EN ISO 11357-2:2020
(Main)Plastics - Differential scanning calorimetry (DSC) - Part 2: Determination of glass transition temperature and step height (ISO 11357-2:2020)
Plastics - Differential scanning calorimetry (DSC) - Part 2: Determination of glass transition temperature and step height (ISO 11357-2:2020)
This document specifies methods for the determination of the glass transition temperature and the step height related to the glass transition of amorphous and partially crystalline plastics.
Kunststoffe - Dynamische Differenz-Thermoanalyse (DSC) - Teil 2: Bestimmung der Glasübergangstemperatur und der Glasübergangsstufenhöhe (ISO 11357-2:2020)
Dieses Dokument legt Verfahren für die Bestimmung der Glasübergangstemperatur und der Glasübergangs¬stufenhöhe von amorphen und teilkristallinen Kunststoffen fest.
Plastiques - Analyse calorimétrique différentielle (DSC) - Partie 2: Détermination de la température et de la hauteur de palier de transition vitreuse (ISO 11357-2:2020)
Le présent document spécifie des méthodes permettant de déterminer la température de transition vitreuse et la hauteur de palier de transition vitreuse associées à la transition vitreuse des plastiques amorphes et partiellement cristallins.
Polimerni materiali - Diferenčna dinamična kalorimetrija (DSC) - 2. del: Ugotavljanje točke posteklenitve in višine prehoda (ISO 11357-2:2020)
General Information
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Standards Content (Sample)
SLOVENSKI STANDARD
01-junij-2020
Nadomešča:
SIST EN ISO 11357-2:2014
Polimerni materiali - Diferenčna dinamična kalorimetrija (DSC) - 2. del:
Ugotavljanje točke posteklenitve in višine prehoda (ISO 11357-2:2020)
Plastics - Differential scanning calorimetry (DSC) - Part 2: Determination of glass
transition temperature and step height (ISO 11357-2:2020)
Kunststoffe - Dynamische Differenz-Thermoanalyse (DSC) - Teil 2: Bestimmung der
Glasübergangstemperatur und der Glasübergangsstufenhöhe (ISO 11357-2:2020)
Plastiques - Analyse calorimétrique différentielle (DSC) - Partie 2: Détermination de la
température et de la hauteur de palier de transition vitreuse (ISO 11357-2:2020)
Ta slovenski standard je istoveten z: EN ISO 11357-2:2020
ICS:
17.200.10 Toplota. Kalorimetrija Heat. Calorimetry
83.080.01 Polimerni materiali na Plastics in general
splošno
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
EN ISO 11357-2
EUROPEAN STANDARD
NORME EUROPÉENNE
March 2020
EUROPÄISCHE NORM
ICS 83.080.01 Supersedes EN ISO 11357-2:2014
English Version
Plastics - Differential scanning calorimetry (DSC) - Part 2:
Determination of glass transition temperature and step
height (ISO 11357-2:2020)
Plastiques - Analyse calorimétrique différentielle (DSC) Kunststoffe - Dynamische Differenz-Thermoanalyse
- Partie 2: Détermination de la température et de la (DSC) - Teil 2: Bestimmung der
hauteur de palier de transition vitreuse (ISO 11357- Glasübergangstemperatur und der
2:2020) Glasübergangsstufenhöhe (ISO 11357-2:2020)
This European Standard was approved by CEN on 29 February 2020.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2020 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 11357-2:2020 E
worldwide for CEN national Members.
Contents Page
European foreword . 3
European foreword
This document (EN ISO 11357-2:2020) has been prepared by Technical Committee ISO/TC 61 "Plastics"
in collaboration with Technical Committee CEN/TC 249 “Plastics” the secretariat of which is held by
NBN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by September 2020, and conflicting national standards
shall be withdrawn at the latest by September 2020.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 11357-2:2014.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the
United Kingdom.
Endorsement notice
The text of ISO 11357-2:2020 has been approved by CEN as EN ISO 11357-2:2020 without any
modification.
INTERNATIONAL ISO
STANDARD 11357-2
Third edition
2020-03
Plastics — Differential scanning
calorimetry (DSC) —
Part 2:
Determination of glass transition
temperature and step height
Plastiques — Analyse calorimétrique différentielle (DSC) —
Partie 2: Détermination de la température et de la hauteur de palier
de transition vitreuse
Reference number
ISO 11357-2:2020(E)
©
ISO 2020
ISO 11357-2:2020(E)
© ISO 2020
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting
on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address
below or ISO’s member body in the country of the requester.
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Published in Switzerland
ii © ISO 2020 – All rights reserved
ISO 11357-2:2020(E)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Apparatus and materials. 2
6 Test specimens. 2
7 Test conditions and specimen conditioning . 2
8 Calibration . 2
9 Procedure. 2
9.1 Setting up the apparatus. 2
9.2 Loading the test specimen into the crucible . 2
9.3 Insertion of crucibles . 2
9.4 Temperature scan . 2
10 Expression of results . 3
10.1 Determination of glass transition temperatures . 3
10.1.1 General. 3
10.1.2 Equal-areas method . 4
10.1.3 Half-step-height method . 6
10.1.4 Inflection-point method . 7
10.2 Determination of glass transition step height . 8
11 Precision . 8
12 Test report . 8
Bibliography . 9
ISO 11357-2:2020(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/ patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation on the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO's adherence to the
World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see the following
URL: www .iso .org/ iso/ foreword .html.
This document was prepared by Technical Committee ISO/TC 61, Plastics, Subcommittee SC 5, Physical-
chemical properties, in collaboration with the European Committee for Standardization (CEN) Technical
Committee CEN/TC 249, Plastics, in accordance with the Agreement on technical cooperation between
ISO and CEN (Vienna Agreement).
This third edition cancels and replaces the second edition (ISO 11357-2:2013), which has been
technically revised. The main changes compared to the previous edition are as follows:
— revision of definition of glass transition step height;
— correction of unit of glass transition step height;
— assessment of methods for determination of T ;
g
— revision of rounding of T ;
g
— strong restriction of re-using crucibles.
A list of all parts in the ISO 11357 series can be found on the ISO website.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www .iso .org/ members .html.
iv © ISO 2020 – All rights reserved
INTERNATIONAL STANDARD ISO 11357-2:2020(E)
Plastics — Differential scanning calorimetry (DSC) —
Part 2:
Determination of glass transition temperature and step
height
1 Scope
This document specifies methods for the determination of the glass transition temperature and the
step height related to the glass transition of amorphous and partially crystalline p
...
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