EN ISO 13000-2:1997

Plastics - Polytetrafluoroethylene (PTFE) semi-finished products - Part 2: Preparation of specimens and determination of properties (ISO 13000-2:1997)

Kunststoffe - Polytetrafluorethylen (PTFE)-Halbzeuge - Teil 2: Herstellung von Probekörpern und Bestimmung von Eigenschaften (ISO 13000-2:1997)

Dieser Teil der Internationalen Norm legt die Herstellung von Probekörpern und die Prüfverfahren für Halbzeuge aus Polytetrafluorethylen (PTFE) fest. Einzelne Prüfverfahren dieser vorliegende Norm können gefährliche Materi- alien, Arbeitsverfahren und Ausrüstungen beinhalten. Die Norm erhebt jedoch keinen  Anspruch auf Vollstädigkeit hinsichtlich der in diesem Zusammenhang eventuell auftretenden Sicherheitsfragen. Der Anwender der Norm trägt die Verantwortung für geeignete Sicherheitmassnahmen und für angemessene Vorkeh- rungen zum Schutze der Gesundheit.

Plastiques - Semi-produits en polytétrafluoroéthylène (PTFE)- Partie 2: Préparation des éprouvettes et détermination despropriétés (ISO 13000-2:1997)

Polimerni materiali – Polizdelki iz politetrafloroetilena (PTFE) – 2. del: Priprava preskušancev in določevanje lastnosti (ISO 13000-2:1997)

General Information

• Status: Withdrawn
• Publication Date: 14-Dec-1997
• Withdrawal Date: 14-Nov-2005
• ICS: 83.140.10 - Films and sheets
• Technical Committee: CEN/TC 249 - Plastics
• Drafting Committee: CEN/TC 249/SC 1/WG 11 - Fluoroplastics
• Current Stage: 9960 - Withdrawal effective - Withdrawal
• Start Date: 15-Nov-2005
• Completion Date: 15-Nov-2005
• Ref Project: SIST EN ISO 13000-2:1999 - Plastics - Polytetrafluoroethylene (PTFE) semi-finished products - Part 2: Preparation of specimens and determination of properties (ISO 13000-2:1997)

Relations

• Replaced By: EN ISO 13000-2:2005 - Plastics - Polytetrafluoroethylene (PTFE) semi-finished products - Part 2: Preparation of test specimens and determination of properties (ISO 13000-2:2005)
• Effective Date: 22-Dec-2008

Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN ISO 13000-2:1999
01-maj-1999
3ROLPHUQLPDWHULDOL±3ROL]GHONLL]SROLWHWUDIORURHWLOHQD37)(±GHO3ULSUDYD
SUHVNXãDQFHYLQGRORþHYDQMHODVWQRVWL,62
Plastics - Polytetrafluoroethylene (PTFE) semi-finished products - Part 2: Preparation of
specimens and determination of properties (ISO 13000-2:1997)
Kunststoffe - Polytetrafluorethylen (PTFE)-Halbzeuge - Teil 2: Herstellung von
Probekörpern und Bestimmung von Eigenschaften (ISO 13000-2:1997)
Plastiques - Semi-produits en polytétrafluoroéthylene (PTFE)- Partie 2: Préparation des
éprouvettes et détermination despropriétés (ISO 13000-2:1997)
Ta slovenski standard je istoveten z: EN ISO 13000-2:1997
ICS:
83.140.01 Izdelki iz gume in polimernih Rubber and plastics products
materialov na splošno in general
SIST EN ISO 13000-2:1999 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 13000-2:1999

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SIST EN ISO 13000-2:1999

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SIST EN ISO 13000-2:1999

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SIST EN ISO 13000-2:1999

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SIST EN ISO 13000-2:1999

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SIST EN ISO 13000-2:1999
INTERNATIONAL
13000-2
STANDARD
First edition
1997-12-15
Plastics - Polytetrafluoroethylene (PTFE)
semi-finished products -
Part 2:
Preparation of test specimens and
determination of properties
Plastiques - Semi-produits en polyt6trafluoro6thykne (PTFE) -
Partie 2: Prkparation des kprouvettes et dktermination des propri&s
Reference number
IS0 13000-2: 1997(E)

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SIST EN ISO 13000-2:1999
IS0 13000=2:1997(E)
CONTENTS
1
1. Scope . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
2. Normative references
2
3. Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
2
................................................................................................................................................
4.
S-PUi!
2
.........................................................................................................
5. Preparation of test specimens
2
......................................................................................
6 . Testing of semi-finished PTFE products
2
. .
61 General
3
6.2 .
Linear dimensions
3
. .
63 Tensile properties
7
6.4 Density .
7
65 . Loss of mass at 300 OC .
7
6.6 Dimensional stability - General method .
67 . Dimensional stability - Special method for determination of dimensional and
.............................................................................. 8
geometric stabilities of thick-walled tube
9
6.8 Electrical properties .
9
6.9 Hardness .
9
6.10 Colour . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .*.
10
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
6.11 Radiographic examination
10
6.12 Resistance to environmental stress cracking (ESC) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
10
6.13 Deformation under load . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Annex A (informative) Other standards relating to testing semi-finished products of
11
PTFE . . .*****.*.*.*.***************.***.
0 IS0 1997
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced
or utilized in any form or by any means, electronic or mechanical, including photocopying and
microfilm, without permission in writing from the publisher.
International Organization for Standardization
Case postale 56 l CH-1211 Geneve 20 l Switzerland
Internet central @I iso.ch
c=ch; a=400net; p=iso; o=isocs; s=central
x.400
Printed in Switzerland
ii

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SIST EN ISO 13000-2:1999
@ IS0 IS0 13000=2:1997(E)
Foreword
IS0 (the International Organization for Standardization) is a worldwide
federation of national standards bodies (IS0 member bodies). The work of
preparing International Standards is normally carried out through IS0
technical committees. Each member body interested in a subject for which
a technical committee has been established has the right to be represented
on that committee. International organizations, governmental and non-
governmental, in liaison with ISO, also take part in the work. IS0
collaborates closely with the International Electrotechnical Commission
(IEC) on all matters of electrotechnical standardization.
Draft International Standards adopted by the technical committees are
circulated to the member bodies for voting. Publication as an International
Standard requires approval by at least 75 % of the member bodies casting
a vote.
International Standard IS0 13000-2 was prepared by Technical Committee
ISOTTC 61, Plastics, Subcommittee SC 9, Thermoplastic materials.
IS0 13000 consists of the following parts, under the general title Plastics -
Polytetrafluoroethylene (PTFE) semi-finished products:
Par? I: Requirements and designation
Par? 2: Preparation of test specimens and determination of properties
Annex A of this part of IS0 13000 is for information only.
. . .
III

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SIST EN ISO 13000-2:1999
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SIST EN ISO 13000-2:1999
INTERNATIONAL STANDARD o Iso IS0 13000-2: 1997(E)
Plastics - Polytetrafluoroethylene (PTFE) semi-finished
products
Part 2:
Preparation of test specimens and determination of properties
WRING - This part of IS0 13000 may involve hazardous materials,
operations, and equipment. It does not purport to address all of the safety
It is the responsibility of the user of this
problems associated with its use.
part of IS0 13000 to establish appropriate safety and health practices and
determine the applicability of regulatory limitations prior to use.
1. Scope
This part of IS0 13000 specifies the preparation of test specimens and gives the test
methods for the requirements of semi-finished products of polytetrafluoroethylene
(PTFE).
2. Normative references
The following standards contain provisions which, through reference in this text,
constitute provisions of this International Standard. At the time of publication, the
editions indicated were valid. All standards are subject to revision, and parties to
agreements based on this International Standard are encouraged to investigate the
possibility of applying the most recent editions of the standards indicated below.
Members of IEC and IS0 maintain registers of currently valid International
Standards.
IS0 472: 1988 Plastics - Vocabulary.
IS0 527-1: 1993 Plastics - Determination of tensile properties - Part I: General principles.
IS0 527-2: 1993 Plastics - Determination of tensile properties - Part 2: Test conditions for
moulding and extrusion plastics.
IS0 527-3: 1995 Plastics - Determination of tensile properties - Part 3: Test conditions for
films and sheets.
IS0 842: 1984 Raw materials for paints and varnishes - Sampling.
-Determination of indentation hardness by means of a
IS0 868:1985 Plastics and ebonite
durometer (Shore hardness).
IS0 1183:1987 Plastics - Methods for determining the density and relative density of
non-cellular plastics.

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SIST EN ISO 13000-2:1999
IS0 13000=2:1997(E)
IS0 1923: 1981 Cellular plastics and rubbers - Determination of linear dimensions.
Part I: Ball indentation method.
IS0 2039-l: 1993 Plastics - Determination of hardness -
IS0 361.1: 1978 Micrometer callipers for external measurement.
-Determination of resistance to environmental stress cracking (ESC)
IS0 4599: 1986 Plastics
-Bent strip method.
Determination of environmental stress cracking (ESC) - Ball or pin impression
IS0 4600: 1992
method.
IS0 13000-l: 1997 Plastics - Polytetrafluoroethylene (PTFE) semi-jinishedproducts. Part 1.
Requirements and designation.
IEC 243- 1: 1988 A4ethods of test for electric strength of solid insulating materials - Part 1.
Tests at power@equencies.
Method of test for dielectric strength of solid insulating materials - Part 2.
IEC 243-2: 1990
Additional requirements for tests using direct voltage.
Test methods for Deformation of Plastics Under Load (Withdrawn - see
ASTM D621-64 (1988)
subclause 6.13 for details of availability).
ASTM D 1389-90 Methods for dielectric proof-voltage testing of thin solid electrical insulating
materials.
ASTM E94-93 Guide for radiographic testing.
CIE Publication 15.2: 1986, Calorimetry.
3. Definitions
The terminology given in IS0 472 and in IS0 13000-l is applicable to this part of IS0
13000.
4. Sampling
Details of procedures for sampling semi-finished products depend to a large extent on
the physical shape of the particular material. Whenever feasible, the materials shall
be sampled in accordance with IS0 842. Adequate statistical sampling shall be
considered an acceptable alternative.
5. Preparation of test specimens
The specimen used for testing shall be taken directly from or be machined from the
semi-finished product without other treatment. Thus, conversion of a semi-finished
product into a test specimen by any moulding procedure is not permitted. Where
In
applicable, IS0 standards shall be followed for the preparation of test specimens.
some instances, special procedures are required that are described either in the
general discussion or in the method.
Testing of semi-finished PTFE products
6.
6.1 General
Properties required for specification shall be determined according to the
International Standards as referenced in this part of IS0 13000 or the procedures in
this part of IS0 13000. For the determination of density, tensile properties, hardness,

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SIST EN ISO 13000-2:1999
IS0 13000=2:1997(E)
and electrical properties, condition the test specimens at 23 * 2 “C for a period of at
least 4 hours prior to test. The other tests require no conditioning.
Informative annex A provides a list of other standards relating to testing semi-
finished products of PTFE.
6.2 Linear dimensions
These shall be determined by the procedures provided in IS0 1923 for cellular
plastics.
6.3 Tensile properties
6.3.1 Tensile specimens
6.3.1.1 General
The appropriate type of test specimen shall be chosen from those given in 6.3.1.2
through 6.3.1.5. At least three test specimens shall be prepared from the sample and
three specimens shall be tested.
NOTE&--Test specimens prepared from the moulded basic shapes, rod, or tube
and conforming to 6.3.1.2 are likely to give similar results to test specimens
prepared from the same product but conforming to 6.3.1.3.
When testing extruded products, the test specimens shall be cut parallel to the axis of
extrusion so that, as far as possible, each test specimen represents a different section
along the axis and a different area of the cross section.
When testing skived tape, skived sheet, or skived film, the test specimens shall be cut
perpendicular to the direction in which the pressure was applied when moulding the
billet from which the product was skived. If this direction is not known, two sets of
test specimens shall be prepared and tested, the test specimens in one set being cut at
90° to those in the other set and the mean results shall be calculated from the higher
set of values (indicating, typically, the direction perpendicular to the axis of applied
pressure). This procedure ensures a uniform way to report results from the testing.
The micro tensile test specimen is used most commonly for PTFE products.
6.3.1.2 Turned dumb-bell test specimens
The test specimens shall be turned so that their dimensions are in the ratios given in
figure 1, with the shape shown in Figure 1. The value of the larger diameter (D) shall
be 7 t 0,5 mm, 10 t 0,5 mm, or 20 t 0,5 mm.

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SIST EN ISO 13000-2:1999
IS0 13000=2:1997(E)
Table of ratios for turned dumb-bell specimens
d = 0,45 D to 0,55 D
L=5Dto6D
I= 3 D to 3,5 D
R = 0,2 D to 0,3 D
Figure 1 - Turned dumb-bell specimen for tensile testing
6.3.1.3 Micro tensile die (Small punched dumb-bell) test specimens
The sample shall be machined to produce a sheet or disc of thickness 1,5 to 2,5 mm, or
turned to produce a rectangular sectioned ring which can be cut and flattened to give
such a sheet.
Test specimens conforming to the shape shown in Figure 2 and the dimensions given
in table 1 for the micro tensile die shall be punched from sheet or disc using a single
stroke press and the appropriate knife-edged die. In any one test specimen, the
thickness of the narrow parallel-sided portion shall nowhere deviate by more than two
percent from the mean. The sheet shall be supported, while the test specimens are
punched from it, on a slightly yielding material having a smooth surface (e. g. leather,
rubber, or high quality cardboard) on a flat rigid base. The cutting edge of the die
shall be sharp and free from notches or other visual defects. In the case of thin sheet
or skived tape of thickness from 0,125 mm to 3,0 mm, the test specimens shall be
punched from the material ‘as received ’.
Table 1 - Dimensions of dumb-bell test specimens
Micro tensile die Large dumb-bells
(Figure 3)
(Figure 2)
mm mm
115
A overall length, minimum 38
25+ 1
B width at ends, minimum 15
C length of narrow parallel-sided portion 12 t 0,5 33*2
portion 5 t 0,25 6 t 0,4
D width of narrow parallel-sided
14+ 1
E small radius 5 t 0,5
F large radius 25iz2
4

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SIST EN ISO 13000-2:1999
IS0 13000-2:1997(E)
Dimensions in millimetres
Rockwell C hardness 45 to 50
-4
A
2 75
Steel-rule die
(Inside dimensions for die are the sa
...