Soft soldering fluxes — Test methods — Part 18: Cleanliness of soldered printed circuit assemblies before and/or after cleaning

This document specifies test methods for the cleanliness of soldered printed circuit assemblies before and/or after soldering and cleaning. The test is applicable to all fluxes as defined in ISO 9454-1.

Titre manque — Partie 18: Titre manque

General Information

Status
Published
Publication Date
15-Aug-2024
Current Stage
6060 - International Standard published
Start Date
16-Aug-2024
Due Date
15-Sep-2024
Completion Date
16-Aug-2024
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ISO 9455-18:2024 - Soft soldering fluxes — Test methods — Part 18: Cleanliness of soldered printed circuit assemblies before and/or after cleaning Released:16. 08. 2024
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International
Standard
ISO 9455-18
First edition
Soft soldering fluxes — Test
2024-08
methods —
Part 18:
Cleanliness of soldered printed
circuit assemblies before and/or
after cleaning
Reference number
© ISO 2024
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
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Published in Switzerland
ii
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Reagents and cleaning solvent . 2
6 Apparatus . 3
7 Procedure . 3
7.1 Preparation of the test sample .3
7.2 Test method .3
7.2.1 SIR .3
7.2.2 Ionic contamination test .3
8 Assessment and expression of results . 3
9 Test report . 3
Annex A (informative) Example of test methods and test results of cleanliness of the soldered
printed circuit boards before and/or after cleaning . 4
Annex B (informative) FT-IR analysis . 9
Bibliography .12

iii
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out through
ISO technical committees. Each member body interested in a subject for which a technical committee
has been established has the right to be represented on that committee. International organizations,
governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely
with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are described
in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the different types
of ISO document should be noted. This document was drafted in accordance with the editorial rules of the
ISO/IEC Directives, Part 2 (see www.iso.org/directives).
ISO draws attention to the possibility that the implementation of this document may involve the use of (a)
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rights in respect thereof. As of the date of publication of this document, ISO had not received notice of (a)
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this may not represent the latest information, which may be obtained from the patent database available at
www.iso.org/patents. ISO shall not be held responsible for identifying any or all such patent rights.
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and expressions
related to conformity assessment, as well as information about ISO's adherence to the World Trade
Organization (WTO) principles in the Technical Barriers to Trade (TBT), see www.iso.org/iso/foreword.html.
This document was prepared by Technical Committee ISO/TC 44, Welding and allied processes, Subcommittee
SC 12, Soldering materials.
A list of all parts in the ISO 9455 series can be found on the ISO website.
Any feedback or questions on this document should be directed to the user’s
national standards body. A complete listing of these bodies can be found at
www.iso.org/members.html. Official interpretations of ISO/TC 44 documents, where they exist, are
available from this page: https://committee.iso.org/sites/tc44/home/interpretation.html.

iv
International Standard ISO 9455-18:2024(en)
Soft soldering fluxes — Test methods —
Part 18:
Cleanliness of soldered printed circuit assemblies before
and/or after cleaning
1 Scope
This document specifies test methods for the cleanliness of soldered printed circuit assemblies before and/
or after soldering and cleaning. The test is applicable to all fluxes as defined in ISO 9454-1.
2 Normative references
There are no normative references in this document.
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.
ISO and IEC maintain terminology databases for use in standardization at the following addresses:
— ISO Online browsing platform: available at https:// www .iso .org/ obp
— IEC Electropedia: available at https:// www .electropedia .org/
3.1
flux residue
flux components remaining around the soldering area after reflow
3.2
white residue
flux components remaining around the soldering area after cleaning
4 Principle
Test sample before and/or after cleaning the soldered printed circuit assemblies is prepared without
contamination. Then, the test sample is tested by the flow chart given in Figure 1. The test methods are
detailed in Table 1.
The first step is to check for the presence or absence of flux residue on the PCB by microscope and/or SEM.
Next step is identification and/or reliability test of the flux residue. Identification of flux residue is carried
out by SEM/EDX and/or FT-IR. Reliability tests are carried out by ionic contamination tester (Ref. ROSE test)
and/or SIR and/or dielectric property test. This second step tests are optional, where users can select the
test methods to meet user’s requirements. An example of test methods and test results of cleanliness of the
soldered printed circuit boards before and/or after cleaning is provided in Annex A. An example for a FT-IR
analysis is shown in Annex B.
ISO 945
...

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