Analysis of natural gas - Biomethane - Determination of the content of compressor oil (ISO 2615:2024)

This document gives general guidance for the sampling and gas chromatographic analysis of compressor oil in biomethane or compressed natural gas (CNG). The compressor oil mass fraction is determined by sampling on coalescing filters under defined operational conditions (the two first cubic meters of gas referring to standard conditions, delivered at a refuelling station).
Compressor oils are lubricants used in mechanical devices where the purpose is to reduce the volume and increase the pressure of gases for use in a variety of applications.
The method is solely applicable to compressed gas (p>18 MPa).
The compressor oil content is expressed as mass fraction. The scope of this method is from 3 mg/kg – 30 mg/kg.

Erdgas - Analyse von Biomethan - Bestimmung des Gehalts an Verdichterö (ISO 2615:2024)

Dieses Dokument enthält einen allgemeinen Leitfaden für die Probenahme und gaschromatographische Analyse von Verdichteröl in Biomethan oder komprimiertem Erdgas (CNG, en: compressed natural gas). Der Massenanteil des Verdichteröls wird durch Probenahme auf Koaleszenzfiltern unter festgelegten Betriebsbedingungen (die ersten beiden Kubikmeter Gas, die unter Standardbedingungen an einer Tankstelle abgegeben werden) bestimmt.
Verdichteröle sind Schmiermittel, die in mechanischen Geräten verwendet werden und deren Zweck es ist, das Volumen von Gasen zu reduzieren und deren Druck zu erhöhen, um sie für eine Vielzahl von Anwendungen zu nutzen.
Das Verfahren ist ausschließlich auf komprimiertes Gas (p > 18 MPa) anwendbar.
Der Gehalt an Verdichteröl wird als Massenanteil angegeben. Der Anwendungsbereich dieses Verfahrens liegt zwischen 3 mg/kg und 30 mg/kg.

Analyse du gaz naturel - Biométhane - Détermination de la teneur en huile de compresseur (ISO 2615:2024)

Le présent document fournit des recommandations générales relatives au prélèvement et à l'analyse par chromatographie en phase gazeuse de l'huile de compresseur présente dans le biométhane ou dans le gaz naturel comprimé (GNC). La fraction massique de l'huile de compresseur est déterminée par prélèvement sur des filtres coalescents dans des conditions d'exploitation définies (les deux premiers mètres cubes de gaz dans les conditions standard, fournis à une station de ravitaillement).
Les huiles de compresseur sont des lubrifiants utilisés dans les dispositifs mécaniques, dont le but est de réduire le volume et d'augmenter la pression des gaz pour une variété d'applications.
La méthode est uniquement applicable aux gaz comprimés (p>18 MPa).
La teneur en huile de compresseur est exprimée en tant que fraction massique. Le domaine d'application de la présente méthode est compris entre 3 mg/kg et 30 mg/kg.

Analiza zemeljskega plina - Biometan - Določanje vsebnosti kompresorskega olja (ISO 2615:2024)

General Information

Status
Published
Publication Date
07-May-2024
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
08-May-2024
Due Date
16-Oct-2024
Completion Date
08-May-2024

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SLOVENSKI STANDARD
01-julij-2024
Analiza zemeljskega plina - Biometan - Določanje vsebnosti kompresorskega olja
(ISO 2615:2024)
Analysis of natural gas - Biomethane - Determination of the content of compressor oil
(ISO 2615:2024)
Erdgas - Analyse von Biomethan - Bestimmung des Gehalts an Verdichterö (ISO
2615:2024)
Analyse du gaz naturel - Biométhane - Détermination de la teneur en huile de
compresseur (ISO 2615:2024)
Ta slovenski standard je istoveten z: EN ISO 2615:2024
ICS:
71.040.50 Fizikalnokemijske analitske Physicochemical methods of
metode analysis
75.060 Zemeljski plin Natural gas
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 2615
EUROPEAN STANDARD
NORME EUROPÉENNE
May 2024
EUROPÄISCHE NORM
ICS 75.060
English Version
Analysis of natural gas - Biomethane - Determination of
the content of compressor oil (ISO 2615:2024)
Analyse du gaz naturel - Biométhane - Détermination Erdgas - Analyse von Biomethan - Bestimmung des
de la teneur en huile de compresseur (ISO 2615:2024) Gehalts an Verdichterö (ISO 2615:2024)
This European Standard was approved by CEN on 15 April 2024.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2024 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 2615:2024 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
This document (EN ISO 2615:2024) has been prepared by Technical Committee ISO/TC 193 "Natural
gas" in collaboration with Technical Committee CEN/TC 408 “Natural gas and biomethane for use in
transport and biomethane for injection in the natural gas grid” the secretariat of which is held by
AFNOR.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by November 2024, and conflicting national standards
shall be withdrawn at the latest by November 2024.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document has been prepared under a standardization request addressed to CEN by the European
Commission. The Standing Committee of the EFTA States subsequently approves these requests for its
Member States.
Any feedback and questions on this document should be directed to the users’ national standards
body/national committee. A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the
United Kingdom.
Endorsement notice
The text of ISO 2615:2024 has been approved by CEN as EN ISO 2615:2024 without any modification.

International
Standard
ISO 2615
First edition
Analysis of natural gas —
2024-04
Biomethane — Determination of the
content of compressor oil
Analyse du gaz naturel — Biométhane — Détermination de la
teneur en huile de compresseur
Reference number
ISO 2615:2024(en) © ISO 2024
ISO 2615:2024(en)
© ISO 2024
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
ISO 2615:2024(en)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 2
5 Chemicals and materials . 2
5.1 Compressor oils .2
5.2 Solvent .3
5.3 Sampling filters .3
5.4 Backup filters .3
5.5 Calibration standards .3
5.6 Nitrogen pure gas .3
5.7 Compressed liquid propane .3
6 Apparatus . 3
6.1 Gas chromatograph .3
6.2 Capillary column .3
6.3 Ultrasonic bath .3
6.4 Pressurised fluid extraction apparatus .3
6.5 Filter housing .4
6.6 Rotary evaporator, concentration apparatus .4
6.7 Laboratory glassware .4
7 Sampling . 4
7.1 Sampling apparatus .4
7.2 Sampling steps .4
8 Methods to recover the oil from the buffer tank . 5
9 Extraction procedure for coalescing filters . 5
9.1 Procedure 1: Ultrasonic extraction – nitrogen flush .5
9.2 Procedure 2: Pressurised fluid extraction .5
10 Analysis . . 6
10.1 GC/MS analysis.6
10.2 GC/FID analysis .6
11 Calculations . 6
12 Test report . 7
Annex A (informative) Example of a GC/MS chromatogram obtained for a compressor oil
(Figure A.1) . 8
Annex B (informative) Example of a GC/FID chromatogram obtained for a compressor oil
(Figure B.1) . 9
Annex C (informative) Different types of oils .11
Bibliography .13

iii
ISO 2615:2024(en)
Foreword
ISO (the International Organi
...

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