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ASTM D7166-10

(Practice)

Standard Practice for Total Sulfur Analyzer Based On-line/At-line for Sulfur Content of Gaseous Fuels

Standard Practice for Total Sulfur Analyzer Based On-line/At-line for Sulfur Content of Gaseous Fuels

SIGNIFICANCE AND USE
On-line, at-line, in-line and other near-real time monitoring systems that measure fuel gas characteristics such as the total sulfur content are prevalent in the natural gas and fuel gas industries. The installation and operation of particular systems vary on the specific objectives, contractual obligations, process type, regulatory requirements, and internal performance requirements needed by the user. This protocol is intended to provide guidelines for standardized start-up procedures, operating procedures, and quality assurance practices for on-line, at-line, in-line and other near-real time total sulfur monitoring systems.
SCOPE
1.1 This practice is for the determination of total sulfur from volatile sulfur-containing compounds in high methane or hydrogen content gaseous fuels using on-line/at-line instrumentation.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Dec-2009
Technical Committee
D03 - Gaseous Fuels
Drafting Committee
D03.12 - On-Line/At-Line Analysis of Gaseous Fuels
Current Stage
Ref Project

Relations

Replaces
ASTM D7166-05 - Standard Practice for Total Sulfur Analyzer Based On-line/At-line for Sulfur Content of Gaseous Fuels
Effective Date
01-Jan-2010
Referred By
ASTM D7800/D7800M-23 - Standard Test Method for Determination of Elemental Sulfur in Natural Gas
Effective Date
01-Jan-2010
Referred By
ASTM D7493-22 - Standard Test Method for Online Measurement of Sulfur Compounds in Natural Gas and Gaseous Fuels by Gas Chromatograph and Electrochemical Detection
Effective Date
01-Jan-2010
Referred By
ASTM D7551-10(2015) - Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases and Natural Gas by Ultraviolet Fluorescence
Effective Date
01-Jan-2010
Referred By
ASTM D4084-23 - Standard Test Method for Analysis of Hydrogen Sulfide in Gaseous Fuels (Lead Acetate Reaction Rate Method)
Effective Date
01-Jan-2010

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ASTM D7166-10 - Standard Practice for Total Sulfur Analyzer Based On-line/At-line for Sulfur Content of Gaseous FuelsASTM D7166-10 - Standard Practice for Total Sulfur Analyzer Based On-line/At-line for Sulfur Content of Gaseous Fuels
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REDLINE ASTM D7166-10 - Standard Practice for Total Sulfur Analyzer Based On-line/At-line for Sulfur Content of Gaseous FuelsREDLINE ASTM D7166-10 - Standard Practice for Total Sulfur Analyzer Based On-line/At-line for Sulfur Content of Gaseous Fuels
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D7166 − 10
StandardPractice for
Total Sulfur Analyzer Based On-line/At-line for Sulfur
1
Content of Gaseous Fuels
This standard is issued under the fixed designation D7166; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
D5503Practice for Natural Gas Sample-Handling and Con-
1.1 Thispracticeisforthedeterminationoftotalsulfurfrom
ditioning Systems for Pipeline Instrumentation
volatile sulfur-containing compounds in high methane or
D5504TestMethodforDeterminationofSulfurCompounds
hydrogen content gaseous fuels using on-line/at-line instru-
in Natural Gas and Gaseous Fuels by Gas Chromatogra-
mentation.
phy and Chemiluminescence
1.2 The values stated in SI units are to be regarded as
D6122Practice for Validation of the Performance of Multi-
standard. No other units of measurement are included in this
variate Online,At-Line, and Laboratory Infrared Spectro-
standard.
photometer Based Analyzer Systems
1.3 This standard does not purport to address all of the D6299Practice for Applying Statistical Quality Assurance
safety concerns, if any, associated with its use. It is the
and Control Charting Techniques to Evaluate Analytical
responsibility of the user of this standard to establish appro- Measurement System Performance
priate safety and health practices and determine the applica-
D6621Practice for Performance Testing of ProcessAnalyz-
bility of regulatory limitations prior to use. ers for Aromatic Hydrocarbon Materials
D6667Test Method for Determination of Total Volatile
2. Referenced Documents
Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum
2
Gases by Ultraviolet Fluorescence
2.1 ASTM Standards:
D6920TestMethodforTotalSulfurinNaphthas,Distillates,
D1070Test Methods for Relative Density of Gaseous Fuels
Reformulated Gasolines, Diesels, Biodiesels, and Motor
D1072Test Method for Total Sulfur in Fuel Gases by
Fuels by Oxidative Combustion and Electrochemical De-
Combustion and Barium Chloride Titration
tection
D3246Test Method for Sulfur in Petroleum Gas by Oxida-
3
tive Microcoulometry 2.2 ISO Standards
ISO 7504Gas Analysis-Vocabulary
D3609Practice for Calibration Techniques Using Perme-
ation Tubes
3. Terminology
D3764PracticeforValidationofthePerformanceofProcess
Stream Analyzer Systems
3.1 Definitions:
D4298Guide for Intercomparing Permeation Tubes to Es-
3.1.1 at-line instrument—instrumentationrequiringoperator
tablish Traceability
interaction that samples gas directly from the pipeline.
D4468Test Method for Total Sulfur in Gaseous Fuels by
3.1.2 calibration gas mixture, n—a certified gas mixture
Hydrogenolysis and Rateometric Colorimetry
with known composition used for the calibration of a measur-
D5287Practice for Automatic Sampling of Gaseous Fuels
ing instrument or for the validation of a measurement or gas
D5453Test Method for Determination of Total Sulfur in
analytical method.
Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel
3.1.2.1 Discussion—Calibration Gas Mixtures are the ana-
logues of measurement standards in physical metrology (ref-
erence ISO 7504 paragraph 4.1).
1
This practice is under the jurisdiction of ASTM Committee D03 on Gaseous
Fuels and is the direct responsibility of Subcommittee D03.12 on On-Line/At-Line
3.1.3 continuous fuel monitor—instrument that samples gas
Analysis of Gaseous Fuels.
directly from the pipeline on a continuous or semi-continuous
Current edition approved Jan. 1, 2010. Published February 2010 Originally
basis.
approved in 2005. Last previous edition approved in 2005 as D7166–05. DOI:
10.1520/D7166-10.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
3
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Available from International Organization for Standardization (ISO), 1, ch. de
Standards volume information, refer to the standard’s Document Summary page on la Voie-Creuse, Case postale 56, CH-1211, Geneva 20, Switzerland, http://
the ASTM website. www.iso.ch.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D7166 − 10
3.1.4 direct sampling—sampling where there is no direct varyonthespecificobjectives,contractualobligations,process
connection between the medium to be sampled and the type, regulatory requirements, and internal performance re-
analytical unit. quirements needed by the user. This protocol is intended to
provide guidelines for standardized start-up procedures, oper-
3.1.5 in-line instrument—
...

This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately,ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D7166–05 Designation: D7166 – 10
Standard Practice for
Total Sulfur Analyzer Based On-line/At-line for Sulfur
1
Content of Gaseous Fuels
This standard is issued under the fixed designation D7166; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 Thispracticeisforthedeterminationoftotalsulfurfromvolatilesulfur-containingcompoundsinhighmethaneorhydrogen
content gaseous fuels using on-line/at-line instrumentation.
1.2The values stated in SI units are standard. Values stated in other units are for information only.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D1070 Test Methods for Relative Density of Gaseous Fuels
D1072 Test Method for Total Sulfur in Fuel Gases by Combustion and Barium Chloride Titration
D3246 Test Method for Sulfur in Petroleum Gas by Oxidative Microcoulometry
D3609 Practice for Calibration Techniques Using Permeation Tubes
D3764 Practice for Validation of the Performance of Process Stream Analyzer Systems
D4298 Guide for Intercomparing Permeation Tubes to Establish Traceability
D4468 Test Method for Total Sulfur in Gaseous Fuels by Hydrogenolysis and Rateometric Colorimetry
D5287 Practice for Automatic Sampling of Gaseous Fuels
D5453 Test Method for Determination ofTotal Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel,
and Engine Oil by Ultraviolet Fluorescence
D5503 Practice for Natural Gas Sample-Handling and Conditioning Systems for Pipeline Instrumentation
D5504 Test Method for Determination of Sulfur Compounds in Natural Gas and Gaseous Fuels by Gas Chromatography and
Chemiluminescence
D6122 PracticeforValidationofthePerformanceofMultivariateProcessInfraredSpectrophotometerBasedAnalyzerSystems
D6299 Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical
Measurement System Performance
D6621 Practice for Performance Testing of Process Analyzers for Aromatic Hydrocarbon Materials
D6667 Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by
Ultraviolet Fluorescence
D6920 Test Method forTotal Sulfur in Naphthas, Distillates, Reformulated Gasolines, Diesels, Biodiesels, and Motor Fuels by
Oxidative Combustion and Electrochemical Detection
3
2.2 ISO Standards
ISO 7504 Gas Analysis-Vocabulary
3. Terminology
3.1 Definitions:
1
ThispracticeisunderthejurisdictionofASTMCommitteeD03onGaseousFuelsandisthedirectresponsibilityofSubcommitteeD03.12onOn-Line/At-LineAnalysis
of Gaseous Fuels.
Current edition approved June 15, 2005. Published June 2005. DOI: 10.1520/D7166-05.
Current edition approved Jan. 1, 2010. Published February 2010 Originally approved in 2005. Last previous edition approved in 2005 as D7166–05. DOI:
10.1520/D7166-10.
2
ForreferencedASTMstandards,visittheASTMwebsite,www.astm.org,orcontactASTMCustomerServiceatservice@astm.org.For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from International Organization for Standardization (ISO), 1, ch. de la Voie-Creuse, Case postale 56, CH-1211, Geneva 20, Switzerland, http://www.iso.ch.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D7166 – 10
3.1.1 at-line instrument—instrumentation requiring operator interaction that samples gas directly from the pipeline.
3.1.2 calibration gas mixture, n—a certified gas mixture with known composition used for the calibration of a measuring
instrument or for the validation of a measurement or gas analytical method.
3.1.2.1 Discussion—Calibration Gas Mixtures are the analogues of measurement standards in physical metrology (reference
ISO 7504 paragraph 4.1).
3.1.3 continuous fuel monitor—instrumentthatsamplesgasdirectlyfromthepipelineonacontinuousorsemi-continuousba
...

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Standard Specification for Nickel Alloy Billets and Bars for Reforging

ABSTRACT
This specification covers UNS N06002, UNS N06030, UNS N06035, UNS N06022, UNS N06200, UNS N06230, UNS N06600, UNS N06617, UNS N06625, UNS N08020, UNS N08026, UNS N08024, UNS N08120, UNS N08926, UNS N08367, UNS N10242, UNS N10276, UNS N10665, UNS N10675, UNS N12160, UNS R20033, UNS N06059, UNS N06686, UNS N10629, UNS N08031, UNS N06045, UNS N06025, and UNS R30556 nickel alloy billets and bars for reforging. The products shall be hot worked from ingots by rolling, forging, extruding, hammering, or pressing. The material shall conform to the chemical composition requirements prescribed by the reference material. The chemical composition of the material shall be determined by chemical analysis in accordance with test method E1473.
SCOPE
1.1 This specification covers UNS N06002, UNS N06030, UNS N06035, UNS N06022, UNS N06200, UNS N10362, UNS N06230, UNS N06600, UNS N06617, UNS N06625, UNS N08020, UNS N08026, UNS N08024, UNS N08120, UNS N08926, UNS N08367, UNS N10242, UNS N10276, UNS N10665, UNS N10675, UNS N12160, UNS R20033, UNS N06059, UNS N06686, UNS N10629, UNS N08031, UNS N06045, UNS N06025, UNS N06699, and UNS R305562 billets and bars for reforging.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to become familiar with all hazards including those identified in the appropriate Safety Data Sheet (SDS) for this product/material as provided by the manufacturer, to establish appropriate safety, health, and environmental practices, and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Technical specification
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  • Technical specification
    5 pages
    English language
    sale 15% off