Liquid petroleum products - Unleaded petrol - Determination of benzene content by gas chromatography

This document specifies a column switching gas chromatographic method for the quantitative determination of benzene content in the range 0,05 % (V/V) to 6 % (V/V) in unleaded petrol having a final boiling point not greater than 220 °C.
The method described in this document is suitable for determining benzene in petrol, including petrol containing oxygenates up to E10 (up to 3,7 % (m/m) oxygen content), in line with the relevant EC Directives [1].
NOTE   For the purposes of this document, the terms "% (V/V)" and "% (m/m)" are used to represent respectively the volume fraction and the mass fraction.
WARNING - Use of this document might involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this document to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Flüssige Mineralölerzeugnisse - Unverbleiter Ottokraftstoff - Bestimmung des Benzolgehaltes mittels Gaschromatographie

Dieses Dokument legt ein gaschromatographisches Verfahren mit Säulenschaltung zur quantitativen Bestimmung des Benzolgehaltes im Bereich von 0,05 % (V/V) bis 6 % (V/V) in unverbleitem Ottokraftstoff, dessen Siedeende nicht höher ist als 220 °C, fest.
Das in diesem Dokument beschriebene Verfahren ist zur Bestimmung von Benzol in Ottokraftstoffen, einschließlich Ottokraftstoffen, die sauerstoffhaltige Verbindungen bis zu E10 (Sauerstoffgehalt bis zu 3,7 % (m/m)) enthalten, in Übereinstimmung mit den einschlägigen EG-Richtlinien [1] geeignet.
ANMERKUNG   Für die Zwecke dieses Dokuments wird zur Angabe des Volumenanteils einer Substanz der Ausdruck „% (V/V)“ und für den Massenanteil einer Substanz der Ausdruck "% (m/m)" verwendet.
WARNUNG - Die Anwendung dieses Dokuments kann die Anwendung gefährlicher Stoffe, Arbeitsgänge und Geräte mit sich bringen. Dieses Dokument beansprucht nicht, alle damit verbundenen Sicherheitsprobleme zu behandeln. Es liegt in der Verantwortung des Anwenders dieses Dokuments, vor der Anwendung geeignete Maßnahmen für die Sicherheit und den Gesundheitsschutz zu ergreifen, und die Geltung weiterer diesbezüglicher Auflagen zu prüfen.

Produits pétroliers liquides - Essence sans plomb - Détermination de la teneur en benzène par chromatographie en phase gazeuse

Le présent document spécifie une méthode de chromatographie en phase gazeuse à commutation de colonne pour la détermination quantitative de la teneur en benzène dans la plage de 0,05 % (V/V) à 6 % (V/V) dans l'essence sans plomb dont le point d'ébullition final n'est pas supérieur à 220 °C.
La méthode décrite dans ce document est adaptée à la détermination du benzène dans l'essence, y compris l'essence contenant des composés oxygénés jusqu'à E10 (jusqu'à 3,7 % (m/m) de teneur en oxygène), conformément aux directives CE pertinentes [1].
NOTE   Pour les besoins du présent document, les termes "% (V/V)" et "% (m/m)" sont utilisés pour représenter respectivement la fraction volumique et la fraction massique.
AVERTISSEMENT — L'utilisation de ce document peut impliquer des matériaux, des opérations et des équipements dangereux. Ce document n'a pas la prétention de traiter tous les problèmes de sécurité liés à son utilisation. Il incombe à l'utilisateur de ce document d'établir des pratiques appropriées en matière de sécurité et de santé et de déterminer l'applicabilité des restrictions réglementaires avant de l'utiliser.

Tekoči naftni proizvodi - Neosvinčeni motorni bencini - Določevanje benzena s plinsko kromatografijo

Ta evropski standard določa metodo plinske kromatografije s preklopom kolon za kvantitativno določevanje benzena v razponu od 0,05 % (V/V) do 10 % (V/V) v neosvinčenem motornem bencinu, katerega končno vrelišče ne presega 220 °C. Metoda, opisana v tem standardu, je primerna za določevanje benzena v motornem bencinu, vključno z bencinom, ki vsebuje kisikove spojine, v skladu z ustreznimi direktivami EU.
Opozorilo: Pri uporabi tega standarda so lahko prisotni nevarni materiali, postopki in oprema. Ta standard ne obravnava vseh varnostnih težav, ki se navezujejo na njegovo uporabo.

General Information

Status
Published
Publication Date
01-Nov-2022
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
02-Nov-2022
Due Date
03-Jan-2023
Completion Date
02-Nov-2022

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN 12177:2023
01-januar-2023
Nadomešča:
SIST EN 12177:1999
SIST EN 12177:1999/AC:2001
Tekoči naftni proizvodi - Neosvinčeni motorni bencini - Določevanje benzena s
plinsko kromatografijo
Liquid petroleum products - Unleaded petrol - Determination of benzene content by gas
chromatography
Flüssige Mineralölerzeugnisse - Unverbleite Ottokraftstoffe - Bestimmung des
Benzolgehaltes mittels Gaschromatographie
Produits pétroliers liquides - Essence sans plomb - Détermination de la teneur en
benzène par chromatographie en phase gazeuse
Ta slovenski standard je istoveten z: EN 12177:2022
ICS:
75.160.20 Tekoča goriva Liquid fuels
SIST EN 12177:2023 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
SIST EN 12177:2023

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SIST EN 12177:2023


EN 12177
EUROPEAN STANDARD

NORME EUROPÉENNE

November 2022
EUROPÄISCHE NORM
ICS 75.160.20 Supersedes EN 12177:1998
English Version

Liquid petroleum products - Unleaded petrol -
Determination of benzene content by gas chromatography
Produits pétroliers liquides - Essence sans plomb - Flüssige Mineralölerzeugnisse - Unverbleiter
Détermination de la teneur en benzène par Ottokraftstoff - Bestimmung des Benzolgehaltes mittels
chromatographie en phase gazeuse Gaschromatographie
This European Standard was approved by CEN on 16 October 2022.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2022 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 12177:2022 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
SIST EN 12177:2023
EN 12177:2022 (E)
Contents Page
European foreword . 3
1 Scope . 4
2 Normative references . 4
3 Terms and definitions . 4
4 Principle . 4
5 Reagents and materials . 5
6 Apparatus . 5
6.1 Gas chromatographic assembly . 5
7 Sampling . 6
8 Procedure . 7
8.1 Setup of the apparatus . 7
8.1.1 General. 7
8.1.2 Carrier gas .
...

SLOVENSKI STANDARD
oSIST prEN 12177:2022
01-januar-2022
Tekoči naftni proizvodi - Neosvinčeni motorni bencini - Določevanje benzena s
plinsko kromatografijo
Liquid petroleum products - Unleaded petrol - Determination of benzene content by gas
chromatography
Flüssige Mineralölerzeugnisse - Unverbleite Ottokraftstoffe - Bestimmung des
Benzolgehaltes mittels Gaschromatographie
Produits pétroliers liquides - Essence sans plomb - Détermination de la teneur en
benzène par chromatographie en phase gazeuse
Ta slovenski standard je istoveten z: prEN 12177
ICS:
75.160.20 Tekoča goriva Liquid fuels
oSIST prEN 12177:2022 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
oSIST prEN 12177:2022

---------------------- Page: 2 ----------------------
oSIST prEN 12177:2022


DRAFT
EUROPEAN STANDARD
prEN 12177
NORME EUROPÉENNE

EUROPÄISCHE NORM

January 2022
ICS 75.160.20 Will supersede EN 12177:1998
English Version

Liquid petroleum products - Unleaded petrol -
Determination of benzene content by gas chromatography
Produits pétroliers liquides - Essence sans plomb - Flüssige Mineralölerzeugnisse - Unverbleite
Détermination de la teneur en benzène par Ottokraftstoffe - Bestimmung des Benzolgehaltes
chromatographie en phase gazeuse mittels Gaschromatographie
This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee
CEN/TC 19.

If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations
which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.

This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other
language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC
Management Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.

Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without
notice and shall not be referred to as a European Standard.


EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2022 CEN All rights of exploitation in any form and by any means reserved Ref. No. prEN 12177:2022 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
oSIST prEN 12177:2022
prEN 12177:2022 (E)
Contents Page
European foreword . 3
1 Scope . 4
2 Normative references . 4
3 Terms and definitions . 4
4 Principle . 4
5 Reagents and materials . 5
6 Apparatus . 5
7 Sampling . 6
8 Procedure . 7
8.1 Setup of the apparatus . 7
8.1.1 General.
...

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