ASTM B417-00
(Test Method)Standard Test Method for Apparent Density of Non-Free-Flowing Metal Powders Using the Carney Funnel
Standard Test Method for Apparent Density of Non-Free-Flowing Metal Powders Using the Carney Funnel
SCOPE
1.1 This test method covers a procedure for determining the apparent density of non-free-flowing metal powders. It is designed for those metal powders that do not freely flow through the Hall flowmeter funnel.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation:B417–00
Standard Test Method for
Apparent Density of Non-Free-Flowing Metal Powders Using
the Carney Funnel
This standard is issued under the fixed designation B 417; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope The degree of correlation between the results of this test
method and the quality of powders in use will vary with each
1.1 This test method covers a procedure for determining the
particular application.
apparent density of non-free-flowing metal powders. It is
designed for those metal powders that do not freely flow
6. Apparatus
through the Hall flowmeter funnel.
6.1 Powder Funnel —A Carney funnel (Fig. 1).
1.2 This standard does not purport to address all of the
6.2 Density Cup —Acylindrical brass cup (Fig. 2) having a
safety concerns, if any, associated with its use. It is the
capacity of 25 cm .The actual cup volume shall be determined
responsibility of the user of this standard to establish appro-
according to Test Method B 873.
priate safety and health practices and determine the applica-
6.3 Stand—A stand (Fig. 1) to support the powder funnel
bility of regulatory limitations prior to use.
concentric with the density cup so that the bottom of the
2. Referenced Documents powder funnel is approximately 25 mm (1 in.) above the top of
the density cup when the apparatus is assembled as shown in
2.1 ASTM Standards:
Fig. 1.
B 215 Practices for Sampling Finished Lots of Metal Pow-
6.4 Base—A level, vibration-free base to support the pow-
ders
der flowmeter.
B 243 Terminology of Powder Metallurgy
6.5 Balance, having a capacity of at least 200 g and a
B 873 Test Method for Measuring the Volume of Apparent
sensitivity of 0.01 g.
Density Cup Used in Test Methods B 212, B 329, and
6.6 Wire, approximately 2.5 mm (0.10 in.) in diameter by
B 417
150 mm (6 in.) in length.
3. Terminology
7. Test Specimen
3.1 Definitions—Terms in Terminology B 243 are appli-
7.1 The test specimen shall consist of a volume of approxi-
cable to this test method.
mately 30 to 40 cm of metal powder obtained in accordance
4. Summary of Test Method with Practice B 215.
7.2 The test specimen shall be tested as sampled. Note,
4.1 A container of definite volume is filled with non-free-
however, that temperature, moisture, oils, stearic acid, stear-
flowing powder under controlled conditions. The mass of
ates, waxes, and so forth may alter the characteristics of the
powder per unit volume is determined and reported as apparent
powder.
density, Carney.
8. Procedure
5. Significance and Use
8.1 Weigh the empty density cup to the nearest 0.1 g or,
5.1 This test method provides a guide for evaluation of the
alternatively, place the empty density cup on the balance and
apparent density physical characteristic of powders. The den-
tare the balance to zero.
sity measured bears a relationship to the mass of powder that
8.2 Load the test specimen carefully into the flowmeter
will fill a fixed volume die cavity when parts are being made.
funnel and permit it to run into the density cup through the
discharge orifice. If necessary, it may be agitated or pushed by
This test method is under the jurisdiction of ASTM Committee B09 on Metal
use of the length of wire but take care to prevent the wire from
Powders and Metal Powder Productsand is the direct responsibility of Subcommit-
tee B09.02 on Base Metal Products.
Current edition approved Nov. 10, 20
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