FprEN 13614

Bitumen and bituminous binders - Determination of adhesivity of bituminous emulsions by water immersion test

This document specifies a method for determining the adhesion of a bituminous emulsion coated onto aggregate when immersed in water.
The method considers two different aspects of adhesivity, i.e. immediate adhesivity and water effect on binder adhesion.
The method may be used with a reference aggregate. In that case, it measures the intrinsic adhesion behaviour of a bituminous emulsion. The method may also be used with a specific aggregate as used on a job site.
WARNING -The use of this document may involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this document to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

Bitumen und bitumenhaltige Bindemittel - Bestimmung des Haftverhaltens von Bitumenemulsionen bei Wasserlagerung

Dieses Dokument legt ein Verfahren zur Bestimmung der Haftung eines Bindemittelüberzuges aus Bitumenemulsion an Gesteinskörnung bei Wasserlagerung fest.
Das Verfahren berücksichtigt zwei verschiedene Aspekte des Haftverhaltens, d. h. das unmittelbare Haft-verhalten und die Wirkung von Wasser auf die Haftung des Bindemittels.
Das Verfahren kann mit einer Referenz-Gesteinskörnung angewendet werden. In diesem Falle misst es das eigentliche Haftungsverhalten einer Bitumenemulsion. Das Verfahren kann ebenso mit einer spezifischen Gesteinskörnung angewendet werden, wie sie auch auf einer Baustelle verwendet wird.
WARNUNG - Die Anwendung dieses Dokuments kann gefährliche Substanzen, Arbeitsgänge und Ausrüstung einschließen. In diesem Dokument werden nicht alle Sicherheitsprobleme angesprochen, die mit seiner Anwendung verbunden sind. Es liegt in der Verantwortung des Anwenders dieses Dokuments, geeignete Sicherheits- und Gesundheitsschutzmaßnahmen vorzusehen und vorher zu klären, ob einschränkende Vorschriften zu berücksichtigen sind.

Bitumes et liants bitumineux - Détermination de l'adhésivité des émulsions bitumineuses par l'essai d'immersion dans l'eau

Le présent document décrit une méthode permettant de déterminer les propriétés d’adhésion d’une émulsion bitumineuse bitume vis-à-vis de granulats, en immersion dans l’eau.
La méthode prend en compte deux aspects distincts de l'adhésivité, à savoir l'adhésivité immédiate et l'effet de l'eau sur l'adhésion du liant.
La méthode peut être mise en oeuvre avec un granulat de référence. Dans ce cas, elle mesure l’aptitude à l’adhésivité intrinsèque de l’émulsion bitumineuse. La méthode peut également être mise en oeuvre avec un granulat spécifique utilisé sur chantier.
AVERTISSEMENT- L'utilisation de ce document implique l'intervention de produits, d'opérations et d'équipements à caractère dangereux. Le présent document n'est pas censé aborder tous les problèmes de sécurité concernés par son usage. Il est de la responsabilité de l'utilisateur de ce document de consulter et d'établir des règles de sécurité et d'hygiène appropriées et de déterminer l'applicabilité des restrictions réglementaires avant utilisation.

Bitumen in bitumenska veziva - Določanje obstojnosti bitumenskega filma pod vodo TC: Bitumen in bitumenska veziva - Določanje adhezije bitumenskih emulzij s preskusom potapljanja v vodo

Standards Content (sample)

SLOVENSKI STANDARD
oSIST prEN 13614:2019
01-december-2019
Bitumen in bitumenska veziva - Določanje obstojnosti bitumenskega filma pod
vodo

Bitumen and bituminous binders - Determination of adhesivity of bituminous emulsions

by water immersion test
Bitumen und bitumenhaltige Bindemittel - Bestimmung des Haftverhaltens von
Bitumenemulsionen bei Wasserlagerung

Bitumes et liants bitumineux - Détermination de l'adhésivité des émulsions de bitume par

l'essai d'immersion dans l'eau
Ta slovenski standard je istoveten z: prEN 13614
ICS:
75.140 Voski, bitumni in drugi naftni Waxes, bituminous materials
proizvodi and other petroleum products
91.100.50 Veziva. Tesnilni materiali Binders. Sealing materials
oSIST prEN 13614:2019 en,fr,de

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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oSIST prEN 13614:2019
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oSIST prEN 13614:2019
DRAFT
EUROPEAN STANDARD
prEN 13614
NORME EUROPÉENNE
EUROPÄISCHE NORM
October 2019
ICS 75.140; 91.100.50 Will supersede EN 13614:2011
English Version
Bitumen and bituminous binders - Determination of
adhesivity of bituminous emulsions by water immersion
test

Bitumes et liants bitumineux - Détermination de Bitumen und bitumenhaltige Bindemittel -

l'adhésivité des émulsions de bitume par l'essai Bestimmung des Haftverhaltens von

d'immersion dans l'eau Bitumenemulsionen bei Wasserlagerung

This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee

CEN/TC 336.

If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations

which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.

This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other

language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC

Management Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,

Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and

United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are

aware and to provide supporting documentation.

Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without

notice and shall not be referred to as a European Standard.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels

© 2019 CEN All rights of exploitation in any form and by any means reserved Ref. No. prEN 13614:2019 E

worldwide for CEN national Members.
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oSIST prEN 13614:2019
prEN 13614:2019 (E)
Contents Page

European foreword ....................................................................................................................................................... 3

1 Scope .................................................................................................................................................................... 4

2 Normative references .................................................................................................................................... 4

3 Terms and definitions ................................................................................................................................... 4

4 Principle ............................................................................................................................................................. 5

5 Reagents and materials ................................................................................................................................. 5

6 Apparatus ........................................................................................................................................................... 5

7 Sampling ............................................................................................................................................................. 6

8 Procedure........................................................................................................................................................... 6

8.1 General ................................................................................................................................................................ 6

8.2 Determination of immediate adhesivity ................................................................................................. 6

8.3 Water effect on binder adhesion ............................................................................................................... 6

8.3.1 General ................................................................................................................................................................ 6

9 Expression of results ...................................................................................................................................... 7

10 Precision ............................................................................................................................................................. 7

11 Test report ......................................................................................................................................................... 8

Annex A (informative) Guidance for the marking of coated surface area ............................................... 9

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oSIST prEN 13614:2019
prEN 13614:2019 (E)
European foreword

This document (prEN 13614:2019) has been prepared by Technical Committee CEN/TC 336 “Bituminous

binders”, the secretariat of which is held by AFNOR.
This document is currently submitted to the CEN Enquiry.
This document will supersede EN 13614:2011.
The main changes with respect to the previous edition are listed below:

— curing and conditioning the coated aggregates within a Petri dish or crystallizer in the form of a single

layer instead of placing them into a beaker (8.2.4 and 8.3.5);

— making the assessment under water, which can be replaced if dirty, with the help of an appropriate

desk lamp (8.2.5 and 8.3.7);

— no requirements for a specific thermometer (6.9) since room temperature can be checked with

ordinary means. After drying, aggregates are to be left to cool down to room temperature before

starting the test procedure (8.1 and 8.3.1);

— acceptable tolerance on conditioning time (8.3.6) is reduced from ± 4 h to ± 2 h;

— guidance for the marking of covered surface area (Annex A) is improved by complementing the

sketches with actual pictures.
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oSIST prEN 13614:2019
prEN 13614:2019 (E)
1 Scope

This document specifies a method for determining the adhesion of a bituminous emulsion coated onto

aggregate when immersed in water.

The method considers two different aspects of adhesivity, i.e. immediate adhesivity and water effect on

binder adhesion.

The method may be used with a reference aggregate. In that case, it measures the intrinsic adhesion

behaviour of a bituminous emulsion. The method may also be used with a specific aggregate as used on a

job site.

WARNING — The use of this document may involve hazardous materials, operations and equipment.

This document does not purport to address all of the safety problems associated with its use. It is the

responsibility of the user of this document to establish appropriate safety and health practices and to

determine the applicability of regulatory limitations prior to use.
2 Normative references

The following documents are referred to in the text in such a way that some or all of their content

constitutes requirements of this document. For dated references, only the edition cited applies. For

undated references, the latest edition of the referenced document (including any amendments) applies.

EN 58, Bitumen and bituminous binders — Sampling bituminous binders
EN 12594, Bitumen and bituminous binders — Preparation of test samples

EN 13043, Aggregates for bituminous mixtures and surface treatments of roads, airfields and other

trafficked areas

EN 13808, Bitumen and bituminous binders — Framework for specifying cationic bituminous emulsions

EN ISO 3696, Water for analytical laboratory use — Specification and test methods (ISO 3696)

3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.

ISO and IEC maintain terminological databases for use in standardization at the following addresses:

— IEC Electropedia: available at http://www.electropedia.org/
— ISO Online browsing platform: available at http://www.iso.org/obp
3.1
adhesion

ability of a binder to coat the surface of an aggregate and to remain bonded over time in the presence of

water
3.2
adhesivity
qualitative assessment of the measurement of the adhesion
3.3
immediate adhesivity

qualitative assessment of the ability of the binder from a bituminous emulsion to resist the action of water

just after coating of the aggregate
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oSIST prEN 13614:2019
prEN 13614:2019 (E)
3.4
water effect on binder adhesion

qualitative assessment of the ability of the binder from a bituminous emulsion to resist

...