Soil, treated biowaste and sludge - Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)

This draft European Standard specifies a method for quantitative determination of seven selected polychlorinated biphenyls (PCB28, PCB52, PCB101, PCB118, PCB138, PCB153 and PCB180) in sludge, treated biowaste and soil using GC-MS and GC-ECD (see Table 2).
(...)
The limit of detection depends on the determinants, the equipment used, the quality of chemicals used for the extraction of the sample and the clean-up of the extract.
Under the conditions specified in this European Standard, limit of application of 1 µg/kg (expressed as dry matter) can be achieved.
Sludge and treated biowaste may differ in properties and also in the expected contamination levels of PCBs and presence of interfering substances. These differences make it impossible to describe one general procedure. This European Standard contains decision tables based on the properties of the sample and the extraction and clean-up procedure to be used.

Boden, behandelter Bioabfall und Schlamm - Bestimmung von polychlorierten Biphenylen (PCB) mittels Gaschromatographie mit Massenspektrometrie-Kopplung (GC-MS) und Gaschromatographie mit Elektroneneinfangdetektion (GC-ECD)

Der vorliegende Europäische Norm Entwurf legt ein Verfahren für die quantitative Bestimmung von sieben ausgewählten polychlorierten Biphenylen (PCB 28, PCB 52, PCB 101, PCB 118, PCB 138, PCB 153 und PCB 180) in Schlamm, behandeltem Bioabfall und Boden unter Anwendung der GC MS und GC ECD fest (siehe Tabelle 2).
(...)
Die Nachweisgrenze hängt von den zu bestimmenden Substanzen, den verwendeten Geräten, der Qualität der für die Extraktion der Probe verwendeten Chemikalien und der Reinigung des Extrakts ab.
Unter den in dieser Europäischen Norm festgelegten Bedingungen kann eine Anwendungsgrenze von 1 µg/kg (angegeben als Trockenmasse) erreicht werden.
Schlamm und behandelter Bioabfall können sich in ihren Eigenschaften sowie in den erwarteten Kontaminationsniveaus von PCB und der Anwesenheit von störenden Substanzen unterscheiden. Aufgrund dieser Unterschiede ist es unmöglich, ein allgemeines Verfahren darzulegen. Die vorliegende Europäische Norm enthält Entscheidungstabellen, die auf den Probeneigenschaften und den anzuwendenden Extraktions  und Reinigungsverfahren basieren.

Sols, biodéchets traités et boues - Dosage des polychlorobiphényles (PCBs) par chromatographie en phase gazeuse-spectrométrie gazeuse couplée avec un détecteur de masse (CG-SM) ou un détecteur par capture d'électrons (CG-ECD)

La présente Norme européenne spécifie une méthode de dosage, par CG-SM et CG-ECD, de sept polychlorobiphényles choisis (PCB28, PCB52, PCB101, PCB118, PCB138, PCB153 et PCB180) dans les boues, les biodéchets traités et les sols (voir Tableau 2).
(...)
La limite de détection dépend des composés à analyser, de l’équipement utilisé, de la qualité des réactifs chimiques utilisés pour l’extraction de l’échantillon et la purification de l’extrait.
Dans les conditions spécifiées dans la présente Norme européenne, une limite d'application de 1 µg/kg (exprimée sur matière sèche) peut être atteinte.
Les boues et les biodéchets traités peuvent présenter des différences en termes de propriétés, de niveaux prévus de contamination par les PCBs et de présence de substances interférentes. En raison de ces différences, il est impossible de décrire un mode opératoire général. La présente Norme européenne contient des tables de décision basées sur les propriétés de l'échantillon ainsi que sur le mode opératoire d'extraction et de purification à utiliser.

Tla, obdelani biološki odpadki in blato - Določevanje polikloriranih bifenilov (PCB) s plinsko kromatografijo z masno selektivnim detektorjem (GC/MS) in s plinsko kromatografijo z detektorjem z zajetjem elektronov (GC/ECD)

Ta osnutek evropskega standarda določa metodo za kvantitativno določevanje sedmih izbranih polikloriranih bifenilov (PCB28, PCB52, PCB101, PCB118, PCB138, PCB153 in PCB180) v blatu, obdelanih bioloških odpadkih ter tleh z metodama GC-MS in GC-ECD (glej preglednico 2).
(...)
Meja detekcije je odvisna od determinant, uporabljene opreme, kakovosti kemikalij, uporabljenih za ekstrakcijo vzorca in očiščenje izvlečka.
Pod pogoji, določenimi v tem evropskem standardu, se lahko doseže meja uporabe 1 μg/kg (izraženo kot suha snov).
Blato in obdelani biološki odpadki se lahko razlikujejo glede lastnosti, predvidenih stopenj onesnaženja s polikloriranimi bifenili ter prisotnosti motečih snovi. Zaradi teh razlik ni možen opis enotnega splošnega postopka. Ta evropski standard vključuje tabele odločanja, ki temeljijo na lastnostih vzorca, ter postopek za ekstrakcijo in očiščenje, ki ga je treba uporabiti.

General Information

Status
Withdrawn
Publication Date
14-Aug-2018
Withdrawal Date
29-Jan-2019
Current Stage
9960 - Withdrawal effective - Withdrawal
Completion Date
30-Jan-2019

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN 16167:2018
01-december-2018
1DGRPHãþD
SIST EN 16167:2013
7ODREGHODQLELRORãNLRGSDGNLLQEODWR'RORþHYDQMHSROLNORULUDQLKELIHQLORY 3&%
VSOLQVNRNURPDWRJUDILMR]PDVQRVHOHNWLYQLPGHWHNWRUMHP *&06 LQVSOLQVNR
NURPDWRJUDILMR]GHWHNWRUMHP]]DMHWMHPHOHNWURQRY *&(&'
Soil, treated biowaste and sludge - Determination of polychlorinated biphenyls (PCB) by
gas chromatography with mass selective detection (GC-MS) and gas chromatography
with electron-capture detection (GC-ECD)
Boden, behandelter Bioabfall und Schlamm - Bestimmung von polychlorierten
Biphenylen (PCB) mittels Gaschromatographie mit Massenspektrometrie-Kopplung (GC-
MS) und Gaschromatographie mit Elektroneneinfangdetektion (GC-ECD)
Sols, biodéchets traités et boues - Dosage des polychlorobiphényles (PCBs) par
chromatographie en phase gazeuse-spectrométrie gazeuse couplée avec un détecteur
de masse (CG-SM) ou un détecteur par capture d'électrons (CG-ECD)
Ta slovenski standard je istoveten z: EN 16167:2018
ICS:
13.030.20 7HNRþLRGSDGNL%ODWR Liquid wastes. Sludge
13.080.10 .HPLMVNH]QDþLOQRVWLWDO Chemical characteristics of
soils
71.040.50 Fizikalnokemijske analitske Physicochemical methods of
metode analysis
SIST EN 16167:2018 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------

SIST EN 16167:2018

---------------------- Page: 2 ----------------------

SIST EN 16167:2018


EN 16167
EUROPEAN STANDARD

NORME EUROPÉENNE

August 2018
EUROPÄISCHE NORM
ICS 13.030.01; 13.080.10 Supersedes EN 16167:2012
English Version

Soil, treated biowaste and sludge - Determination of
polychlorinated biphenyls (PCB) by gas chromatography
with mass selective detection (GC-MS) and gas
chromatography with electron-capture detection (GC-
ECD)
Sols, biodéchets traités et boues - Dosage des Boden, behandelter Bioabfall und Schlamm -
polychlorobiphényles (PCBs) par chromatographie en Bestimmung von polychlorierten Biphenylen (PCB)
phase gazeuse-spectrométrie gazeuse couplée avec un mittels Gaschromatographie mit
détecteur de masse (CG-SM) ou un détecteur par Massenspektrometrie-Kopplung (GC-MS) und
capture d'électrons (CG-ECD) Gaschromatographie mit Elektroneneinfangdetektion
(GC-ECD)
This European Standard was approved by CEN on 20 March 2018.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2018 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 16167:2018 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------

SIST EN 16167:2018
EN 16167:2018 (E)
Contents Page
European foreword . 3
Introduction . 4
1 Scope . 5
2 Normative references . 5
3 Terms and definitions . 6
4 Principle . 7
5 Interferences .
...

SLOVENSKI STANDARD
oSIST prEN 16167:2017
01-december-2017
%ODWRREGHODQLELRORãNLRGSDGNLLQWOD'RORþHYDQMHSROLNORULUDQLKELIHQLORY 3&%
VSOLQVNRNURPDWRJUDILMR]PDVQRVHOHNWLYQLPGHWHNWRUMHP *&06 LQVSOLQVNR
NURPDWRJUDILMR]GHWHNWRUMHP]]DMHWMHPHOHNWURQRY *&(&'
Soil, treated biowaste and sludge - Determination of polychlorinated biphenyls (PCB) by
gas chromatography with mass selective detection (GC-MS) and gas chromatography
with electron-capture detection (GC-ECD)
Boden, behandelter Bioabfall und Schlamm - Bestimmung von polychlorierten
Biphenylen (PCB) mittels Gaschromatographie mit Massenspektrometrie-Kopplung (GC-
MS) und Gaschromatographie mit Elektroneneinfangdetektion (GC-ECD)
Sols, biodéchets traités et boues - Dosage des polychlorobiphényles (PCBs) par
chromatographie en phase gazeuse-spectrométrie gazeuse couplée avec un détecteur
de masse (CG-SM) ou un détecteur par capture d'électrons (CG-ECD)
Ta slovenski standard je istoveten z: prEN 16167
ICS:
13.030.20 7HNRþLRGSDGNL%ODWR Liquid wastes. Sludge
13.080.10 .HPLMVNH]QDþLOQRVWLWDO Chemical characteristics of
soils
oSIST prEN 16167:2017 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
oSIST prEN 16167:2017

---------------------- Page: 2 ----------------------
oSIST prEN 16167:2017


DRAFT
EUROPEAN STANDARD
prEN 16167
NORME EUROPÉENNE

EUROPÄISCHE NORM

October 2017
ICS 13.030.01; 13.080.10 Will supersede EN 16167:2012
English Version

Soil, treated biowaste and sludge - Determination of
polychlorinated biphenyls (PCB) by gas chromatography
with mass selective detection (GC-MS) and gas
chromatography with electron-capture detection (GC-
ECD)
 Schlamm, behandelter Bioabfall und Boden -
Bestimmung von polychlorierten Biphenylen (PCB)
mittels Gaschromatographie mit
massenspektrometrischer Detektion (GC-MS) und
Gaschromatographie mit Elektroneneinfangdetektion
(GC-ECD)
This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee
CEN/TC 444.

If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations
which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.

This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other
language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC
Management Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.

Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without
notice and shall not be referred to as a European Standard.


EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2017 CEN All rights of exploitation in any form and by any means reserved Ref. No. prEN 16167:2017 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
oSIST prEN 16167:2017
prEN 16167:2017 (E)
Contents Page
European foreword . 4
Introduction . 5
1 Scope . 6
2 Normative references . 6
3 Terms and definitions . 7
4 Principle . 8
5 Interferences
...

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