ISO 20407:2017

Fine ceramics (advanced ceramics, advanced technical ceramics) — Test method for interfacial tensile and shear fatigue properties of ceramic joining loaded in constant amplitude at room temperature

ISO 20407:2017 specifies a test method for determining interfacial tensile/tensile or shear/shear cyclic fatigue properties of ceramic-ceramic, ceramic-metal, and ceramic-glass joining loaded in the constant amplitude at room temperature. Procedures for test piece preparation, test modes and rates (load rate or displacement), data collection and reporting procedures are given. ISO 20407:2017 applies primarily to ceramic materials, including monolithic fine ceramics and whisker-, fibre- or particle-reinforced ceramic composites. This test method can be used for material research, quality control, and characterization and design data-generation purposes.

Céramiques fines (céramiques avancées, céramiques techniques avancées) — Méthode d'essai relatives aux propriétés de tension interfaciale et de fatigue en cisaillement des jonctions céramiques à amplitude constante

General Information

• Status: Published
• Publication Date: 07-Sep-2017
• ICS: 81.060.30 - Advanced ceramics
• Technical Committee: ISO/TC 206 - Fine ceramics
• Drafting Committee: ISO/TC 206/WG 8 - Joining
• Current Stage: 9093 - International Standard confirmed
• Completion Date: 03-Dec-2022

Standards Content (Sample)

INTERNATIONAL ISO
STANDARD 20407
First edition
2017-09
Fine ceramics (advanced ceramics,
advanced technical ceramics) — Test
method for interfacial tensile and
shear fatigue properties of ceramic
joining loaded in constant amplitude
at room temperature
Céramiques fines (céramiques avancées, céramiques techniques
avancées) — Méthode d'essai relatives aux propriétés de tension
interfaciale et de fatigue en cisaillement des jonctions céramiques à
amplitude constante
Reference number
ISO 20407:2017(E)
ISO 2017
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ISO 20407:2017(E)
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© ISO 2017, Published in Switzerland

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ii © ISO 2017 – All rights reserved
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ISO 20407:2017(E)
Contents Page

Foreword ........................................................................................................................................................................................................................................iv

1 Scope ................................................................................................................................................................................................................................. 1

2 Normative references ...................................................................................................................................................................................... 1

3 Terms and definitions ..................................................................................................................................................................................... 1

4 Principle ........................................................................................................................................................................................................................ 2

5 Apparatus ..................................................................................................................................................................................................................... 3

6 Test pieces ................................................................................................................................................................................................................... 5

6.1 Test-piece size .......................................................................................................................................................................................... 5

6.2 Test-piece preparation ..................................................................................................................................................................... 5

6.2.1 General...................................................................................................................................................................................... 5

6.2.2 Test-piece storage ........................................................................................................................................................... 5

6.2.3 Number of test pieces .................................................................................................................................................. 5

7 Test procedure ........................................................................................................................................................................................................ 6

7.1 Measurement of the test piece dimensions .................................................................................................................... 6

7.2 Measurement of the interfacial tensile fatigue properties ................................................................................ 6

7.3 Measurement of the interfacial shear fatigue properties ................................................................................... 6

7.4 Residual properties ............................................................................................................................................................................. 7

7.5 Test validity ................................................................................................................................................................................................ 7

8 Calculation of results ....................................................................................................................................................................................... 8

9 Test report ................................................................................................................................................................................................................... 8

© ISO 2017 – All rights reserved iii
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ISO 20407:2017(E)
Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards

bodies (ISO member bodies). The work of preparing International Standards is normally carried out

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electrotechnical standardization.

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described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the

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This document was prepared by Technical Committee ISO/TC 206, Fine ceramics.
iv © ISO 2017 – All rights reserved
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INTERNATIONAL STANDARD ISO 20407:2017(E)
Fine ceramics (advanced ceramics, advanced technical
ceramics) — Test method for interfacial tensile and shear
fatigue properties of ceramic joining loaded in constant
amplitude at room temperature
1 Scope

This document specifies a test method for determining interfacial tensile/tensile or shear/shear cyclic

fatigue properties of ceramic-ceramic, ceramic-metal, and ceramic-glass joining loaded in the constant

amplitude at room temperature. Procedures for test piece preparation, test modes and rates (load rate

or displacement), data collection and reporting procedures are given.

This document applies primarily to ceramic materials, including monolithic fine ceramics and whisker-,

fibre- or particle-reinforced ceramic composites. This test method can be used for material research,

quality control, and characterization and design data-generation purposes.
2 Normative references

The following documents are referred to in the text in such a way that some or all of their content

constitutes requirements of this document. For dated references, only the edition cited applies. For

undated references, the latest edition of the referenced document (including any amendments) applies.

ISO 3611, Geometrical product specifications (GPS) — Dimensional measuring equipment: Micrometers for

external measurements — Design and metrological characteristics

ISO 7500-1, Metallic materials — Calibration and verification of static uniaxial testing machines — Part 1:

Tension/compression testing machines — Calibration and verification of the force-measuring system

ISO 13124, Fine ceramics (advanced ceramics, advanced technical ceramics) — Test method for interfacial

bond strength of ceramic materials
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.

ISO and IEC maintain terminological databases for use in standardization at the following addresses:

— ISO Online browsing platform: available at http://www.iso.org/obp
— IEC Electropedia: available at http://www.electropedia.org/
3.1
cross-bonded test piece
test sample in the form of a symmetrical cross

Note 1 to entry: Prepared by joining two rectangular bars with the same shape and size, as described in

ISO 13124.
3.2
average applied stress during cyclic fatigue

average value between the maximum applied stress and the minimum applied stress during cyclic fatigue

© ISO 2017 – All rights reserved 1
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ISO 20407:2017(E)
3.3
constant amplitude loading

under a given average applied stress, σ , keeping peak loads and valley loads constant for wave form

loading in cyclic fatigue loading, Δσ = (σ − σ )/2 = σ − σ = σ − σ
max min max m m min
3.4
number of cycles
total number of loading cycles applied to the test piece during the test
3.5
cyclic fatigue life
total number of loading cycles until the test piece is up to failure
3.6
time to failure
time duration until the test piece is up to failure
4 Principle

A cross-bonded test piece is cycled under a given average stress with constant amplitude loading at

room temperature, which yields cyclic tensile/tensile or shear/shear stress in the interface. Typical

cyclic loading waves including sine wave, triangular wave and trapezoidal wave are shown in Figure 1.

...