prEN 16987

Foodstuffs - Determination of acrylamide in coffee and coffee products by HPLC-MS/MS and GC-MS

This standard specifies methods for the determination of acrylamide in coffee and coffee products by extraction with water, clean-up by solid-phase extraction and determination by HPLC-MS/MS and GC-MS. It was validated in a method validation study on roasted coffee, soluble coffee, coffee substitutes and coffee products with ranges from 53 μg/kg to 612,1 μg/kg.

Lebensmittel - Bestimmung von Acrylamid in Kaffee und Kaffee-Erzeugnissen mit HPLC-MS/MS und GC-MS

Diese Norm legt Verfahren zur Bestimmung von Acrylamid in Kaffee und Kaffee-Erzeugnissen durch Extraktion mit Wasser, Aufreinigung mit Festphasenextraktion und Bestimmung mittels HPLC-MS/MS bzw. GC-MS fest. Es wurde in einem Ringversuch für Röstkaffee, löslichen Kaffee, Kaffeesurrogate und Kaffee-Erzeugnisse in Bereichen von 53 μg/kg bis 612,1 μg/kg validiert.

Produits alimentaires - Détermination de la teneur en acrylamide dans le café et les produits du café par CLHP-SM/SM et CG-SM

La présente norme spécifie des méthodes de détermination de la teneur en acrylamide dans le café et les produits du café par extraction à l’eau, puis purification par extraction en phase solide et détermination par CLHP-SM/SM et CG-SM. Elle a été validée lors d’une étude de validation de méthode sur le café torréfié, le café soluble, les succédanés de café et les produits du café dans des gammes allant de 53 μg/kg à 612,1 μg/kg.

Živila - Določevanje akrilamida v kavi in proizvodih iz kave s HPLC-MS/MS in GC-MS

General Information

• Status: Not Published
• Publication Date: 03-Dec-2017
• ICS: 67.140.20 - Coffee and coffee substitutes
• Technical Committee: CEN/TC 275 - Food analysis - Horizontal methods
• Drafting Committee: CEN/TC 275/WG 13 - Neoformed contaminants
• Current Stage: 4098 - Decision to abandon - Enquiry
• Completion Date: 05-Dec-2017
• Directive: 882/2004 - Regulation (EC) No 882/2004 of the European Parliament and of the Council of 29 April 2004 onofficial controls performed to ensure the verification of compliance with feed and food law, animal health and animal welfare rules
• Mandate: M/463 - Mandate for Standardisation addressed to CEN for the methods of analysis for food contaminants
• Ref Project: oSIST prEN 16987:2016 - Foodstuffs - Determination of acrylamide in coffee and coffee products by HPLC-MS/MS and GC-MS

Standards Content (Sample)

SLOVENSKI STANDARD
oSIST prEN 16987:2016
01-junij-2016
äLYLOD'RORþHYDQMHDNULODPLGDYNDYLLQSURL]YRGLKL]NDYHV+3/&0606LQ*&
06
Foodstuffs - Determination of acrylamide in coffee and coffee products by HPLC-MS/MS
and GC-MS
Lebensmittel - Bestimmung von Acrylamid in Kaffee und Kaffee-Erzeugnissen mit HPLC-
MS/MS und GC-MS
Produits alimentaires - Détermination de la teneur en acrylamide dans le café et les
produits du café par CLHP-SM/SM et CG-SM
Ta slovenski standard je istoveten z: prEN 16987
ICS:
67.140.20 Kava in kavni nadomestki Coffee and coffee substitutes
oSIST prEN 16987:2016 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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oSIST prEN 16987:2016

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oSIST prEN 16987:2016


DRAFT
EUROPEAN STANDARD
prEN 16987
NORME EUROPÉENNE

EUROPÄISCHE NORM

April 2016
ICS 67.140.20
English Version

Foodstuffs - Determination of acrylamide in coffee and
coffee products by HPLC-MS/MS and GC-MS
 Lebensmittel - Bestimmung von Acrylamid in Kaffee
und Kaffee-Erzeugnissen mit HPLC-MS/MS und GC-MS
This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee
CEN/TC 275.

If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations
which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.

This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other
language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC
Management Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.

Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without
notice and shall not be referred to as a European Standard.


EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2016 CEN All rights of exploitation in any form and by any means reserved Ref. No. prEN 16987:2016 E
worldwide for CEN national Members.

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oSIST prEN 16987:2016
prEN 16987:2016 (E)
Contents Page
Introduction . 3
European foreword . 3
1 Scope . 5
2 Normative references . 5
3 Principle . 5
4 Reagents . 5
5 Apparatus . 7
6 Procedure. 8
6.1 General . 8
6.2 Preparation of the sample extract . 8
6.3 Clean-up of the extracts . 8
6.3.1 Carrez p
...