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ASTM D5334-22ae1

(Test Method)

Standard Test Method for Determination of Thermal Conductivity of Soil and Rock by Thermal Needle Probe Procedure

Standard Test Method for Determination of Thermal Conductivity of Soil and Rock by Thermal Needle Probe Procedure

SIGNIFICANCE AND USE
5.1 The thermal conductivity of intact soil specimens, reconstituted soil specimens, and rock specimens is used to analyze and design systems involving underground transmission lines, oil and gas pipelines, radioactive waste disposal, geothermal applications, and solar thermal storage facilities, among others. Measurements can be made on site (in situ), or samples can be tested in a lab environment.
Note 2: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing. Users of this standard are cautioned that compliance with Practice D3740 does not in itself ensure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 This test method presents a procedure for determining the thermal conductivity (λ) of soil and rock using a transient heat method. This test method is applicable for both intact specimens of soil and rock and reconstituted soil specimens, and is effective in the lab and in the field. This test method is most suitable for homogeneous materials, but can also give a representative average value for non-homogeneous materials.  
1.2 This test method is applicable to dry, unsaturated or saturated materials that can sustain a hole for the sensor. It is valid over temperatures ranging from 100°C, depending on the suitability of the thermal needle probe construction to temperature extremes. However, care must be taken to prevent significant error from: (1) redistribution of water due to thermal gradients resulting from heating of the needle probe; (2) redistribution of water due to hydraulic gradients (gravity drainage for high degrees of saturation or surface evaporation); (3) phase change of water in specimens with temperatures near 0°C or 100°C.  
1.3 Units—The values stated in SI units are to be regarded as the standard. No other units of measurements are included in this standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.  
1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.  
1.4.1 The procedures used to specify how data are collected/recorded or calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analytical methods for engineering design.
Note 1: This test method is also applicable and commonly used for determining thermal conductivity of a variety of engineered porous materials of geologic origin including concrete, Fluidized Thermal Backfill (FTB), and thermal grout.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
30-Sep-2022
ICS
13.080.20 - Physical properties of soils
Technical Committee
D18 - Soil and Rock
Drafting Committee
D18.12 - Rock Mechanics
Current Stage
Ref Project

Relations

Replaces
ASTM D5334-22a - Standard Test Method for Determination of Thermal Conductivity of Soil and Rock by Thermal Needle Probe Procedure
Effective Date
01-Oct-2022
Referred By
ASTM C1903-21 - Standard Specification for Precast Concrete Duct Bank
Effective Date
01-Oct-2022
Referred By
ASTM D4612-16 - Standard Test Method for Calculating Thermal Diffusivity of Rock and Soil
Effective Date
01-Oct-2022
Referred By
ASTM D7294-13(2021) - Standard Guide for Collecting Treatment Process Design Data at a Contaminated Site—A Site Contaminated with Chemicals of Interest
Effective Date
01-Oct-2022

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ASTM D5334-22ae1 - Standard Test Method for Determination of Thermal Conductivity of Soil and Rock by Thermal Needle Probe ProcedureASTM D5334-22ae1 - Standard Test Method for Determination of Thermal Conductivity of Soil and Rock by Thermal Needle Probe Procedure
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ASTM D5334-22ae1 - Standard Test Method for Determination of Thermal Conductivity of Soil and Rock by Thermal Needle Probe Procedure
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
´1
Designation: D5334 − 22a
Standard Test Method for
Determination of Thermal Conductivity of Soil and Rock by
1
Thermal Needle Probe Procedure
This standard is issued under the fixed designation D5334; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1
ε NOTE—Editorially corrected dry density units in October 2023.
1. Scope* commensurate with these considerations. It is beyond the scope
of this standard to consider significant digits used in analytical
1.1 This test method presents a procedure for determining
methods for engineering design.
the thermal conductivity (λ) of soil and rock using a transient
NOTE 1—This test method is also applicable and commonly used for
heat method. This test method is applicable for both intact
determining thermal conductivity of a variety of engineered porous
specimens of soil and rock and reconstituted soil specimens,
materials of geologic origin including concrete, Fluidized Thermal Back-
and is effective in the lab and in the field. This test method is
fill (FTB), and thermal grout.
most suitable for homogeneous materials, but can also give a
1.5 This standard does not purport to address all of the
representative average value for non-homogeneous materials.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
1.2 This test method is applicable to dry, unsaturated or
priate safety, health, and environmental practices and deter-
saturated materials that can sustain a hole for the sensor. It is
mine the applicability of regulatory limitations prior to use.
valid over temperatures ranging from <0 to >100°C, depending
1.6 This international standard was developed in accor-
on the suitability of the thermal needle probe construction to
dance with internationally recognized principles on standard-
temperature extremes. However, care must be taken to prevent
ization established in the Decision on Principles for the
significant error from: (1) redistribution of water due to thermal
Development of International Standards, Guides and Recom-
gradients resulting from heating of the needle probe; (2)
mendations issued by the World Trade Organization Technical
redistribution of water due to hydraulic gradients (gravity
Barriers to Trade (TBT) Committee.
drainage for high degrees of saturation or surface evaporation);
(3) phase change of water in specimens with temperatures near
2. Referenced Documents
0°C or 100°C.
2
2.1 ASTM Standards:
1.3 Units—The values stated in SI units are to be regarded
D653 Terminology Relating to Soil, Rock, and Contained
as the standard. No other units of measurements are included in
Fluids
this standard. Reporting of test results in units other than SI
D2216 Test Methods for Laboratory Determination of Water
shall not be regarded as nonconformance with this standard.
(Moisture) Content of Soil and Rock by Mass
1.4 All observed and calculated values shall conform to the
D3740 Practice for Minimum Requirements for Agencies
guidelines for significant digits and rounding established in
Engaged in Testing and/or Inspection of Soil and Rock as
Practice D6026.
Used in Engineering Design and Construction
1.4.1 The procedures used to specify how data are collected/
D4753 Guide for Evaluating, Selecting, and Specifying Bal-
recorded or calculated in this standard are regarded as the
ances and Standard Masses for Use in Soil, Rock, and
industry standard. In addition, they are representative of the
Construction Materials Testing
significant digits that generally should be retained. The proce-
D6026 Practice for Using Significant Digits and Data Re-
dures used do not consider material variation, purpose for
cords in Geotechnical Data
obtaining the data, special purpose studies, or any consider-
3. Terminology
ations for the user’s objectives; and it is common practice to
increase or reduce significant digits of reported data to be
3.1 Definitions—For definitions of common technical terms
used in this standard, refer to Terminology D653.
1
This test method is under the jurisdiction of ASTM Committee D18 on Soil and
2
Rock and is the direct responsibility of Subcommittee D18.12 on Rock Mechanics. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Oct. 1, 2022. Published October 2022. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 1992. Last previous editi
...

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1.2 Methods A and B can be used to determine the angle of internal friction, angle of shearing resistance, and cohesion intercept.  
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ASTM D6938-23(Test Method)
Standard Test Methods for In-Place Density and Water Content of Soil and Soil-Aggregate by Nuclear Methods (Shallow Depth)

SIGNIFICANCE AND USE
4.1 The test method described is useful as a rapid, nondestructive technique for in-place measurements of wet density and water content of soil and soil-aggregate and the determination of dry density.  
4.2 The test method is used for quality control and acceptance testing of compacted soil and soil-aggregate mixtures as used in construction and also for research and development. The nondestructive nature allows repetitive measurements at a single test location and statistical analysis of the results.  
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Note 1: The quality of the result produced by this standard test method is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection, and the like. Users of this standard are cautioned that compliance with Practice D3740 does not in itself ensure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
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1.1 This test method describes the procedures for measuring in-place density and moisture of soil and soil-aggregate by use of nuclear equipment (hereafter referred to as “gauge”). The density of the material may be measured by direct transmission, backscatter, or backscatter/air-gap ratio methods. Measurements for water (moisture) content are taken at the surface in backscatter mode regardless of the mode being used for density.  
1.1.1 For limitations see Section 5 on Interferences.  
1.2 The total or wet density of soil and soil-aggregate is measured by the attenuation of gamma radiation where, in direct transmission, the source is placed at a known depth up to 300 mm (12 in.) and the detector(s) remains on the surface (some gauges may reverse this orientation); or in backscatter or backscatter/air-gap the source and detector(s) both remain on the surface.  
1.2.1 The density of the test sample in mass per unit volume is calculated by comparing the detected rate of gamma radiation with previously established calibration data.  
1.2.2 The dry density of the test sample is obtained by subtracting the water mass per unit volume from the test sample wet density (Section 11). Most gauges display this value directly.  
1.3 The gauge is calibrated to read the water mass per unit volume of soil or soil-aggregate. When divided by the density of water and then multiplied by 100, the water mass per unit volume is equivalent to the volumetric water content. The water mass per unit volume is determined by the thermalizing or slowing of fast neutrons by hydrogen, a component of water. The neutron source and the thermal neutron detector are both located at the surface of the material being tested. The water content most prevalent in engineering and construction activities is known as the gravimetric water content, w, and is the ratio of the mass of the water in pore spaces to the total mass of solids, expressed as a percentage.  
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ASTM D5334-22a(Test Method)
Standard Test Method for Determination of Thermal Conductivity of Soil and Rock by Thermal Needle Probe Procedure

SIGNIFICANCE AND USE
5.1 The thermal conductivity of intact soil specimens, reconstituted soil specimens, and rock specimens is used to analyze and design systems involving underground transmission lines, oil and gas pipelines, radioactive waste disposal, geothermal applications, and solar thermal storage facilities, among others. Measurements can be made on site (in situ), or samples can be tested in a lab environment.
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ASTM D5334-22(Test Method)
Standard Test Method for Determination of Thermal Conductivity of Soil and Rock by Thermal Needle Probe Procedure

SIGNIFICANCE AND USE
5.1 The thermal conductivity of intact soil specimens, reconstituted soil specimens, and rock specimens is used to analyze and design systems involving underground transmission lines, oil and gas pipelines, radioactive waste disposal, geothermal applications, and solar thermal storage facilities, among others. Measurements can be made on site (in situ), or samples can be tested in a lab environment.
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1.1 This test method presents a procedure for determining the thermal conductivity (λ) of soil and rock using a transient heat method. This test method is applicable for both intact specimens of soil and rock and reconstituted soil specimens, and is effective in the lab and in the field. This test method is most suitable for homogeneous materials, but can also give a representative average value for non-homogeneous materials.  
1.2 This test method is applicable to dry, unsaturated or saturated materials that can sustain a hole for the sensor. It is valid over temperatures ranging from 100°C, depending on the suitability of the thermal needle probe construction to temperature extremes. However, care must be taken to prevent significant error from: (1) redistribution of water due to thermal gradients resulting from heating of the needle probe; (2) redistribution of water due to hydraulic gradients (gravity drainage for high degrees of saturation or surface evaporation); (3) phase change of water in specimens with temperatures near 0°C or 100°C.  
1.3 Units—The values stated in SI units are to be regarded as the standard. No other units of measurements are included in this standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.  
1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.  
1.4.1 The procedures used to specify how data are collected/recorded or calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analytical methods for engineering design.
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ASTM D7380/D7380M-21(Test Method)
Standard Test Method for Soil Compaction Determination at Shallow Depths Using 2.3-kg [5-lbm] Dynamic Cone Penetrometer

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5.1 The test method is used to assess the compaction effort of compacted materials. The number of drops required to drive the cone a distance of 83 mm [3.25 in.] is used as a criterion to determine the pass or fail in terms of soil percent compaction.  
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5.4 There are other DCPs with different dimensions, hammer weights, cone sizes, and cone geometries. Different test methods exist for these devices (such as D6951) and the correlations of the 5-lbm DCP with soil percent compaction are unique to this device.  
5.5 The 5-lbm DCP is a simple device, capable of being handled and operated by a single operator in field conditions. It is typically used as Quality Control (QC) of layer-by-layer compaction by construction crew in roadway pavement, backfill compaction in confined cuts and trenches, and utility pavement restoration work.
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1.1 This test method covers the procedure for the determination of the number of drops required for a dynamic cone penetrometer with a 2.3-kg [5-lbm] drop hammer falling 508 mm [20 in.] to penetrate a certain depth in compacted backfill.  
1.2 The device is used in the compaction verification of fine- and coarse-grained soils, granular materials, and weak stabilized or modified material used in subgrade, base layers, and backfill compaction in confined cuts and trenches at shallow depth.  
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1.4 The method is dependent upon knowing the field water content and the user having performed calibration tests to determine cone penetration resistance of various compaction levels and water contents.  
1.5 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined. Within the text of this standard, SI units appear first followed by the inch-pound [or other non-SI] units in brackets. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.  
1.6 It is common practice in the engineering profession to concurrently use pounds to represent both a unit of mass [lbm] and a force [lbf]. This implicitly combines two separate systems of units; that is, the absolute system and the gravitational system. This standard has been written using the absolute system of units when dealing with the inch-pound system. In this system, the pound [lbf] represents a unit of force (weight). However, the use of balances or scales recording pounds of mass [lbm] or the reading of density in lbm/ft3 shall not be regarded as a nonconformance with this standard.  
1.7 All observed and calculated values shall conform to the guidelines for significant digits and rounding...

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ASTM D6467-21e1(Test Method)
Standard Test Method for Torsional Ring Shear Test to Determine Drained Residual Shear Strength of Fine-Grained Soils

SIGNIFICANCE AND USE
5.1 The ring shear test is suited to the relatively rapid determination of drained residual shear strength because of the short drainage path through the thin specimen, the constant cross-sectional area of the shear surface during shear, unlimited rotational displacement in one direction, and the capability of testing one specimen under different effective normal stresses to obtain clay particles that are oriented parallel to the direction of shear to obtain residual shear strength envelope.  
5.2 The apparatus allows a reconstituted specimen to be overconsolidated and presheared prior to drained shearing. Overconsolidation and preshearing of the reconstituted specimen significantly reduces the horizontal displacement required to reach a residual condition, and therefore, reduces soil extrusion, wall friction, and other problems (Stark and Eid, 1993)3. This simulates a preexisting shear surface along which the drained residual strength can be mobilized.  
5.3 The ring shear test specimen is annular so the angular displacement differs from the inner edge to the outer edge. At the residual condition, the shear strength is constant across the specimen so the difference in shear stress between the inner and outer edges of the specimen is negligible.
Note 1: Notwithstanding the statements on precision and bias contained in this test method: The precision of this test method is dependent on the competence of the personnel performing it and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent testing. Users of this test method are cautioned that compliance with Practice D3740 does not ensure reliable testing. Reliable testing depends on several factors; Practice D3740 provides a means of evaluating some of those factors.
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1.1 Fine-grained soils in this Test Method are restricted to soils containing no more than 15 % fine sand (100 % passing the 425 μm (No. 40) sieve and no more than 15 % retained on the 75 μm (No. 200) sieve).A Summary of Changes section appears at the end of this standard.  
1.2 This test method provides a procedure for performing a torsional ring shear test under a drained condition to determine the residual shear strength of fine-grained soils. This test method is performed by shearing a reconstituted, overconsolidated, presheared specimen at a controlled displacement rate until the constant drained shear resistance is established on a single shear surface determined by the configuration of the apparatus.  
1.3 In this test, the specimen rotates in one direction until the constant or residual shear resistance is established. The amount of rotation is converted to displacement using the average radius of the specimen and multiplying it by numbers of degrees traveled and 0.0174.  
1.4 An intact specimen or a specimen with a natural shear surface can be used for testing. However, obtaining a natural slip surface specimen, determining the direction of field shearing, and trimming and aligning the usually non-horizontal shear surface in the ring shear apparatus is difficult. As a result, this test method focuses on the use of a reconstituted specimen to determine the residual strength. An unlimited amount of continuous shear displacement can be achieved to obtain a residual strength condition in a ring shear device.  
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1.6 The selection of effective normal stresses and determination of the shear strength parameters for design analyses are the responsibility of the professional or office requesting the test. Generally, three or more effective normal s...

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ASTM D6467-21(Test Method)
Standard Test Method for Torsional Ring Shear Test to Determine Drained Residual Shear Strength of Fine-Grained Soils

SIGNIFICANCE AND USE
5.1 The ring shear test is suited to the relatively rapid determination of drained residual shear strength because of the short drainage path through the thin specimen, the constant cross-sectional area of the shear surface during shear, unlimited rotational displacement in one direction, and the capability of testing one specimen under different effective normal stresses to obtain clay particles that are oriented parallel to the direction of shear to obtain residual shear strength envelope.  
5.2 The apparatus allows a reconstituted specimen to be overconsolidated and presheared prior to drained shearing. Overconsolidation and preshearing of the reconstituted specimen significantly reduces the horizontal displacement required to reach a residual condition, and therefore, reduces soil extrusion, wall friction, and other problems (Stark and Eid, 1993)3. This simulates a preexisting shear surface along which the drained residual strength can be mobilized.  
5.3 The ring shear test specimen is annular so the angular displacement differs from the inner edge to the outer edge. At the residual condition, the shear strength is constant across the specimen so the difference in shear stress between the inner and outer edges of the specimen is negligible.
Note 1: Notwithstanding the statements on precision and bias contained in this test method: The precision of this test method is dependent on the competence of the personnel performing it and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent testing. Users of this test method are cautioned that compliance with Practice D3740 does not ensure reliable testing. Reliable testing depends on several factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 Fine-grained soils in this Test Method are restricted to soils containing no more than 15 % fine sand (100 % passing the 425 μm (No. 40) sieve and no more than 15 % retained on the 75 μm (No. 200) sieve).A Summary of Changes section appears at the end of this standard.  
1.2 This test method provides a procedure for performing a torsional ring shear test under a drained condition to determine the residual shear strength of fine-grained soils. This test method is performed by shearing a reconstituted, overconsolidated, presheared specimen at a controlled displacement rate until the constant drained shear resistance is established on a single shear surface determined by the configuration of the apparatus.  
1.3 In this test, the specimen rotates in one direction until the constant or residual shear resistance is established. The amount of rotation is converted to displacement using the average radius of the specimen and multiplying it by numbers of degrees traveled and 0.0174.  
1.4 An intact specimen or a specimen with a natural shear surface can be used for testing. However, obtaining a natural slip surface specimen, determining the direction of field shearing, and trimming and aligning the usually non-horizontal shear surface in the ring shear apparatus is difficult. As a result, this test method focuses on the use of a reconstituted specimen to determine the residual strength. An unlimited amount of continuous shear displacement can be achieved to obtain a residual strength condition in a ring shear device.  
1.5 A shear stress-displacement relationship may be obtained from this test method. However, a shear stress-strain relationship or any associated quantity, such as modulus, cannot be determined from this test method because the height of the shear zone unknown, so an accurate or representative shear strain cannot be determined.  
1.6 The selection of effective normal stresses and determination of the shear strength parameters for design analyses are the responsibility of the professional or office requesting the test. Generally, three or more effective normal s...

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ASTM
ASTM D7830/D7830M-14(2021)e1(Test Method)
Standard Test Method for In-Place Density (Unit Weight) and Water Content of Soil Using an Electromagnetic Soil Density Gauge

SIGNIFICANCE AND USE
5.1 The method described determines wet density and gravimetric water content by correlating complex impedance measurement data to an empirically developed model. The empirical model is generated by comparing the electrical properties of typical soils encountered in civil construction projects to their wet densities and gravimetric water contents determined by other accepted methods.  
5.2 The test method described is useful as a rapid, non-destructive technique for determining the in-place total density and gravimetric water content of soil and soil-aggregate mixtures and the determination of dry density.  
5.3 This method may be used for quality control and acceptance of compacted soil and soil-aggregate mixtures as used in construction and also for research and development. The non-destructive nature allows for repetitive measurements at a single test location and statistical analysis of the results.
Note 2: The quality of the result produced by this standard test method is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the requirements of Practice D3740 are generally considered capable of competent and objective sampling/testing/inspection, and the like. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluation some of those factors.
SCOPE
1.1 This test method covers the procedures for determining in-place properties of non-frozen, unbound soil and soil aggregate mixtures such as total density, gravimetric water content and relative compaction by measuring the intrinsic impedance of the compacted soil.  
1.1.1 The method and device described in this test method are intended for in-process quality control of earthwork projects. Site or material characterization is not an intended result.  
1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.2.1 The gravitational system of inch-pound units is used when dealing with inch-pound units. In this system, the pound (lbf) represents a unit of force (weight) while the unit for mass is slugs. The rationalized slug unit is not given in this standard.  
1.2.2 In the engineering profession, it is customary practice to use, interchangeably, units representing both mass and force, unless dynamic calculations are involved. This implicitly combines two separate systems of units, that is, the absolute system and the gravimetric system. It is undesirable to combine the use of two separate systems within a single standard. The use of balances or scales recording pounds of mass (lbm), or the recording of density in lbm/ft3 should not be regarded as nonconformance with this standard.  
1.3 All observed and calculated values shall conform to the Guide for Significant Digits and Rounding established in Practice D6026.  
1.3.1 The procedures used to specify how data is collected, recorded, and calculated in this standard are regarded as industry standard. In addition, they are representative of the significant digits that should generally be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or decrease the number of significant digits of reported data commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in the analysis methods for engineering design.  
1.4 This standard does not purport to address all of the safety concerns, if any,...

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ASTM D7928-21(Test Method)
Standard Test Method for Particle-Size Distribution (Gradation) of Fine-Grained Soils Using the Sedimentation (Hydrometer) Analysis

SIGNIFICANCE AND USE
5.1 Particle-size distribution (gradation) is a descriptive term referring to the proportions by dry mass of a soil distributed over specified particle-size ranges. The gradation curve generated using this method yields the distribution of silt and clay size fractions present in the soil based on size definitions, not mineralogy or Atterberg limit classification.  
5.2 Unless the sedimentation sample is representative of the entire sample, the sedimentation results must be combined with a sieve analysis to obtain the complete particle size distribution.  
5.3 The clay size fraction is material finer than 2 µm. The clay size fraction is used in combination with the Plasticity Index (Test Methods D4318) to compute the activity, which provides an indication of the mineralogy of the clay fraction.  
5.4 The gradation of the silt and clay size fractions is an important factor in determining the susceptibility of fine-grained soils to frost action.  
5.5 The gradation of a soil is an indicator of engineering properties such as hydraulic conductivity, compressibility, and shear strength. However, soil behavior for engineering and other purposes is dependent upon many factors, such as effective stress, mineral type, structure, plasticity, and geological origin, and cannot be based solely upon gradation.  
5.6 Some types of soil require special treatment in order to correctly determine the particle sizes. For example, chemical cementing agents can bond clay particles together and should be treated in an effort to remove the cementing agents when possible. Hydrogen peroxide and moderate heat can digest organics. Hydrochloric acid can remove carbonates by washing and Dithionite-Citrate-Bicarbonate extraction can be used to remove iron oxides. Leaching with test water can be used to reduce salt concentration. All of these treatments, however, add significant time and effort when performing the sedimentation test and are allowable but outside the scope of this test method. ...
SCOPE
1.1 This test method covers the quantitative determination of the distribution of particle sizes of the fine-grained portion of soils. The sedimentation by hydrometer method is used to determine the particle-size distribution (gradation) of the material that is finer than the No. 200 (75-µm) sieve and larger than about 0.2-µm. The test is performed on material passing the No. 10 (2.0-mm) or finer sieve and the results are presented as the mass percent finer of this fraction versus the log of the particle diameter.  
1.2 This method can be used to evaluate the fine-grained fraction of a soil with a wide range of particle sizes by combining the sedimentation results with results from a sieve analysis using D6913 to obtain the complete gradation curve. The method can also be used when there are no coarse-grained particles or when the gradation of the coarse-grained material is not required or not needed.
Note 1: The significant digits recorded in this test method preclude obtaining the grain size distribution of materials that do not contain a significant amount of fines. For example, clean sands will not yield detectable amounts of silt and clay sized particles, and therefore should not be tested with this method. The minimum amount of fines in the sedimentation specimen is 15 g.  
1.3 When combining the results of the sedimentation and sieve tests, the procedure for obtaining the material for the sedimentation analysis and calculations for combining the results will be provided by the more general test method, such as Test Methods D6913 (Note 2).
Note 2: Subcommittee D18.03 is currently developing a new test method “Test Method for Particle-Size Analysis of Soils Combining the Sieve and Sedimentation Techniques.”  
1.4 The terms “soil” and “material” are used interchangeably throughout the standard.  
1.5 The sedimentation analysis is based on the concept that larger particles will fall through a fluid faster than...

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ASTM D7928-21e1(Test Method)
Standard Test Method for Particle-Size Distribution (Gradation) of Fine-Grained Soils Using the Sedimentation (Hydrometer) Analysis

SIGNIFICANCE AND USE
5.1 Particle-size distribution (gradation) is a descriptive term referring to the proportions by dry mass of a soil distributed over specified particle-size ranges. The gradation curve generated using this method yields the distribution of silt and clay size fractions present in the soil based on size definitions, not mineralogy or Atterberg limit classification.  
5.2 Unless the sedimentation sample is representative of the entire sample, the sedimentation results must be combined with a sieve analysis to obtain the complete particle size distribution.  
5.3 The clay size fraction is material finer than 2 µm. The clay size fraction is used in combination with the Plasticity Index (Test Methods D4318) to compute the activity, which provides an indication of the mineralogy of the clay fraction.  
5.4 The gradation of the silt and clay size fractions is an important factor in determining the susceptibility of fine-grained soils to frost action.  
5.5 The gradation of a soil is an indicator of engineering properties such as hydraulic conductivity, compressibility, and shear strength. However, soil behavior for engineering and other purposes is dependent upon many factors, such as effective stress, mineral type, structure, plasticity, and geological origin, and cannot be based solely upon gradation.  
5.6 Some types of soil require special treatment in order to correctly determine the particle sizes. For example, chemical cementing agents can bond clay particles together and should be treated in an effort to remove the cementing agents when possible. Hydrogen peroxide and moderate heat can digest organics. Hydrochloric acid can remove carbonates by washing and Dithionite-Citrate-Bicarbonate extraction can be used to remove iron oxides. Leaching with test water can be used to reduce salt concentration. All of these treatments, however, add significant time and effort when performing the sedimentation test and are allowable but outside the scope of this test method. ...
SCOPE
1.1 This test method covers the quantitative determination of the distribution of particle sizes of the fine-grained portion of soils. The sedimentation by hydrometer method is used to determine the particle-size distribution (gradation) of the material that is finer than the No. 200 (75-µm) sieve and larger than about 0.2-µm. The test is performed on material passing the No. 10 (2.0-mm) or finer sieve and the results are presented as the mass percent finer of this fraction versus the log of the particle diameter.  
1.2 This method can be used to evaluate the fine-grained fraction of a soil with a wide range of particle sizes by combining the sedimentation results with results from a sieve analysis using D6913 to obtain the complete gradation curve. The method can also be used when there are no coarse-grained particles or when the gradation of the coarse-grained material is not required or not needed.
Note 1: The significant digits recorded in this test method preclude obtaining the grain size distribution of materials that do not contain a significant amount of fines. For example, clean sands will not yield detectable amounts of silt and clay sized particles, and therefore should not be tested with this method. The minimum amount of fines in the sedimentation specimen is 15 g.  
1.3 When combining the results of the sedimentation and sieve tests, the procedure for obtaining the material for the sedimentation analysis and calculations for combining the results will be provided by the more general test method, such as Test Methods D6913 (Note 2).
Note 2: Subcommittee D18.03 is currently developing a new test method “Test Method for Particle-Size Analysis of Soils Combining the Sieve and Sedimentation Techniques.”  
1.4 The terms “soil” and “material” are used interchangeably throughout the standard.  
1.5 The sedimentation analysis is based on the concept that larger particles will fall through a fluid faster than...

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