynamic Viscos-
NOTE 2—Test Method D6278 uses essentially the same procedure with
ity)
30 cycles but without the 90 cycles portion of the test. The correlation
between results from this test method at 30 cycles and results from Test
D2603 Test Method for Sonic Shear Stability of Polymer-
Method D6278 has been established and shown in Research Report
Containing Oils
RR:D02-2041 to be equivalent.
D5275 Test Method for Fuel Injector Shear Stability Test
NOTE 3—Test Method D2603 has been used for similar evaluation of
(FISST) for Polymer Containing Fluids
shear stability; limitations are as indicated in the significance statement.
Nodetailedattempthasbeenundertakentocorrelatetheresultsofthistest D6278 Test Method for Shear Stability of Polymer Contain-
method with those of the sonic shear test method.
ing Fluids Using a European Diesel Injector Apparatus
NOTE 4—This test method uses test apparatus as defined in CEC
D6299 Practice for Applying Statistical Quality Assurance
L-14-A-93.This test method differs from CEC-L-14-A-93 in the period of
and Control Charting Techniques to Evaluate Analytical
time required for calibration.
Measurement System Performance
NOTE 5—Test Method D5275 also shears oils in a diesel injector
apparatus but may give different results. D7042 Test Method for Dynamic Viscosity and Density of
NOTE 6—This test method has different calibration and operational
Liquids by Stabinger Viscometer (and the Calculation of
requirements than withdrawn Test Method D3945.
Kinematic Viscosity)
1.2 The values stated in SI units are to be regarded as
2.2 Coordinated European Council (CEC) Standard:
standard. The values given in parentheses after SI units are
CEC L-14-A-93 Evaluation of the Mechanical Shear Stabil-
3
provided for information only and are not considered standard.
ity of Lubricating Oils Containing Polymers
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the 3. Terminology
responsibility of the user of this standard to establish appro-
3.1 Definitions:
priate safety, health, and environmental practices and deter-
1 2
This test method is under the jurisdiction of ASTM Committee D02 on For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Subcommittee D02.07 on Flow Properties. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved May 1, 2022. Published May 2022. Originally the ASTM website.
3
approved in 2004. Last previous edition approved in 2020 as D7109 – 20a. DOI: Available from CEC Secretariat, InterlynkAdministrative Ser
...

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5.1 This practice covers a series of methods offered to aid users in calibrating U-tube density meters to provide a measure of density and an associated expanded uncertainty. The reference density, as obtained from either an equation of state (EOS) or CRM has an uncertainty that arises from the uncertainty of the measurements of temperature, pressure, and also the chemical purity of the substance studied (origin) or for that matter of the certified reference material. This uncertainty results in an additional uncertainty for the density of these samples. Because the measurements made with U-tube density meters are not absolute, the uncertainty with which the instrument calibration is determined is directly related to the uncertainty of the density obtained.
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1.3 This practice pertains to fluids with viscosities  
1.4 4 The values listed in SI units are regarded as the standard, unless otherwise stated. The SI unit for mass density is kilograms per cubic metre (kg·m-3) and can be given as grams per cubic centimetre (g·cm-3).  
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5.1 Density is a fundamental physical property that can be used in conjunction with other properties to characterize both the light and heavy fractions of petroleum and petroleum products.  
5.2 Determination of the density or relative density of petroleum and its products is necessary for the conversion of measured volumes to volumes at the standard temperature of 15 °C.
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1.1 This test method covers the determination of the density, relative density, and API Gravity of petroleum distillates and viscous oils that can be handled in a normal fashion as liquids at the temperature of test, utilizing either manual or automated sample injection equipment. Its application is restricted to liquids with total vapor pressures (see Test Method D5191) typically below 100 kPa and viscosities (see Test Method D445 or D7042) typically below about 15 000 mm2/s at the temperature of test. The total vapor pressure limitation however can be extended to >100 kPa provided that it is first ascertained that no bubbles form in the U-tube, which can affect the density determination. Some examples of products that may be tested by this procedure include: gasoline and gasoline-oxygenate blends, diesel, jet, basestocks, waxes, and lubricating oils.  
1.1.1 Waxes and highly viscous samples were not included in the 1999 interlaboratory study (ILS) sample set that was used to determine the current precision statements of the method, since all samples evaluated at the time were analyzed at a test temperature of 15 °C. Wax and highly viscous samples require a temperature cell operated at elevated temperatures necessary to ensure a liquid test specimen is introduced for analysis. Consult instrument manufacturer instructions for appropriate guidance and precautions when attempting to analyze wax or highly viscous samples. Refer to the Precision and Bias section of the method and Note 9 for more detailed information about the 1999 ILS that was conducted.  
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5.1 Many petroleum products, and some non-petroleum materials, are used as lubricants and the correct operation of the equipment depends upon the appropriate viscosity of the liquid being used. In addition, the viscosity of many petroleum fuels is important for the estimation of optimum storage, handling, and operational conditions. Thus, the accurate determination of viscosity is essential to many product specifications.  
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5.1 Density is a fundamental physical property that can be used in conjunction with other properties to characterize both the light and heavy fractions of petroleum and to assess the quality of crude oils.  
5.2 Determination of the density or relative density of petroleum and its products is necessary for the conversion of measured volumes to volumes at the standard temperatures of 15 °C.  
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1.1 This test method covers two procedures for the measurement of the density of materials which are fluid at the desired test temperature. Its application is restricted to liquids of vapor pressures below 80 kPa (600 mm Hg) and viscosities below 40 000 mm2/s (cSt) at the test temperature. The method is designed for use at any temperature between 20 °C and 100 °C. It can be used at higher temperatures; however, in this case the precision section does not apply.  
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1.2 This test method provides a calculation procedure for converting density to specific gravity.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
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ASTM D7483-21(Test Method)
Standard Test Method for Determination of Dynamic Viscosity and Derived Kinematic Viscosity of Liquids by Oscillating Piston Viscometer

SIGNIFICANCE AND USE
5.1 Many petroleum products, as well as non-petroleum materials, are used as lubricants for bearings, gears, compressor cylinders, hydraulic equipment, etc. Proper operation of this equipment depends upon the viscosity of these liquids.  
5.2 Oscillating piston viscometers allow viscosity measurement of a broad range of materials including transparent, translucent and opaque liquids. The measurement principle and stainless steel construction makes the Oscillating Piston Viscometer resistant to damage and suitable for portable operations. The measurement itself is automatic and does not require an operator to time the oscillation of the piston. The electromagnetically driven piston mixes the sample while under test. The instrument requires a sample volume of less than 5 mL and typical solvent volume of less than 10 mL which minimizes cleanup effort and waste.
SCOPE
1.1 This test method covers the measurement of dynamic viscosity and derivation of kinematic viscosity of liquids, such as new and in-service lubricating oils, by means of an oscillating piston viscometer.  
1.2 This test method is applicable to Newtonian and non-Newtonian liquids; however the precision statement was developed using Newtonian liquids.  
1.3 The range of dynamic viscosity covered by this test method is from 0.2 mPa·s to 20 000 mPa·s (which is approximately the kinematic viscosity range of 0.2 mm2/s to 22 000 mm2/s for new oils) in the temperature range between –40 °C to 190 °C; however the precision has been determined only for new and used oils in the range of 34 mPa·s to 1150 mPa·s at 40 °C, 5.7 mPa·s to 131 mPa·s at 100 °C, and 46.5 mm2/s to 436 mm2/s at 40 °C.  
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ASTM D6616-21(Test Method)
Standard Test Method for Measuring Viscosity at High Shear Rate by Tapered Bearing Simulator Viscometer at 100 °C

SIGNIFICANCE AND USE
5.1 Viscosity at the shear rate and temperature of this test method is thought to be particularly representative of bearing conditions in large medium speed reciprocating engines as well as automotive and heavy duty engines operating in this temperature regime.  
5.2 The importance of viscosity under these conditions has been stressed in railroad specifications.  
5.3 For other industry needs this method may also be run at 80 °C by using different crossover calibration oils available from the manufacturer. No precision has been determined at this temperature. The equipment is also used at higher temperatures as shown in Test Method D4683 and CEC L-36-90 (also referenced from IP 370).
SCOPE
1.1 This test method covers the laboratory determination of the viscosity of engine oils at 100 °C and 1·106s–1 using the Tapered Bearing Simulator (TBS) viscometer.2
Note 1: This test method is similar to Test Method D4683 which uses the same TBS viscometer to measure high shear viscosity at 150 °C.  
1.2 The Newtonian calibration oils used to establish this test method range from approximately 5 mPa·s (cP) to 12 mPa·s (cP) at 100 °C and either the manual or automated protocol was used by each participant in developing the precision statement. The viscosity range of the test method at this temperature is from 1 mPa·s (cP) to above 25 mPa·s (cP), depending on the model of TBS.  
1.3 The non-Newtonian reference oil used to establish the shear rate of 1·106s–1 for this test method has a viscosity of approximately 10 mPa·s at 100 °C.  
1.4 Application to petroleum products other than engine oil has not been determined in preparing the viscometric information for this test method.  
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. This test method uses the milliPascal second (mPa·s) as the unit of viscosity. This unit is equivalent to the centiPoise (cP), which is shown in parentheses.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and to determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D2161-20(Practice)
Standard Practice for Conversion of Kinematic Viscosity to Saybolt Universal Viscosity or to Saybolt Furol Viscosity

SIGNIFICANCE AND USE
4.1 At one time the petroleum industry relied on measuring kinematic viscosity by means of the Saybolt viscometer, and expressing kinematic viscosity in units of Saybolt Universal Seconds (SUS) and Saybolt Furol Seconds (SFS). This practice is now obsolete in the petroleum industry.  
4.2 This practice establishes the official equations relating SUS and SFS to the SI kinematic viscosity units, mm2/s.  
4.3 This practice allows for the conversion between SUS and SFS units and SI units of kinematic viscosity.
SCOPE
1.1 This practice2 covers the conversion tables and equations for converting kinematic viscosity in mm2/s at any temperature to Saybolt Universal viscosity in Saybolt Universal seconds (SUS) at the same temperature and for converting kinematic viscosity in mm2/s at 122 °F and 210 °F (50 °C and 98.9 °C) to Saybolt Furol viscosity in Saybolt Furol seconds (SFS) at the same temperatures. Kinematic viscosity values are based on water being 1.0034 mm2/s (cSt) at 68 °F (20 °C).  
1.2 If a method other than Test Method D445 is used to generate the kinematic viscosity data, apply appropriate relative-bias correction factors as found in the precision section of that method, before performing the calculations of this practice.
Note 1: The equations in D2161 were originally empirically derived using data from both D445 and the Saybolt viscometer method. Therefore, it is conceivable that an error could result if the kinematic viscosities used are not bias-corrected to D445 results. It is recommended that kinematic viscosity be reported in millimetres squared per second, instead of Saybolt Universal Seconds (SUS) or Saybolt Furol Seconds (SFS). This method is being retained for the purpose of calculation of kinematic viscosities from SUS and SFS data that appear in past literature. One millimetre squared per second (mm2/s) equals one centistoke (cSt), which is another unit commonly found in older literature.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for reference information purposes only. The SI unit of kinematic viscosity is mm2/s.  
1.3.1 Exception—Fahrenheit temperature units are used in this practice because they are accepted by industry for the type of legacy conversions described in this practice.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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