Standard Specification for Expanded or Exfoliated Vermiculite Thermal Insulating Cement

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1.1 This specification covers expanded or exfoliated vermiculite thermal insulating material in the form of dry cement or plaster, intended to be mixed with a suitable proportion of water, applied as a plastic mass, and dried in place, for use as insulation on surfaces operating at temperatures between 100°F (38°C) and 1800°F (982°C). The cement shall not be used where it will be exposed to combustion conditions, such as the hot face lining of a furnace.  
1.2 The values stated in inch-pound units are to be regarded as the standard. The SI equivalents of inch-pound units are given in parentheses and may be approximate.  
1.3 The following safety hazards caveat pertains only to the test method portion, Section 9, of this specification. This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.4 When the installation or use of thermal insulation materials, accessories and systems, may pose safety or health problems, the manufacturer shall provide the user with appropriate current information regarding any known problems associated with the recommended use of the company's products. The manufacturer shall also recommend protective measures to be employed in the safe utilization of said products.

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Publication Date
09-Jan-2000
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ASTM C196-00 - Standard Specification for Expanded or Exfoliated Vermiculite Thermal Insulating Cement
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C 196 – 00
Standard Specification for
Expanded or Exfoliated Vermiculite Thermal Insulating
Cement
This standard is issued under the fixed designation C 196; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope C 166 Test Method for Covering Capacity and Volume
Change Upon Drying of Thermal Insulating Cement
1.1 This specification covers expanded or exfoliated ver-
C 168 Terminology Relating to Thermal Insulating Materi-
miculite thermal insulating material in the form of dry cement
als
or plaster, intended to be mixed with a suitable proportion of
C 177 Test Method for Steady-State Heat Flux Measure-
water, applied as a plastic mass, and dried in place, for use as
ments and Thermal Transmission Properties by Means of
insulation on surfaces operating at temperatures between
the Guarded-Hot-Plate Apparatus
100°F (38°C) and 1800°F (982°C). The cement shall not be
C 353 Test Method for Adhesion of Dried Thermal Insulat-
used where it will be exposed to combustion conditions, such
ing or Finishing Cement
as the hot face lining of a furnace.
C 354 Test Method for Compressive Strength of Thermal
1.2 The values stated in inch-pound units are to be regarded
Insulating or Finishing Cement
as the standard. The SI equivalents of inch-pound units are
C 356 Test Method for Linear Shrinkage of Preformed
given in parentheses and may be approximate.
High-Temperature Thermal Insulation Subjected to Soak-
1.3 The following safety hazards caveat pertains only to the
ing Heat
test method portion, Section 10, of this specification. This
C 390 Criteria for Sampling and Acceptance of Preformed
standard does not purport to address all of the safety concerns,
Thermal Insulation Lots
if any, associated with its use. It is the responsibility of the user
C 405 Practice for Estimating Consistency of Wet-Mixed
of this standard to establish appropriate safety and health
Thermal Insulating Cement
practices and determine the applicability of regulatory limita-
C 518 Test Method for Steady-State Heat Flux Measure-
tions prior to use.
ments and Thermal Transmission Properties by Means of
1.4 When the installation or use of thermal insulation
the Heat Flow Meter Apparatus
materials, accessories and systems, may pose safety or health
C 1058 Practice for Selecting Temperatures for Reporting
problems, the manufacturer shall provide the user with appro-
and Evaluating Thermal Properties of Thermal Insulation
priate current information regarding any known problems
associated with the recommended use of the company’s
3. Terminology
products. The manufacturer shall also recommend protective
3.1 Definitions:
measures to be employed in the safe utilization of said
3.2 Terminology C 168 shall be considered as applying to
products.
the terms used in this specification.
2. Referenced Documents
4. Materials and Manufacture
2.1 ASTM Standards:
4.1 The cement shall be composed predominantly of ex-
C 163 Practice for Mixing Thermal Insulating Cement
panded or exfoliated vermiculite, with a suitable proportion of
Samples
heat-resistant binder. Asbestos shall not be used as an ingredi-
ent or component part of the product.
This specification is under the jurisdiction of ASTM Committee C-16 on
Thermal Insulation and is the direct responsibility of Subcommittee C16.20 on
Homogeneous Inorganic Thermal Insulations.
Current edition approved Jan. 10, 2000. Published April 2000. Originally
published as C 196 – 44 T. Last previous edition C 196 – 93.
Annual Book of ASTM Standards, Vol 04.06.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
C 196
5. Other Requirements 9. Specimen Preparation
5.1 The cement shall conform to the requirements given in 9.1 Mix specimens for testing in accordance with Practice
Table 1. Conformance shall be based on results of tests on C 163.
specimens first mixed with water, according to the ratio for 9.2 The amount of water to be used in preparing samples for
proper troweling consistency determined in accordance with all tests shall be that amount which results in the specified
Section 10. consistency, determined in accordance with Practice C 405.
10. Test Methods
6. Qualification Requirements
10.1 Consistency— Practice C 405.
6.1 The following requirements are employed for purposes
10.2 Dry Covering Capacity—Test Method C 166.
of initial material or product qualification:
10.3 Volume Change upon Drying—Test Method C 166.
6.1.1 Consistency,
10.4 Compressive Strength—Test Method C 354.
6.1.2 Compressive strength,
10.5 Linear Shrinkage— Test Method C 356.
6.1.3 Linear shrinkage,
10.6 Apparent Thermal Conductivity—Test Method C 177
6.1.4 Apparent thermal conductivity, and
or Test Method C 518, except prepare the test specimens as
6.1.5 Dry adhesion to steel.
follows:
10.6.1 Mold test specimens in a mold of suitable size and
7. Sampling
shape for the equipment to be used and 1 ⁄2 in. (38 mm) in
7.1 The cement shall be sampled, for the purpose of tests
depth. The cement shall be mixed with water in accordance
using one of the following procedures.
with Practice C 163. Place the mold in a horizontal position on
7.1.1 Inspection Requirements:
a piece of glass 14 in. (356 mm) or 15 in. (381 mm) square, or
7.1.1.1 Use Criteria C 390. Each bag shall represent a unit.
slightly larger than the specimen required. Place the mixed
7.1.1.2 In a single sampling plan by attributes the accept-
cemen
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