EN 47:2016
(Main)Wood preservatives - Determination of the toxic values against larvae of Hylotrupes bajulus (Linnaeus) - (Laboratory method)
Wood preservatives - Determination of the toxic values against larvae of Hylotrupes bajulus (Linnaeus) - (Laboratory method)
This document specifies a method for the determination of the toxic values of a wood preservative against the larvae of Hylotrupes bajulus (Linnaeus), introduced into wood treated previously by full impregnation. This method is applicable to: ¾ water-insoluble chemicals which are being studied as active insecticides; ¾ organic formulations, as supplied or as prepared in the laboratory by dilution of concentrates; ¾ organic water-dispersible formulations as supplied or as prepared in the laboratory by dilution of concentrates; ¾ water-soluble materials, for example salts. The method is applicable whether or not the test specimens have been subjected to appropriate ageing procedures.
Holzschutzmittel - Bestimmung der Grenze der Wirksamkeit gegenüber Larven von Hylotrupes bajulus (Linnaeus) - (Laboratoriumsverfahren)
Diese Europäische Norm legt ein Verfahren zur Bestimmung der Grenze der Wirksamkeit eines Holzschutzmittels gegenüber Larven von Hylotrupes bajulus (Linnaeus) fest, die in Holz eingesetzt wurden, das zuvor durch Volltränkung behandelt wurde.
Das Verfahren gilt für:
- wasserunlösliche Chemikalien, die als wirksame Insektizide untersucht werden;
- organische Formulierungen im Anlieferungszustand oder in Form von im Laboratorium hergestellten Verdünnungen von Konzentraten;
- organische, in Wasser dispergierbare Formulierungen im Anlieferungszustand oder in Form von im Laboratorium hergestellten Verdünnungen von Konzentraten; und
- wasserlösliche Stoffe, zum Beispiel Salze.
Das Verfahren gilt unabhängig davon, ob die Proben einer angemessenen Alterungsbeanspruchung ausgesetzt wurden oder nicht.
Produits de préservation du bois - Détermination du seuil d'efficacité contre les larves d'Hylotrupes bajulus (Linnaeus) - (Méthode de laboratoire)
La norme européenne définit une méthode de détermination du seuil d’efficacité d'un produit de préservation du bois contre les larves d’Hylotrupes bajulus (Linnaeus) après leur introduction dans du bois traité préalablement par imprégnation totale.
La présente méthode est applicable :
- aux produits chimiques non hydrosolubles étudiés en tant que matières actives insecticides ;
- aux formules organiques telles qu'elles sont fournies ou préparées en laboratoire par dilution de concentrés ;
- aux formulations organiques hydrodispersables telles qu'elles sont fournies ou préparées en laboratoire par dilution de concentrés ; et,
- aux produits solubles dans l’eau, par exemple aux sels.
Cette méthode s’applique à des éprouvettes ayant subi ou non des épreuves de vieillissement appropriées.
Biocidni proizvodi za zaščito lesa - Ugotavljanje toksičnih vrednosti proti ličinkam hišnega kozlička Hylotrupes bajulus (Linnaeus) (laboratorijska metoda)
Ta dokument določa metodo za ugotavljanje toksičnih vrednosti biocidnega proizvoda za zaščito lesa proti ličinkam hišnega kozlička Hylotrupes bajulus (Linnaeus), uporabljenega na lesu, ki je bil obdelan s popolno impregnacijo. Ta metoda se uporablja za: ¾ v vodi netopne kemikalije, ki se preučujejo kot aktivni insekticidi; ¾ organske formulacije, ki so dobavljene ali pripravljene v laboratoriju z redčenjem koncentratov; ¾ organske formulacije, ki se razpršijo v vodi in so dobavljene ali pripravljene v laboratoriju z redčenjem koncentratov; ¾ v vodi topne materiale, na primer sol. Metoda se uporablja ne glede na to, ali so preskušanci izpostavljeni ustreznim postopkom staranja ali ne.
General Information
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Overview
EN 47:2016 - published by CEN - specifies a laboratory method to determine the toxic values of wood preservatives against larvae of Hylotrupes bajulus (Linnaeus) introduced into wood previously treated by full impregnation. The method applies to water‑insoluble chemicals, organic formulations (including water‑dispersible types), and water‑soluble materials (eg salts). Tests may be performed on specimens that have or have not undergone ageing procedures. EN 47:2016 supersedes EN 47:2005 and adds harmonized wood‑quality specifications.
Key topics and technical requirements
- Test principle: impregnate sets of susceptible wood specimens with a range of preservative concentrations, introduce Hylotrupes bajulus larvae, and determine survival rates at fixed intervals to derive toxic values.
- Biological material: two larval categories are defined - Category 1 (larvae ≤ 3 days after hatching) and Category 2 (larvae 50–150 mg). Guidance is given for sourcing, culturing and selecting healthy larvae (see Annex B).
- Wood specimens: reference species is Scots pine (Pinus sylvestris). Specimens are prepared to precise dimensions after conditioning: (50 ± 0.5) mm × (25 ± 0.5) mm × (15 ± 0.5) mm; nominal volume = 18.75 cm3. Wood quality rules (sapwood, growth rate, ring proportions) are specified.
- Test materials & apparatus: permitted solvents and water quality (EN ISO 3696), treatment vessels, vacuum impregnation equipment, conditioning and testing chambers with controlled temperature and relative humidity (eg conditioning chamber (20 ± 2) °C, RH 65 ± 5 %; culturing chamber (28 ± 2) °C, RH 70 ± 5 %), drill sizes for larval introduction and optional X‑ray radiography.
- Procedure & reporting: preparation of at least five test concentrations, control specimens (untreated and solvent/diluent controls), post‑treatment conditioning, larval introduction, observation and expression of results and full test reporting (Annex A example included).
- Safety: specific environmental, health and safety precautions are recommended (Annex D), particularly when handling highly active formulations or volatile solvents.
Applications and users
- Who uses EN 47:2016: product manufacturers, independent testing laboratories, research institutions, regulatory bodies, and specification writers assessing or demonstrating insecticidal efficacy of wood preservatives against Hylotrupes bajulus.
- Practical value: provides reproducible laboratory data for product development, comparative efficacy assessment, registration dossiers and quality control of preservative treatments for timber protection against wood‑boring larvae.
Related standards
- EN 46‑1 (surface treatment infestation tests) - method differs in application (surface treatment vs full impregnation).
- EN ISO 3696 - water for analytical laboratory use (referenced).
- EN 212 - sampling procedures (referenced).
- Replaces EN 47:2005 (superseded).
Keywords: EN 47:2016, wood preservatives, Hylotrupes bajulus, laboratory method, toxic values, wood preservative testing, impregnation, Scots pine, CEN.
Frequently Asked Questions
EN 47:2016 is a standard published by the European Committee for Standardization (CEN). Its full title is "Wood preservatives - Determination of the toxic values against larvae of Hylotrupes bajulus (Linnaeus) - (Laboratory method)". This standard covers: This document specifies a method for the determination of the toxic values of a wood preservative against the larvae of Hylotrupes bajulus (Linnaeus), introduced into wood treated previously by full impregnation. This method is applicable to: ¾ water-insoluble chemicals which are being studied as active insecticides; ¾ organic formulations, as supplied or as prepared in the laboratory by dilution of concentrates; ¾ organic water-dispersible formulations as supplied or as prepared in the laboratory by dilution of concentrates; ¾ water-soluble materials, for example salts. The method is applicable whether or not the test specimens have been subjected to appropriate ageing procedures.
This document specifies a method for the determination of the toxic values of a wood preservative against the larvae of Hylotrupes bajulus (Linnaeus), introduced into wood treated previously by full impregnation. This method is applicable to: ¾ water-insoluble chemicals which are being studied as active insecticides; ¾ organic formulations, as supplied or as prepared in the laboratory by dilution of concentrates; ¾ organic water-dispersible formulations as supplied or as prepared in the laboratory by dilution of concentrates; ¾ water-soluble materials, for example salts. The method is applicable whether or not the test specimens have been subjected to appropriate ageing procedures.
EN 47:2016 is classified under the following ICS (International Classification for Standards) categories: 71.100.50 - Wood-protecting chemicals. The ICS classification helps identify the subject area and facilitates finding related standards.
EN 47:2016 has the following relationships with other standards: It is inter standard links to EN 47:2005/AC:2007, EN 47:2005, prEN 47. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
You can purchase EN 47:2016 directly from iTeh Standards. The document is available in PDF format and is delivered instantly after payment. Add the standard to your cart and complete the secure checkout process. iTeh Standards is an authorized distributor of CEN standards.
Standards Content (Sample)
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.WRGDHolzschutzmittel - Bestimmung der Grenze der Wirksamkeit gegenüber Larven von Hylotrupes bajulus (Linnaeus) - (Laboratoriumsverfahren)Produits de préservation des bois - Détermination des valeurs toxiques contre les larves d'Hylotrupes bajulus (Linnaeus) - (Méthode de laboratoire)Wood preservatives - Determination of the toxic values against larvae of Hylotrupes bajulus (Linnaeus) - (Laboratory method)71.100.50Wood-protecting chemicalsICS:Ta slovenski standard je istoveten z:EN 47:2016SIST EN 47:2017en,fr,de01-januar-2017SIST EN 47:2017SLOVENSKI
STANDARDSIST EN 47:2005/AC:2007SIST EN 47:20051DGRPHãþD
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 47
August
t r s x ICS
y sä s r rä w r Supersedes EN
v yã t r r wEnglish Version
Wood preservatives æ Determination of the toxic values Produits de préservation du bois æ Détermination du seuil d 5efficacité contre les larves d 5Hylotrupes bajulus
Holzschutzmittel æ Bestimmung der Grenze der Wirksamkeit gegenüber Larven von Hylotrupes bajulus This European Standard was approved by CEN on
t January
t r s yä
egulations which stipulate the conditions for giving this European Standard the status of a national standard without any alterationä Upætoædate lists and bibliographical references concerning such national standards may be obtained on application to the CENæCENELEC Management Centre or to any CEN memberä
translation under the responsibility of a CEN member into its own language and notified to the CENæCENELEC Management Centre has the same status as the official versionsä
CEN members are the national standards bodies of Austriaá Belgiumá Bulgariaá Croatiaá Cyprusá Czech Republicá Denmarká Estoniaá Finlandá Former Yugoslav Republic of Macedoniaá Franceá Germanyá Greeceá Hungaryá Icelandá Irelandá Italyá Latviaá Lithuaniaá Luxembourgá Maltaá Netherlandsá Norwayá Polandá Portugalá Romaniaá Slovakiaá Sloveniaá Spainá Swedená Switzerlandá Turkey andUnited Kingdomä
EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre:
Avenue Marnix 17,
B-1000 Brussels
t r s x CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Membersä Refä Noä EN
v yã t r s x ESIST EN 47:2017
Example of a test report . 16 Annex B (informative)
Technique for culturing Hylotrupes bajulus (Linnaeus) . 18 Annex C (normative)
Differentiation of heartwood and sapwood in Pinus species . 21 Annex D (informative)
Environmental, health and safety precautions within chemical/biological laboratory . 22 Bibliography . 23
Untreated control test specimens 0 5 30 10 10 7 7 Solvent or diluent control test specimens (including water) 0 5 30 10 10 7 7 Total for 5 concentrations 35 210 70 70 49 49 a The use of radiography is only recommended in the case of tests with larvae in Category 2. 5.2 Products and reagents 5.2.1 Xylene, technical grade, mixed isomers. 5.2.2 Water, complying with grade 3 of EN ISO 3696. 5.2.3 Solvent or diluent, a volatile liquid that will dissolve or dilute the preservative but does not leave a residue in the wood at the end of the post-treatment conditioning period that has a toxic effect on the insects. CAUTION — Do not use benzene or other solvents which pose a health risk. 5.2.4 Cellulose or absorbent cotton wool and filter paper 5.3 Apparatus 5.3.1 Culturing chamber, with air circulation, and controlled at (28 ± 2) °C and at relative humidity (70 ± 5) %. 5.3.2 Conditioning chamber, well ventilated and controlled at (20 ± 2) °C and at relative humidity (65 ± 5) %. NOTE The conditioning of test specimens can be carried out in the laboratory work area (see 5.3.3) provided that this has the conditions specified for the conditioning chamber (see 5.3.2). 5.3.3 Laboratory work area, well ventilated, where treatment of the test specimens is carried out. SIST EN 47:2017
Protective gloves 6 Sampling The sample of preservative shall be representative of the product to be tested. Samples shall be stored and handled in accordance with any written recommendations from the supplier. For the sampling of preservatives from bulk supplies, the procedure given in EN 212 should be used.
1) 100 Pa = 1 mbar. SIST EN 47:2017
2) In southern European countries the species of pine most frequently infested by Hylotrupes bajulus may be used as an alternative, provided that the suitability of the species for use in the tests specified in this document has been demonstrated in all aspects (development of larvae, resistance to impregnation, etc.). SIST EN 47:2017
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The EN 47:2016 standard serves as a comprehensive guideline for the determination of toxic values of wood preservatives specifically against the larvae of *Hylotrupes bajulus* (Linnaeus). This standard outlines a laboratory method that is crucial for industry stakeholders involved in the development and testing of wood preservatives. Its extensive scope highlights its applicability to various formulations, including water-insoluble chemicals, organic formulations, organic water-dispersible formulations, and water-soluble materials, thereby ensuring versatility in testing methods. One of the key strengths of this standard is its meticulous approach to the examination of wood preservatives, providing clarity in the testing process. The inclusion of both ready-to-use formulations and those prepared through laboratory dilutions emphasizes its relevance for both manufacturers and researchers. This adaptability allows for a broad range of substances to be evaluated effectively, ensuring that the results are applicable across different product types. Moreover, the standard accommodates the use of test specimens whether or not they have undergone ageing procedures, which adds an additional layer of robustness to the testing method. This aspect ensures that it remains practical in real-world applications, as wood preservatives may be exposed to various environmental conditions over time. The EN 47:2016 standard is undeniably relevant in today's market, where the need for effective wood preservation methods is paramount due to increasing concerns over pest infestations that can compromise wood products. The focus on *Hylotrupes bajulus*, a significant pest affecting wood, underscores the urgency in assessing the effectiveness of wood preservatives. By providing a standardized approach, it enhances consistency in research and development efforts, ultimately contributing to the advancement of more effective wood treatment solutions. In summary, the EN 47:2016 standard presents a thorough and relevant framework for evaluating the toxic effects of wood preservatives, offering significant strengths through its flexible methodology and comprehensive scope. It serves as an essential tool for professionals aiming to ensure the efficacy and safety of wood preservation products against one of the most challenging wood pests.
EN 47:2016 표준은 Hylotrupes bajulus (Linnaeus)의 유충에 대한 목재 방부제의 독성 값을 결정하는 방법을 명시하고 있습니다. 이 문서의 범위는 방부제가 목재에 완전 침투된 상태에서 유충에 대한 독성 값을 정량화하는 방법으로, 이는 목재 보호 및 관리에 있어 중요한 기준이 됩니다. 이 표준의 강점 중 하나는 다양한 화학 물질에 적용 가능하다는 점입니다. 수용성 및 비수용성 화학 물질, 유기 제형 등 다양한 형태의 방부제를 시험할 수 있도록 설계되어 있어, 연구자와 제조업체가 특정 방부제의 효과를 보다 정확히 평가할 수 있게 합니다. 또한, 이 표준은 적절한 노화 절차를 거쳤는지 여부에 관계없이 시험할 수 있는 유연성을 제공함으로써, 실제 환경에서의 적용 가능성을 높이고 있습니다. EN 47:2016은 목재 방부제의 유효성을 평가하는 데 있어 필수적인 문서로, 환경과 인체에 대한 안전성을 고려함으로써 지속 가능한 목재 관리에 기여하고 있습니다. 이 표준은 방부제의 효과를 명확히 하고, 목재의 수명 연장을 위한 과학적 근거를 마련함으로써, 관련 분야에 필수적인 자료로 자리잡고 있습니다. 이러한 점에서 EN 47:2016은 목재 제조 및 보존 산업에서 매우 중요한 표준이라 할 수 있습니다.
SIST EN 47:2017は、Hylotrupes bajulus（リンネ）幼虫に対する木材防腐剤の毒性値を測定するための信頼性の高い標準化文書です。この標準の範囲は、木材にフルインプルス処理を施した後に導入された幼虫に対する防腐剤の毒性を評価する方法を特定しています。 この標準の強みは、様々なタイプの防腐剤を包括的に評価できる点です。水不溶性の化学物質や有機処方、さらに水溶性の材料、例えば塩も対象に含まれており、研究者や業界関係者にとって非常に有用です。また、試験標本が適切な経年劣化処理を受けたかどうかにかかわらず、方法が適用可能であるため、多様な条件下での試験が可能です。 この標準は、木材防腐剤の評価に必要不可欠であり、木材性能の向上と害虫対策に貢献します。そのため、SIST EN 47:2017は、木材に関わる業界において、品質管理や規制遵守のための重要な参考基準として位置付けられています。
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