EN 16294:2012
(Main)Petroleum products and fat and oil derivatives - Determination of phosphorus content in fatty acid methyl esters (FAME) - Optical emission spectral analysis with inductively coupled plasma (ICP OES)
Petroleum products and fat and oil derivatives - Determination of phosphorus content in fatty acid methyl esters (FAME) - Optical emission spectral analysis with inductively coupled plasma (ICP OES)
This European Standard specifies an inductively coupled plasma optical emission spectrometry (ICP OES) method for the determination of phosphorus content of Fatty Acid Methyl Esters (FAME) in the range of 2,5 mg/kg to 8,0 mg/kg.
WARNING - The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Mineralölprodukte und Erzeugnisse aus pflanzlichen und tierischen Fetten und Ölen - Bestimmung des Gehalts an Phosphor in Fettsäuremethylestern (FAME) - Direkte Bestimmung durch optische Emissionsspektralanalyse mit induktiv gekoppeltem Plasma (ICP OES)
Diese Europäische Norm legt ein Verfahren zur Bestimmung des Phosphorgehalts in Fettsäuremethylestern (FAME) im Bereich von 2,5 mg/kg bis 8,0 mg/kg mit Hilfe der optischen Emissionsspektrometrie mit induktiv gekoppeltem Plasma (ICP OES) fest. WARNUNG — Die Anwendung dieses Dokument kann den Einsatz gefährlicher Stoffe, Arbeitsgänge und Geräte mit sich bringen. Dieses Dokument gibt nicht vor, alle mit seiner Anwendung verbundenen Sicherheitsprobleme anzusprechen. Der Anwender dieses Dokuments ist dafür verantwortlich, vorher angemessene Maßnahmen in Hinblick auf Sicherheit und Gesundheit zu ergreifen und die Anwendbarkeit einschränkender Vorschriften zu ermitteln.
Produits pétroliers et produits dérivés des corps gras - Détermination de la teneur en phosphore des esters méthyliques d'acides gras (EMAG) - Méthode par spectrométrie d’émission atomique par plasma à couplage inductif (ICP OES)
La présente Norme Européenne spécifie une méthode pour la détermination de la teneur en phosphore des esters méthyliques d’acides gras (EMAG) par spectrométrie d’émission atomique par plasma à couplage inductif (ICP OES). Cette méthode est applicable à des teneurs en phosphore comprises entre 2,5 mg/kg et 8,0 mg/kg.
AVERTISSEMENT - L'utilisation de la présente Norme européenne peut impliquer l'intervention de produits, d'opérations et d'équipements à caractère dangereux. La présente Norme européenne n'est pas censée aborder tous les problèmes de sécurité concernés par son usage. Il est de la responsabilité de l'utilisateur de consulter et d'établir des règles de sécurité et d'hygiène appropriées et de déterminer l'applicabilité des restrictions réglementaires avant utilisation.
Naftni proizvodi in derivati maščob ter olj - Določevanje fosforja v metilnih estrih maščobnih kislin (FAME) - Optična emisijska spektrometrija z induktivno sklopljeno plazmo (ICP OES)
Ta evropski standard določa metodo optične emisijske spektrometrije z induktivno sklopljeno plazmo (ICP OES) za določevanje fosforja v metilnih estrih maščobnih kislin (FAME) v razponu od 2,5 mg/kg do 8,0 mg/kg.
General Information
Standards Content (Sample)
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.NWLYQRMineralölprodukte und Erzeugnisse aus pflanzlichen und tierischen Fetten und Ölen - Bestimmung des Gehalts an Phosphor in Fettsäuremethylestern (FAME) - Direkte Bestimmung durch optische Emissionsspektralanalyse mit induktiv gekoppeltem Plasma (ICP OES)Produits pétroliers et produits dérivés des corps gras - Détermination de la teneur en phosphore des esters méthyliques d'acides gras (EMAG) - Méthode par spectrométrie d'émission atomique à couplage inductif par plasma (ICP OES)Petroleum products and fat and oil derivatives - Determination of phosphorus content in fatty acid methyl esters (FAME) - Optical emission spectral analysis with inductively coupled plasma (ICP OES)75.160.20Liquid fuelsICS:Ta slovenski standard je istoveten z:EN 16294:2012SIST EN 16294:2013en,de01-februar-2013SIST EN 16294:2013SLOVENSKI
STANDARD
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 16294
November 2012 ICS 75.160.20 English Version
Petroleum products and fat and oil derivatives - Determination of phosphorus content in fatty acid methyl esters (FAME) - Optical emission spectral analysis with inductively coupled plasma (ICP OES)
Produits pétroliers et produits dérivés des corps gras - Détermination de la teneur en phosphore des esters méthyliques d'acides gras (EMAG) - Méthode par spectrométrie d'émission atomique par plasma
à couplage inductif (ICP OES)
Mineralölprodukte und Erzeugnisse aus pflanzlichen und tierischen Fetten und Ölen - Bestimmung des Gehalts an Phosphor in Fettsäuremethylestern (FAME) - Direkte Bestimmung durch optische Emissionsspektralanalyse mit induktiv gekoppeltem Plasma (ICP OES) This European Standard was approved by CEN on 13 October 2012.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2012 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 16294:2012: ESIST EN 16294:2013
4.4 Phosphorus intermediate solution (25 mg/kg).
Weigh 0,50 g ± 0,01 g of phosphorus standard solution (4.3) into a 50 ml bottle (5.2). Add kerosene (4.2) to 20,00 g ± 0,01 g. Each mass shall be weighed to the nearest 0,1 mg. SIST EN 16294:2013
Element Wavelength nm Phosphorus 177,499 (177,434) 178,287 (178,222) 213,618 214,914 Cobalt 238,892
Scandium 361,383
Yttrium 224,306 371,029 360,073
As the magnitude of the background signal highly depends on spectral structures caused by the sample nature and origin, only net intensities have to be recorded. To keep background noise as low as possible, signal and background shall be measured simultaneously. 6 Sampling Unless otherwise specified in the commodity specification, samples shall be taken as described in EN ISO 3170 or EN ISO 3171 and/or in accordance with the requirements of national standards or regulations for the sampling of the product under test. New or thoroughly cleaned sample bottles made of plastic material (HDPE (high-density polyethylene), FEP (fluorinated ethylene propylene), or P
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