Standard Test Method for Measuring Non-Fibrous Content of Man-Made Rock and Slag Mineral Fiber Insulation

SIGNIFICANCE AND USE
Inorganic fibrous thermal insulation can contain varying amounts of non-fibrous material. Non-fibrous material does not contribute to the insulating value of the insulation and therefore a procedure for determining that amount is desirable. Several specifications refer to shot content and percent (%) retained on various screen sizes determined by this test method.
SCOPE
1.1 This test method covers a procedure for determining the non-fibrous content (shot) of man-made rock and slag mineral fiber insulation. The procedure covers a dry sieve analysis method to distinguish between fiberized and non-fiberized (shot) portions of a specimen of man-made rock and slag mineral fiber insulation specimen.
1.2 This test method does not apply to rock or slag materials containing any components other than rock and slag mineral fiber and organic thermal setting binders. Products containing other types of fibers, inorganic binders, or refractory clays are excluded.
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C1335 − 12
Standard Test Method for
Measuring Non-Fibrous Content of Man-Made Rock and
1
Slag Mineral Fiber Insulation
This standard is issued under the fixed designation C1335; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3. Terminology
1.1 This test method covers a procedure for determining the 3.1 Definitions—Terminology C168 shall be considered as
non-fibrous content (shot) of man-made rock and slag mineral applying to the terms used in this test method.
fiber insulation. The procedure covers a dry sieve analysis
3.2 Definitions of Terms Specific to This Standard:
method to distinguish between fiberized and non-fiberized
3.2.1 shot—material that cannot be brushed or mechanically
(shot) portions of a specimen of man-made rock and slag
shaken through a No. 100 (150 µm) sieve.
mineral fiber insulation specimen.
4. Significance and Use
1.2 This test method does not apply to rock or slag materials
containing any components other than rock and slag mineral
4.1 Inorganic fibrous thermal insulation can contain varying
fiber and organic thermal setting binders. Products containing
amountsofnon-fibrousmaterial.Non-fibrousmaterialdoesnot
other types of fibers, inorganic binders, or refractory clays are
contributetotheinsulatingvalueoftheinsulationandtherefore
excluded.
a procedure for determining that amount is desirable. Several
specifications refer to shot content and percent (%) retained on
1.3 The values stated in inch-pound units are to be regarded
various screen sizes determined by this test method.
as standard. The values given in parentheses are mathematical
conversions to SI units that are provided for information only
5. Apparatus
and are not considered standard.
5.1 Furnace, capable of maintaining 1100 6 10°F (593 6
1.4 This standard does not purport to address all of the
5.6°C) for rock and slag wool.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro- 5.2 U.S.A. Standard Sieve Shaker Machine.
priate safety and health practices and determine the applica-
5.3 Balance Scale, capable of weighing to an accuracy of
bility of regulatory limitations prior to use.
0.00035 oz (0.01 g).
2. Referenced Documents 5.4 Sieves—Three 8 in. (203 mm) diameter U.S.A. Standard
2 Sieves. Nos. 20 (850 µm), 50 (300 µm), and 100 (150 µm)
2.1 ASTM Standards:
nested in order with bottom receiver pan. All sieve design and
C168 Terminology Relating to Thermal Insulation
construction shall be in accordance with Specification E11.
C390 Practice for Sampling and Acceptance of Thermal
Insulation Lots 5.5 Brush—Approximately 1 in. (25 mm) diameter plastic
E11 Specification for Woven Wire Test Sieve Cloth and Test bristle brush, and approximately 1 in. (25 mm) wide soft paint
Sieves brush.
E178 Practice for Dealing With Outlying Observations
5.6 Crucible Weighing Dish, tared.
E691 Practice for Conducting an Interlaboratory Study to
5.7 Stoppers, rubber, No. 12 or 13.
Determine the Precision of a Test Method
5.8 Cork Borer, approximately 0.8 in. (20 mm) diameter.
1
ThistestmethodisunderthejurisdictionofASTMCommitteeC16onThermal
6. Sampling and Preparation of Test Specimen
Insulation and is the direct responsibility of Subcommittee C16.32 on Mechanical
Properties.
6.1 For the purposes of standard tests, sampling shall be in
CurrenteditionapprovedMay1,2012.PublishedJuly2012.Originallyapproved
accordance with Practice C390 and Practice E178 with a
in 1996. Last previous edition approved in 2009 as C1335 – 04(2009). DOI:
minimum of three specimens per lot to be tested.
10.1520/C1335-12.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 6.1.1 Specimen—This test method requires approximately a
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
0.35 oz (10 g) specimen.
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. 6.2 Specimen Preparation:
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1335 − 12
6.2.1 Obtainarepresentativespecimenutilizinga0.8in.(20
WT = mass of specimen after firing/before seperation.
mm) cork borer for blanket or board and random specimens for
8.2 Adding the total percentages of all WC(s) (minimum of
loosefill.Firethespecimeninatareddishat1100 610°F(593
three specimens/tests) and dividing by the number of WC(s)
6 5.6°C) for 15 min. Remove tared dish with specimen and
equals the average total percent of shot (shot co
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:C1335–04 (Reapproved 2009) Designation: C1335 – 12
Standard Test Method for
Measuring Non-Fibrous Content of Man-Made Rock and
1
Slag Mineral Fiber Insulation
This standard is issued under the fixed designation C1335; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers a procedure for determining the non-fibrous content (shot) of man-made rock and slag mineral fiber
insulation. The procedure covers a dry sieve analysis method to distinguish between fiberized and non-fiberized (shot) portions of
a specimen of man-made rock and slag mineral fiber insulation specimen.
1.2 This test method does not apply to rock or slag materials containing any components other than rock and slag mineral fiber
and organic thermal setting binders. Products containing other types of fibers, inorganic binders, or refractory clays are excluded.
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical
conversions to SI units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
C168 Terminology Relating to Thermal Insulation
C390 Practice for Sampling and Acceptance of Thermal Insulation Lots
E11 Specification for Woven Wire Test Sieve Cloth and Test Sieves
E178 Practice for Dealing With Outlying Observations
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
3. Terminology
3.1 Definitions—Terminology C168 shall be considered as applying to the terms used in this test method.
3.2 Definition of Term Specific to This Standard:
3.2.1 shot—material that cannot be brushed or mechanically shaken through a No. 100 (150 µm) sieve.
4. Significance and Use
4.1 Inorganic fibrous thermal insulation can contain varying amounts of non-fibrous material. Non-fibrous material does not
contribute to the insulating value of the insulation and therefore a procedure for determining that amount is desirable. Several
specifications refer to shot content and percent (%) retained on various screen sizes determined by this test method.
5. Apparatus
5.1 Furnace, capable of maintaining 1100 6 10°F (593 6 5.6°C) for rock and slag wool.
5.2 U.S.A. Standard Sieve Shaker Machine.
5.3 Balance Scale, capable of weighing to an accuracy of 0.00035 oz (0.01 g).
5.4 Sieves—Three 8 in. (203 mm) diameter U.S.A. Standard Sieves. Nos. 20 (850 µm), 50 (300 µm), and 100 (150 µm) nested
in order with bottom receiver pan. All sieve design and construction shall be in accordance with Specification E11.
5.5 Brush—Approximately 1 in. (25 mm) diameter plastic bristle brush, and approximately 1 in. (25 mm) wide soft paint brush.
5.6 Crucible Weighing Dish, tared.
1
This test method is under the jurisdiction of ASTM Committee C16 on Thermal Insulation and is the direct responsibility of Subcommittee C16.32 on Mechanical
Properties.
Current edition approved Sept.May 1, 2009.2012. Published September 2009.July 2012. Originally approved in 1996. Last previous edition approved in 20042009 as
C1335 – 04(2009). DOI: 10.1520/C1335-04R09.10.1520/C1335-12.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
C1335 – 12
5.7 Stoppers, rubber, No. 12 or 13.
5.8 Cork Borer, approximately 0.8 in. (20 mm) diameter.
6. Sampling and Preparation of Test Specimen
6.1 For the purposes of standard tests, sampling shall be in accordance with Practice C390 and Practice E178 with a minimum
of three specimens per lot to be tested.
6.1.1 Specimen—This test method requires approximately a 0.35 oz (10 g) specimen.
6.2 Specimen Preparation:
6.2.1 Obtain a representative specimen utilizing
...

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