Coil coated metals - Test methods - Part 1: Film thickness

This document specifies the procedures for determining the dry-film thickness of an organic coating on a metallic substrate (coil coating).
Five appropriate methods are given in this document:
a)   magnetic induction;
b)   eddy current;
c)   micrometer;
d)   optical;
e)   ruggedized optical interference.
The methods are applicable only to products with smooth and flat substrates, but the coating itself can be textured. In that case, for methods a) and b), the average of a series of readings will represent an average of the thickness of the organic coating, while method c) will give the maximum thickness, method d) can provide the minimum, maximum and average thickness, and e) will give the total thickness.
Non-destructive continuous-web methods on measurement of dry-film thickness are only applicable on method a).

Bandbeschichtete Metalle - Prüfverfahren - Teil 1: Schichtdicke

Dieses Dokument legt die Verfahren zum Bestimmen der Trockenschichtdicke einer organischen Beschichtung auf einem metallischen Substrat (Bandbeschichtung) fest.
Fünf geeignete Verfahren werden in diesem Dokument angegeben:
a)   Magnetoinduktion;
b)   Wirbelstrom;
c)   Messschraube;
d)   optisch;
e)   robuste optische Interferenz.
Die Verfahren sind nur auf Produkte mit glatten und ebenen Substraten anwendbar, die Beschichtung selbst kann aber strukturiert sein. In diesem Fall stellt bei den Verfahren a) und b) der Mittelwert einer Reihe von Messungen einen Durchschnittswert der Dicke der organischen Beschichtung dar, während Verfahren c) die größte Schichtdicke ergibt, mit Verfahren d) die kleinste, größte und durchschnittliche Schichtdicke ermittelt werden kann und Verfahren e) die Gesamtdicke ergibt.
Nicht zerstörende Verfahren zum Messen der Trockenschichtdicke für Endlosbahnen sind nur bei Verfahren a) anwendbar.

Tôles prélaquées - Méthodes d’essai - Partie 1 : Épaisseur du feuil

Le présent document spécifie les méthodes de détermination de l’épaisseur de feuil sec d’un revêtement organique sur un subjectile métallique (prélaquage en bandes continues).
Cinq méthodes adaptées sont décrites dans le présent document :
a)   induction magnétique ;
b)   courants de Foucault ;
c)   micromètre ;
d)   optique ;
e)   interférences optiques renforcées (ROI).
Ces méthodes s’appliquent seulement aux produits qui comprennent des subjectiles lisses et plats, le revêtement lui même pouvant être texturé. Dans ce cas, pour les méthodes a) et b), la moyenne d’une série de lectures représentera une moyenne de l’épaisseur du revêtement organique, tandis que la méthode c) donnera l’épaisseur maximale, que la méthode d) peut fournir les épaisseurs minimales, maximales et moyennes, et que la technique e) fournira l’épaisseur totale.
Les méthodes non destructives sur toiles continues visant à déterminer l’épaisseur de feuil sec s’appliquent uniquement à la méthode a).

Prevlečene kovine, ki se navijajo - Preskusne metode - 1. del: Debelina premaza

Ta del skupine standardov EN 13523 določa postopke za ugotavljanje debeline suhega premaza organske prevleke na kovinski podlagi (prevlečene kovine, ki se navijajo).
V tem evropskem standardu so podane štiri ustrezne metode.
a)   magnetna indukcija;
b)   vrtinčni tok;
c)   mikrometer;
d)   optična metoda.
Metode se uporabljajo samo za proizvode z gladko in ravno podlago, medtem ko je lahko prevleka teksturirana. V tem primeru bo za metodi a) in b) povprečje niza odčitkov odražalo povprečno debelino organske prevleke, metoda c) bo podala največjo debelino, metoda d) pa bo podala najmanjšo, največjo in povprečno debelino.
Ta dokument ne obravnava neporušitvenih metod z neprekinjeno mrežo za merjenje debeline suhega premaza (glej standard EN ISO 2808).

General Information

Status
Published
Publication Date
23-Apr-2024
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
24-Apr-2024
Due Date
06-Aug-2025
Completion Date
24-Apr-2024

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SLOVENSKI STANDARD
01-september-2024
Nadomešča:
SIST EN 13523-1:2017
Prevlečene kovine, ki se navijajo - Preskusne metode - 1. del: Debelina premaza
Coil coated metals - Test methods - Part 1: Film thickness
Bandbeschichtete Metalle - Prüfverfahren - Teil 1: Schichtdicke
Tôles prélaquées - Méthodes d'essai - Partie 1 : Épaisseur du revêtement
Ta slovenski standard je istoveten z: EN 13523-1:2024
ICS:
17.040.20 Lastnosti površin Properties of surfaces
25.220.60 Organske prevleke Organic coatings
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN 13523-1
EUROPEAN STANDARD
NORME EUROPÉENNE
April 2024
EUROPÄISCHE NORM
ICS 17.040.20; 25.220.60 Supersedes EN 13523-1:2017
English Version
Coil coated metals - Test methods - Part 1: Film thickness
Tôles prélaquées - Méthodes d'essai - Partie 1 : Bandbeschichtete Metalle - Prüfverfahren - Teil 1:
Épaisseur du feuil Schichtdicke
This European Standard was approved by CEN on 1 January 2024.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2024 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 13523-1:2024 E
worldwide for CEN national Members.

Contents Page
European foreword . 3
1 Scope . 5
2 Normative references . 5
3 Terms and definitions . 5
4 Principle . 6
4.1 Method A: Measurement on magnetic substrate – magnetic induction . 6
4.2 Method B: Measurement on a non-magnetic substrate – eddy current . 6
4.3 Method C: Measurement on all substrates – micrometer method . 6
4.4 Method D: Measurement on all substrates – optical method . 6
4.5 Method E: Measurement on all substrates – ruggedized optical interference (ROI) . 6
5 Apparatus and materials . 6
6 Sampling . 6
7 Test panels . 7
8 Procedure . 7
8.1 Calibration . 7
8.1.1 General. 7
8.1.2 Calibration standards . 7
8.2 Scale rating . 7
8.3 Measurement . 7
8.3.1 Ambient conditions . 7
8.3.2 Number of measurements . 7
8.3.3 Method A: Magnetic induction . 8
8.3.4 Method B: Eddy current . 8
8.3.5 Method C: Micrometer method . 8
8.3.6 Method D: Optical method . 9
8.3.7 Method E: Ruggedized optical interference (ROI) . 9
9 Expression of results . 10
10 Accuracy . 10
11 Test report . 10
Bibliography . 11

European foreword
This document (EN 13523-1:2024) has been prepared by Technical Committee CEN/TC 139 “Paints and
varnishes”, the secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by October 2024, and conflicting national standards shall
be withdrawn at the latest by October 2024.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN 13523-1:2017.
a) ruggedized optical interference (ROI) has been added as method E;
b) the text has been editorially revised and the normative references have been updated.
The EN 13523 series, Coil coated metals — Test methods, consists of the following parts:
— Part 0: General introduction
— Part 1: Film thickness
— Part 2: Gloss
— Part 3: Colour difference and metamerism — Instrumental comparison
— Part 4: Pencil hardness
— Part 5: Resistance to rapid deformation (impact test)
— Part 6: Adhesion after indentation (cupping test)
— Part 7: Resistance to cracking on bending (T-bend test)
— Part 8: Resistance to salt spray (fog)
— Part 9: Resistance to water immersion
— Part 10: Resistance to fluorescent UV radiation and water condensation
— Part 11: Resistance to solvents (rubbing test)
— Part 12: Resistance to scratching
— Part 13: Resistance to accelerated ageing by the use of heat
— Part 14: Chalking (Helmen method)
— Part 16: Resistance to abrasion
— Part 17: Adhesion of strippable films
— Part 18: Resistance to staining
— Part 19: Panel design and method of atmospheric exposure testing
— Part 20: Foam adhesion
— Part 21: Evaluation of outdoor exposed panels
— Part 22: Colour difference — Visual comparison
— Part 23: Resistance to humid atmospheres containing sulfur dioxide
— Part 24: Resistance to blocking and pressure marking
— Part 25: Resistance to humidity
— Part 26: Resistance to condensation of water
— Part 27: Resistance to humid poultice (Cataplasm test)
— Part 29: Resistance to environmental soiling (Dirt pick-up and striping)
Any feedback and questions on this document should be directed to the users’ national standards body.
A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organisations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia,
Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland,
Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of North
Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the United
Kingdom.
1 Scope
This document specifies the procedures for determining the dry-film thickness of an organic coating on
a metallic substrate (coil coating).
Five appropriate methods are given in this document:
a) magnetic induction;
b) eddy current;
c) micrometer;
d) optical;
e) ruggedized optical interference.
The methods are applicable only to products with smooth and flat substrates, but the coating itself can
be textured. In that case, for methods a) and b), the average of a series of readings will represent an
average of the thickness of the organic coating, while method c) will give the maximum thickness, method
d) can provide the minimum, maximum and average thickness, and e) will give the total thickness.
Non-destructive continuous-web methods on measurement of dry-film thickness are only applicable on
method a).
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
EN 13523-0:2021, Coil coated metals - Test methods - Part 0: General introduction
EN 23270, Paints and varnishes and their raw materials - Temperatures and humidities for conditioning
and testing (ISO 3270)
EN ISO 3611, Geometrical product specifications (GPS) - Dimensional measuring equipment - Design and
metrological characteristics of micrometers for external measurements (ISO 3611)
ASTM D8331, Standard Test Method for Measurement of Film Thickness of Thin-Film Coatings by Non-
Destructive Means Using Ruggedized Optical Interference
3 Terms and definitions
For the purposes of this document, the terms and definitions given in EN 13523-0 and the following apply.
ISO and IEC maintain terminology databases for use in standardization at the following addresses:
• IEC Electropedia: available at https://www.electropedia.org/
• ISO Online browsing platform: available at https://www.iso.org/obp
3.1
film thickness
distance between the surface of the film and the surface of the substrate
[SOURCE: EN ISO 2808:2019, 3.1]
4 Principle
4.1 Method A: Measurement on magnetic substrate – magnetic induction
The film thickness on a magnetic substrate is determined by means of an electromagnetic probe placed
on the coating and developing an electromagnetic field. The variation of this field is a function of the
distance between the probe and the substrate. This signal is measured and converted to the film thickness
reading.
4.2 Method B: Measurement on a non-magnetic substrate – eddy current
The film thickness on a non-magnetic conductive substrate is determined by means of an electromagnetic
probe placed on the coating and generating eddy currents in the substrate. The magnitude of the eddy
currents is a function of the distance between the probe and the substrate. This measuring signal is
derived from the impedance change in the probe and converted to the film thickness reading.
4.3 Method C: Measurement on all substrates – micrometer method
The film thickness is determined by measuring the coated sample and then removing the organic coating
and re-measuring the sample minus the coating or by measuring a film of organic coating that has been
removed from the sample.
4.4 Method D: Measurement on all substrates – optical method
The film thickness is determined by microscopical measurement of a section cut through the film. The
defined cut may be made in the coating using a special blade (symmetrical cut), a special paint borer
(conical bore) or a milling tool (sloping cut).
4.5 Method E: Measurement on all substrates – ruggedized optical interference (ROI)
The film thickness on a non-magnetic conductive substrate is determined by means of non-contact, ROI
technology which measures multi-layer coatings and thin film thicknesses down to sub-micron levels.
5 Apparatus and materials
5.1 Instruments for measuring film thickness, using the principles described in Clause 4.
5.2 Solvent, suitable for removing organic coatings, for example methyl ethyl ketone (2-butanone).
5.3 Suitable abrasive and/or blunt knife or other means of removing softened organic coatings that
do not damage the substrate.
5.4 Cutting tool, for Method D.
5.4.1 Blad
...

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