EN 15413:2011
(Main)Solid recovered fuels - Methods for the preparation of the test sample from the laboratory sample
Solid recovered fuels - Methods for the preparation of the test sample from the laboratory sample
This European Standard specifies the correct sequence of operations to ensure the representativity of the test
portions that have been taken according to the sampling plan, prior to physical and/or chemical analysis (e.g.
extractions, digestion and/or analytical determinations) of solid samples.
This European Standard specifies the correct sequence of operations and treatments to be applied to the
laboratory sample in order to obtain suitable test portions in compliance with the specific requirements defined
in the corresponding analytical procedures.
Feste Sekundärbrennstoffe - Verfahren zur Herstellung der Versuchprobe aus der Laboratoriumsprobe
Diese Europäische Norm legt die richtige Reihenfolge von Arbeitsschritten fest, damit die Repräsentativität
von nach dem Probenahmeplan entnommenen Prüfmengen vor der physikalischen und/oder chemischen
Analyse (z. B. Extraktionen, Aufschlüsse und/oder analytischen Bestimmungen) von Feststoffproben sichergestellt
wird.
Diese Europäische Norm legt die richtige Reihenfolge von Arbeitsschritten und Behandlungen fest, die auf die
Laboratoriumsproben anzuwenden sind, um geeignete Prüfmengen unter Beachtung der in den entsprechenden
Analysenverfahren festgelegten spezifischen Anforderungen zu erhalten.
Combustibles solides de récupération - Méthodes de préparation d'échantillons pour essai à partir d'échantillons pour laboratoire
La présente Norme européenne spécifie la succession correcte des opérations destinées à garantir la
représentativité des prises d'essai qui ont été prélevées conformément au plan d'échantillonnage, avant une
analyse physique et/ou chimique (par exemple, extractions, digestion et/ou déterminations analytiques)
d'échantillons solides.
La présente Norme européenne spécifie la succession correcte des opérations et des traitements à appliquer
à l'échantillon de laboratoire afin d’obtenir des prises d'essai appropriées conformément aux exigences
spécifiques définies dans les modes opératoires analytiques correspondants.
Trdna alternativna goriva - Metode za pripravo preskusnega vzorca iz laboratorijskega vzorca
Ta evropski standard določa pravilno zaporedje operacij za zagotavljanje reprezentativnosti preskusnih odmerkov, vzetih v skladu z načrtom vzorčenja, pred fizikalno in/ali kemijsko analizo (npr. ekstrakcijami, razklopom in/ali analitskimi določevanji) trdnih vzorcev. Ta tehnična specifikacije določa pravilno zaporedje operacij in obdelav, ki se uporabljajo na laboratorijskem vzorcu, da se pridobijo ustrezni preskusni odmerki v skladu s specifičnimi zahtevami, opredeljenimi v ustreznih analitskih postopkih.
General Information
Relations
Frequently Asked Questions
EN 15413:2011 is a standard published by the European Committee for Standardization (CEN). Its full title is "Solid recovered fuels - Methods for the preparation of the test sample from the laboratory sample". This standard covers: This European Standard specifies the correct sequence of operations to ensure the representativity of the test portions that have been taken according to the sampling plan, prior to physical and/or chemical analysis (e.g. extractions, digestion and/or analytical determinations) of solid samples. This European Standard specifies the correct sequence of operations and treatments to be applied to the laboratory sample in order to obtain suitable test portions in compliance with the specific requirements defined in the corresponding analytical procedures.
This European Standard specifies the correct sequence of operations to ensure the representativity of the test portions that have been taken according to the sampling plan, prior to physical and/or chemical analysis (e.g. extractions, digestion and/or analytical determinations) of solid samples. This European Standard specifies the correct sequence of operations and treatments to be applied to the laboratory sample in order to obtain suitable test portions in compliance with the specific requirements defined in the corresponding analytical procedures.
EN 15413:2011 is classified under the following ICS (International Classification for Standards) categories: 75.160.10 - Solid fuels; 75.160.40 - Biofuels. The ICS classification helps identify the subject area and facilitates finding related standards.
EN 15413:2011 has the following relationships with other standards: It is inter standard links to CEN/TS 15413:2006, EN ISO 21646:2022. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
EN 15413:2011 is associated with the following European legislation: Standardization Mandates: M/325. When a standard is cited in the Official Journal of the European Union, products manufactured in conformity with it benefit from a presumption of conformity with the essential requirements of the corresponding EU directive or regulation.
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Standards Content (Sample)
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Trdna alternativna goriva - Metode za pripravo preskusnega vzorca iz laboratorijskega vzorcaFeste Sekundärbrennstoffe - Verfahren zur Herstellung einer Prüfprobe aus einer LaborprobeCombustibles solides de récupération - Méthodes pour la préparation d'échantillons pour essai à partir d'échantillons pour laboratoireSolid recovered fuels - Methods for the preparation of the test sample from the laboratory sample75.160.10Trda gorivaSolid fuelsICS:Ta slovenski standard je istoveten z:EN 15413:2011SIST EN 15413:2011en,fr01-november-2011SIST EN 15413:2011SLOVENSKI
STANDARDSIST-TS CEN/TS 15413:20071DGRPHãþD
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 15413
September 2011 ICS 75.160.10 Supersedes CEN/TS 15413:2006English Version
Solid recovered fuels - Methods for the preparation of the test sample from the laboratory sample
Combustibles solides de récupération - Méthodes pour la préparation d'échantillons pour essai à partir d'échantillons pour laboratoire
Feste Sekundärbrennstoffe - Verfahren zur Herstellung der Versuchprobe aus der Laboratoriumsprobe This European Standard was approved by CEN on 15 July 2011.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2011 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 15413:2011: ESIST EN 15413:2011
Guideline for choosing sample treatment techniques. 11A.1General . 11A.2Homogenisation . 11A.3Fraction separation. 12A.4Drying . 13A.5Particle size reduction . 15A.6Sub-sampling . 17Annex B (informative)
Relationship between minimum amount of sample and particle size - Equation for the estimation of the minimum amount of sample . 19Annex C (informative)
Sample treatment equipment . 22Annex D (normative)
Guidelines - Characteristics of the laboratory sample for chemical analysis of SRF . 23Annex E (informative)
Results of ruggedness testing . 25E.1Abstract . 25E.2Preparation of samples and application of statistical formula . 25E.3Evaluation of influence of particle size reduction systems . 28E.4Conclusions . 34Bibliography . 36 SIST EN 15413:2011
This European Standard specifies the correct sequence of operations and treatments to be applied to the laboratory sample in order to obtain suitable test portions in compliance with the specific requirements defined in the corresponding analytical procedures. 2 Normative references The following referenced documents are indispensable for the application of this European Standard. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 15357:2011, Solid recovered fuels — Terminology, definitions and descriptions EN 15443, Solid recovered fuels — Methods for the preparation of the laboratory sample 3 Terms and definitions For the purposes of this document, the terms and definitions given in EN 15357:2011 and the following apply. 3.1 drying process of removing water from a sample NOTE For the purpose of test portion preparation, it may be useful to remove just the amount of water that could interfere with other processes involved (e.g. during crushing or milling). In order to minimise the alteration of the sample during test portion preparation, removing the total amount of water present in the sample is not necessarily needed. 3.2 fraction separation process of dividing components, particles or layers if homogenisation of the sample is practically not applicable and/or the analyses of different fractions or phases are appropriate 3.3 homogenisation process of combining of components, particles or layers into a more homogeneous state of the original samples (in the case of composite samples) or pre-treated fractions of samples in order to ensure equal distribution of substances in and properties of the sample 3.4 sub-sampling process of selecting one or more sub-samples from a sample 3.5 test portion; analytical portion quantity of material of proper size, for measurement of the concentration or other properties of interest, removed from the test sample NOTE The test portion may be taken from the laboratory sample directly if no preparation of sample is required (e.g. with liquids or samples of proper homogeneity, size and fineness), but usually it is taken from the prepared test sample. SIST EN 15413:2011
Figure 1 — Flow sheet - sequence of operations SIST EN 15413:2011
Guideline for choosing sample treatment techniques A.1 General The preparation of test samples from a laboratory sample will frequently involve a sequence of operations such as homogenisation, phase separation, drying, particle size reduction and sub-sampling. Specific forms of these operations are described in this annex. The sample treatment techniques prescribed in the analytical standards have to be fulfilled in any case. A.2 Homogenisation A.2.1 General information Before each operation that implies sub-sampling, a homogenisation step is required, in order to guarantee that all sub-samples or sample fractions have the same properties and composition. The homogenisation technique to be used is chosen depending on the properties of the sample. In many cases before homogenisation, particle size reduction may be necessary. A.2.2 Homogenisation techniques A.2.2.1 Manual homogenisation When to use it Generally usable; in cases when mechanical homogenisation could lead to loss of volatile compounds of interest (mercury). When not to use it For samples that form layers because of the presence of particles of different density; for samples with particles of such a large size that homogenisation by manual mixing cannot be reached; for samples that form layers because of the presence of particles with large differences in particle size. Procedure Mix the sample with an appropriate tool (e.g. shovel, pestle and mortar). If there is a risk of losses of volatile substances the manual homogenisation has to be done very carefully. A.2.2.2 Mechanical homogenisation When to use it Generally usable especially in cases when manual homogenisation is not suitable; SIST EN 15413:2011
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EN 15413:2011 is a European Standard that outlines the correct steps to ensure that test portions taken from a laboratory sample are representative. These test portions are used for physical and/or chemical analysis of solid samples. The standard also specifies the appropriate operations and treatments to be applied to the laboratory sample in order to obtain suitable test portions that meet the requirements outlined in the corresponding analytical procedures.
この記事は、EN 15413:2011という欧州標準について述べています。この標準は、固形廃棄物からの実験室のサンプルからテストサンプルを準備する方法についての指示を提供しています。この標準は、サンプリング計画に従って取られたテスト部分が、物理的および/または化学的な分析（例：抽出、消化、および/または分析決定）に適しているかどうかを確認するためのものです。該当する分析手順で定義された特定の要件を満たすために、実験室のサンプルに適用する必要のある正しい手順と処理方法を明示しています。
제목: EN 15413:2011 - 고형 연료로 회수된 물질 - 실험실 시료에서 실험시료를 생성하기 위한 방법 내용: 이 유럽 표준은 고형 시료의 물리 및/또는 화학 분석 (예: 추출, 소화 및/또는 분석 결정) 이전에 채취 계획에 따라 추출된 시험부분의 대표성을 보장하기 위해 수행해야 할 올바른 작업 순서를 명시합니다. 이 유럽 표준은 실험실 시료에 적용해야 할 올바른 작업 순서와 처리 방법을 명시하여 해당 분석 절차에 정의된 특정 요구 사항과 일치하는 적합한 시험부분을 얻기 위한 것입니다.
이 기사는 유럽 표준인 EN 15413:2011에 대해 다루고 있습니다. 이 표준은 고형 연료로부터 실험실 샘플로부터 시험 샘플을 준비하는 방법에 대한 지침을 제공합니다. 이 표준은 시험용 샘플에서 채취된 시험 부분이 대표성을 가지고 있는지 확인하여 물리적 및/또는 화학적 분석(예: 추출, 소화 및/또는 분석 결정)에 적합한지 보장합니다. 해당 표준은 분석 절차에 정의된 특정 요구 사항을 준수하기 위해 실험실 샘플에 적용해야 하는 올바른 순서의 작업 및 처리 방법을 명시합니다.
記事のタイトル: EN 15413:2011 - 固形化燃料 - 実験室サンプルから試験用サンプルの準備方法 記事内容: このヨーロッパ標準は、実験室サンプルから採取された試験部分が、物理的および/または化学的な分析（例: 抽出、消化、および/または分析決定）の前に、サンプリング計画に従って採取されたサンプルの代表性を確保するために行うべき正しい操作手順の順序を指定しています。 このヨーロッパ標準はさらに、対応する分析手順で定義された特定の要件に準拠した適切な試験部分を入手するために、実験室サンプルに適用する必要な操作や処理手順を指定しています。
The article discusses the European standard EN 15413:2011, which provides instructions for preparing test samples from laboratory samples of solid recovered fuels. The standard ensures that the test portions taken from the samples are representative and suitable for physical and chemical analysis. It outlines the correct sequence of operations and treatments to be applied to the laboratory sample to meet the requirements of specific analytical procedures.
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