Sludge, treated biowaste and soil - Determination of selected phthalates using capillary gas chromatography with mass spectrometric detection (GC-MS)

This Technical Specification specifies a method for the determination of selected phthalates in sludge, treated biowaste and soil, after extraction and gas chromatographic analysis with mass spectrometric detection.
The method is applicable for the determination of phthalates (see Table 2) at the lowest mass content of 0,1 mg/kg to 0,5 mg/kg (expressed as dry matter), depending on the individual substance.
The applicability of the method to other phthalates not specified in Table 2 is not excluded except the isomeric mixtures e.g. DiNP (Di-isononylphthalate), but shall be verified in each case.

Schlamm, behandelter Bioabfall und Boden - Bestimmung ausgewählter Phthalate mittels kapillarer Gaschromatographie mit massenspektrometrischer Detektion (GC-MS)

Diese Technische Spezifikation legt ein Verfahren zur Bestimmung ausgewählter Phthalate in Schlamm,
behandeltem Bioabfall und Boden nach Extraktion und gaschromatographischer Analyse mit
massenspektrometrischer Detektion fest.
Das Verfahren ist für die Bestimmung von Phthalaten (siehe Tabelle 2) mit einem Mindestmassengehalt von
0,1 mg/kg bis 0,5 mg/kg (angegeben als Trockenmasse), geeignet, abhängig von der jeweiligen Substanz.
Die Anwendbarkeit des Verfahrens auf weitere, in Tabelle 2 nicht angegebene Phthalate, ist bis auf die
Isomerengemische, wie z. B. DINP (Di-isononylphthalat), nicht ausgeschlossen, muss aber für jeden Fall
nachgewiesen werden.

Boues, biodéchets traités et sols - Détermination de certains phtalates par chromatographie en phase gazeuse capillaire avec détection par spectrométrie de masse (CG-SM)

La présente Spécification technique spécifie une méthode pour la détermination de certains phtalates dans
les boues, les biodéchets traités et les sols, après extraction et analyse par chromatographie en phase
gazeuse/spectrométrie de masse.
La méthode est applicable pour la détermination de phtalates (voir Tableau 2) à la plus faible teneur massique
de 0,1 mg/kg à 0,5 mg/kg (exprimée en teneur en matière sèche), selon la substance individuelle.
L'applicabilité de la méthode à d'autres phtalates non spécifiés dans le Tableau 2 n'est pas exclue, à
l'exception des mélanges isomériques tels que DiNP (Di-isononylphtalate), mais elle doit être vérifiée dans
chaque cas.

Blato, obdelani biološki odpadki in tla - Določevanje izbranih ftalatov s kapilarno plinsko kromatografijo z masno selektivno detekcijo (GC/MS)

Ta tehnična specifikacija opredeljuje metodo za določevanje izbranih ftalatov v blatu, obdelanih bioloških odpadkih in tleh po ekstrakciji in plinski kromatografiji z masno selektivno detekcijo. Ta metoda se uporablja za določevanje ftalatov (glejte preglednico 2) pri najnižji masni vsebnosti od 0,1 mg/kg do 0,5 mg/kg (izraženo kot suha snov), odvisno od posamezne snovi. Uporabnost metode pri drugih ftalatih, ki niso navedeni v preglednici 2, ni izključena, razen pri mešanicah izomerov, npr. DiNP (di-izononilftalat), vendar mora biti preverjena pri vsakem posameznem primeru.

General Information

Status
Published
Publication Date
21-Feb-2012
Current Stage
9060 - Closure of 2 Year Review Enquiry - Review Enquiry
Start Date
02-Dec-2020
Completion Date
02-Dec-2020

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST-TS CEN/TS 16183:2012
01-junij-2012
%ODWRREGHODQLELRORãNLRGSDGNLLQWOD'RORþHYDQMHL]EUDQLKIWDODWRYVNDSLODUQR
SOLQVNRNURPDWRJUDILMR]PDVQRVHOHNWLYQRGHWHNFLMR *&06
Sludge, treated biowaste and soil - Determination of selected phthalates using capillary
gas chromatography with mass spectrometric detection (GC-MS)
Schlamm, behandelter Bioabfall und Boden - Bestimmung ausgewählter Phthalate
mittels kapillarer Gaschromatographie mit massenspektrometrischer Detektion (GC-MS)
Boues, bio-déchets traités et sols - Détermination de certains phtalates par
chromatographie en phase gazeuse capillaire avec détection par spectrométrie de
masse (CG-SM)
Ta slovenski standard je istoveten z: CEN/TS 16183:2012
ICS:
13.030.20 7HNRþLRGSDGNL%ODWR Liquid wastes. Sludge
13.080.10 .HPLMVNH]QDþLOQRVWLWDO Chemical characteristics of
soils
SIST-TS CEN/TS 16183:2012 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------

SIST-TS CEN/TS 16183:2012

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SIST-TS CEN/TS 16183:2012


TECHNICAL SPECIFICATION
CEN/TS 16183

SPÉCIFICATION TECHNIQUE

TECHNISCHE SPEZIFIKATION
February 2012
ICS 13.030.01
English Version
Sludge, treated biowaste and soil - Determination of selected
phthalates using capillary gas chromatography with mass
spectrometric detection (GC-MS)
Boues, biodéchets traités et sols - Détermination de Schlamm, behandelter Bioabfall und Boden - Bestimmung
certains phtalates par chromatographie en phase gazeuse ausgewählter Phthalate mittels kapillarer
capillaire avec détection par spectrométrie de masse (CG- Gaschromatographie mit massenspektrometrischer
SM) Detektion (GC-MS)
This Technical Specification (CEN/TS) was approved by CEN on 24 April 2011 for provisional application.

The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to submit their
comments, particularly on the question whether the CEN/TS can be converted into a European Standard.

CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS available
promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in parallel to the CEN/TS)
until the final decision about the possible conversion of the CEN/TS into an EN is reached.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland,
Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2012 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN/TS 16183:2012: E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------

SIST-TS CEN/TS 16183:2012
CEN/TS 16183:2012 (E)
Contents Page
Foreword .3
Introduction .4
1 Scope .5
2 Normative references .5
3 Principle .6
4 Interferences .6
4.1 General .6
4.2 Interferences during sampling .6
4.3 Cross contamination .6
4.4 Interferences in gas chromatography .6
5 Reagents .
...

SLOVENSKI STANDARD
kSIST-TS FprCEN/TS 16183:2011
01-februar-2011
%ODWRREGHODQLELRORãNLRGSDGNLLQWOD'RORþHYDQMHL]EUDQLKIWDODWRYVNDSLODUQR
SOLQVNRNURPDWRJUDILMR]PDVQRVHOHNWLYQRGHWHNFLMR *&06
Sludge, treated biowaste and soil - Determination of selected phthalates using capillary
gas chromatography with mass spectrometric detection (GC-MS)
Schlamm, behandelter Bioabfall und Boden - Bestimmung ausgewählter Phthalate
mittels kapillarer Gaschromatographie mit massenspektrometrischer Detektion (GC-MS)
Boue, biodéchet traité et sol - Détermination de certains phtalates par chromatographie
en phase gazeuse/spectrométrie de masse (GC-MS)
Ta slovenski standard je istoveten z: FprCEN/TS 16183
ICS:
13.030.20 7HNRþLRGSDGNL%ODWR Liquid wastes. Sludge
kSIST-TS FprCEN/TS 16183:2011 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
kSIST-TS FprCEN/TS 16183:2011

---------------------- Page: 2 ----------------------
kSIST-TS FprCEN/TS 16183:2011


TECHNICAL SPECIFICATION
FINAL DRAFT
FprCEN/TS 16183
SPÉCIFICATION TECHNIQUE

TECHNISCHE SPEZIFIKATION

December 2010
ICS
English Version
Sludge, treated biowaste and soil - Determination of selected
phthalates using capillary gas chromatography with mass
spectrometric detection (GC-MS)
Boue, biodéchet traité et sol - Détermination de certains Schlamm, behandelter Bioabfall und Boden - Bestimmung
phtalates par chromatographie en phase ausgewählter Phthalate mittels kapillarer
gazeuse/spectrométrie de masse (GC-MS) Gaschromatographie mit massenspektrometrischer
Detektion (GC-MS)


This draft Technical Specification is submitted to CEN members for Technical Committee Approval. It has been drawn up by the Technical
Committee CEN/TC 400.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland,
Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.



Warning : This document is not a Technical Specification. It is distributed for review and comments. It is subject to change without notice
and shall not be referred to as a Technical Specification.


EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2010 CEN All rights of exploitation in any form and by any means reserved Ref. No. FprCEN/TS 16183:2010: E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
kSIST-TS FprCEN/TS 16183:2011
FprCEN/TS 16183:2010 (E)
Contents Page
Foreword .3
Introduction .4
1 Scope .5
2 Normative references .5
3 Principle .6
4 Interferences .6
4.1 General .6
4.2 Interferences during sampling .6
4.3 Cross contamination .6
4.4 Interferences in gas chromatography .6
5 Reagents .6
6 Apparatus .8
7 Sampling and sample storage . 10
8 Procedure .
...

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