Thermal insulation products for building equipment and industrial installations - Determination of thermal resistance by means of the guarded hot plate method - Part 1: Measurements at elevated temperatures from 100 °C to 850 °C

This document provides the additional information to that given in EN 12667, EN 12664, EN 12939 and ISO 8302 on the design of apparatus and operational procedures required to determine the thermal resistance of thermal insulation products in the temperature range 100 C to 850 C using the guarded hot plate method.

Wärmedämmstoffe für die Haustechnik und für betriebstechnische Anlagen - Bestimmung des Wärmedurchlasswiderstandes nach dem Verfahren mit dem Plattengerät - Teil 1: Messungen bei erhöhten Temperaturen von 100 °C bis 850 °C

Dieses Dokument stellt zusätzliche Informationen zu den in EN 12667, EN 12664, EN 12939 und ISO 8302 enthal¬tenen Angaben zur Konstruktion des Prüfgeräts und zu den Arbeitsabläufen zur Verfügung, die für die Bestim¬mung des Wärmedurchlasswiderstandes von Wärmedämmstoffen im Temperaturbereich von 100 °C bis 850 °C bei Anwendung des Verfahrens mit dem Plattengerät erforderlich sind.

Produits isolants thermiques pour les équipements de bâtiments et les installations industrielles - Détermination de la résistance thermique par la méthode de la plaque chaude gardée - Partie 1: Mesurages à haute témperature entre 100 °C et 850 °C

Le présent document fournit des informations supplémentaires par rapport à celles données dans l’EN 12667, l’EN 12664, l’EN 12939 et l’ISO 8302 sur la conception de l’appareillage et les modes opératoires de fonctionnement nécessaires pour déterminer la résistance thermique des produits isolants thermiques dans la plage de températures allant de 100 °C à 850 °C par la méthode de la plaque chaude gardée.

Toplotnoizolacijski proizvodi za opremo stavb in industrijske inštalacije - Ugotavljanje toplotne upornosti z zaščiteno vročo ploščo - 1. del: Meritve pri povišani temperaturi od 100 °C do 850 °C

Ta dokument vsebuje dodatne informacije za standarde EN 12667, EN 12664, EN 12939 in ISO 8302 o načrtovanju naprav in delovnih postopkov za ugotavljanje toplotne upornosti toplotnoizolacijskih proizvodov v temperaturnem območju od 100 °C do 850 °C z zaščiteno vročo ploščo.

General Information

Status
Withdrawn
Publication Date
29-Nov-2011
Withdrawal Date
05-Aug-2014
Current Stage
9960 - Withdrawal effective - Withdrawal
Completion Date
06-Aug-2014

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01-marec-2012
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Thermal insulation products for building equipment and industrial installations -
Determination of thermal resistance by means of the guarded hot plate method - Part 1:
Measurements at elevated temperatures from 100 °C to 850 °C
Wärmedämmstoffe für betriebstechnische Anlagen in der Industrie und in der
technischen Gebäudeausrüstung - Bestimmung des Wärmedurchlasswiderstandes nach
dem Verfahren mit dem Plattengerät - Teil 1: Messungen bei erhöhten Temperaturen
von 100 °C bis 850 °C
Produits isolants thermiques pour l’équipement du bâtiment et les installations
industrielles - Détermination de la résistance thermique par la méthode de la plaque
chaude gardée - Partie 1: Mesurages a températures élevées comprises entre 100 °C et
850 °C
Ta slovenski standard je istoveten z: CEN/TS 15548-1:2011
ICS:
91.100.60 0DWHULDOL]DWRSORWQRLQ Thermal and sound insulating
]YRþQRL]RODFLMR materials
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

TECHNICAL SPECIFICATION
CEN/TS 15548-1
SPÉCIFICATION TECHNIQUE
TECHNISCHE SPEZIFIKATION
November 2011
ICS 91.100.60
English Version
Thermal insulation products for building equipment and industrial
installations - Determination of thermal resistance by means of
the guarded hot plate method - Part 1: Measurements at
elevated temperatures from 100 °C to 850 °C
Produits isolants thermiques pour les équipements de
Wärmedämmstoffe für die Haustechnik und für
bâtiments et les installations industrielles - Détermination betriebstechnische Anlagen - Bestimmung des
de la résistance thermique par la méthode de la plaque Wärmedurchlasswiderstandes nach dem Verfahren mit
chaude gardée - Partie 1 : Mesurages à haute témperature dem Plattengerät - Teil 1: Messungen bei erhöhten
entre 100 °C et 850 °C Temperaturen von 100 °C bis 850 °C
This Technical Specification (CEN/TS) was approved by CEN on 14 May 2011 for provisional application.

The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to submit their
comments, particularly on the question whether the CEN/TS can be converted into a European Standard.

CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS available
promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in parallel to the CEN/TS)
until the final decision about the possible conversion of the CEN/TS into an EN is reached.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland,
Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.

EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2011 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN/TS 15548-1:2011: E
worldwide for CEN national Members.

Contents Page
Foreword .3
Introduction .3
1 Scope .4
2 Normative references .4
3 Definitions, symbols and units .4
3.1 Terms and definitions .4
3.2 Symbols and units .5
4 Principle .5
4.1 Apparatus .5
4.2 Measuring the density of heat flow rate .6
4.3 Measuring the temperature difference .6
4.4 Deriving the thermal resistance or transfer factor .6
4.5 Computing thermal conductivity or thermal transmissivity .6
4.6 Apparatus limits .6
4.7 Specimen limits.6
5 Apparatus description and design requirement .6
5.1 General .6
5.2 Two specimen apparatus .7
5.3 Single specimen apparatus .7
5.4 Plates .7
5.5 Main heating unit . 10
5.6 Edge insulation and auxiliary guards . 11
5.7 Cold plates . 11
5.8 Thickness measurement system . 11
5.9 Accuracy and repeatability . 11
5.10 Error analysis and equipment performance checks . 11
6 Test specimen . 11
6.1 General . 11
6.2 Selection and size . 12
6.3 Specimen preparation . 12
7 Testing procedure. 13
7.1 General . 13
7.2 Conditioning . 13
7.3 Measurements . 13
8 Calculations and test report . 15
8.1 Density and mass changes . 15
8.2 Heat transfer properties . 16
9 Test report . 17
Annex A (normative) Limits for equipment performance and test conditions . 19
A.1 General . 19
A.2 Accuracy and repeatability, stability, uniformity . 19
A.3 Suggested apparatus sizes . 20
A.4 Equipment design requirements . 20
A.5 Acceptable specimen characteristics . 21
A.6 Acceptable testing conditions . 23

Foreword
This document (CEN/TS 15548-1:2011) has been prepared by Technical Committee CEN/TC 89 “Thermal
performance of buildings and building components”, the secretariat of which is held by SIS.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to announce this Technical Specification: Austria, Belgium, Bulgaria, Croatia, Cyprus,
Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy,
Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia,
Spain, Sweden, Switzerland and the United Kingdom.
Introduction
This technical specification is an interim solution to the need for a standard to complement EN 12667:2001 in
the approximate temperature range 100 °C to 850 °C.
The technical specification is chosen to publish the knowledge gained in the field of measuring thermal
conductivity at elevated temperature now, as the finalisation of a standard is a complex matter requiring
further investigations.
Among existing apparatus for steady state thermal testing, the guarded hot plate can be operated at selected
mean temperatures over the temperature range -100 °C to 850 °C. In general, these apparatus exist in three
forms covering roughly the following temperature ranges -100 °C to ambient, ambient to 100 °C and above
100 °C. However, it has been found that it is not possible to achieve the uncertainties of ± 2 % claimed as
achievable for the low and ambient temperature forms when using the high temperature version in accordance
with ISO 8302. More realistic figures adopting the method and procedures detailed in this document are ± 5 %
up to 450 °C and ± 7 % at temperatures above 450 °C.
Many issues are more difficult at high temperatures. There are design issues due to apparatus material
stability, the level of temperature measurement uncertainty is higher than at ambient temperatures and there
is also greater degradation in the performance of temperature sensors when operated at high temperatures,
requiring calibration checks to be more frequent. At high temperatures, it is more likely to get hot spots on a
plate due to non-uniformity of a heater; these could be near temperature sensors and give false readings. Any
air gaps will have greater heat flow across them due to radiation heat exchange and finally provisions for
specimen expansion or shrinkage are needed.
Due to the above considerations the following clauses of EN 12667:2001 have been expanded and detailed:
5 Apparatus
5.1 General
5.2.4 Heating Unit
5.2.5 Metering Area
5.2.6 Edge insulation and auxiliary guards
5.2.7 Cooling units
5.3.5 Accuracy and repeatability
6 Test specimens
6.2 Selection and size
7 Testing procedure
7.3.8 Settling time and measurement interval
Annex A
Annex B.2
1 Scope
This document provides the additional information to that given in EN 12667, EN 12664, EN 12939 and
ISO 8302 on the design of apparatus and operational procedures required to determine the thermal resistance
of thermal insulation products in the temperature range 100 °C to 850 °C using the guarded hot plate method.
2 Normative references
The following referenced documents are indispensable for the application of this document. For dated
references, only the edition cited applies. For undated references, the latest edition of the referenced
document (including any amendments) applies.
EN 1946-2, Thermal performance of building products and components – Specific criteria for the assessment
of laboratories measuring heat transfer properties – Part 2: Measurements by guarded hot plate method
EN 12664, Thermal performance of building materials and products – Determination of thermal resistance by
means of guarded hot plate and heat flow meter methods – Dry and moist p
...

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