Lignins — Determination of dry matter content — Oven-drying and freeze-drying methods

This document describes methods for the determination of the dry matter content of lignins by oven-drying and freeze-drying. The methods are applicable to all types of lignins isolated from kraft, organosolv, soda, and sulfite pulping processes, and to lignin obtained by enzymatic or acid hydrolysis of biomass. However, the oven-drying method is not applicable to kraft lignins in the base form, also referred to as sodium form. Both methods are applicable only to lignins in the solid form.

Lignines — Détermination de la teneur en matières sèches — Méthodes par séchage à l’étuve et par lyophilisation

Le présent document décrit des méthodes pour la détermination de la teneur en matières sèches des lignines par séchage à l’étuve et par lyophilisation. Les méthodes sont applicables à tous les types de lignines isolées par des procédés de mise en pâte kraft, organosolve, soude et lignosulfates, et à la lignine obtenue par hydrolyse enzymatique ou acide de la biomasse. Toutefois, la méthode par séchage à l’étuve n’est pas applicable aux lignines kraft sous forme de base, également appelée forme de sodium. Les deux méthodes s’appliquent uniquement aux lignines sous forme solide.

General Information

Status
Published
Publication Date
13-Feb-2024
Current Stage
6060 - International Standard published
Start Date
14-Feb-2024
Due Date
09-Jul-2024
Completion Date
14-Feb-2024
Ref Project

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Standards Content (Sample)

FINAL
INTERNATIONAL ISO/FDIS
DRAFT
STANDARD 6350
ISO/TC 6
Lignins — Determination of dry
Secretariat: SCC
matter content — Oven-drying and
Voting begins on:
2023-10-06 freeze-drying methods
Voting terminates on:
Lignines — Détermination de la teneur en matières sèches —
2023-12-01
Méthodes par séchage à l'étuve et lyophilisation
RECIPIENTS OF THIS DRAFT ARE INVITED TO
SUBMIT, WITH THEIR COMMENTS, NOTIFICATION
OF ANY RELEVANT PATENT RIGHTS OF WHICH
THEY ARE AWARE AND TO PROVIDE SUPPOR TING
DOCUMENTATION.
IN ADDITION TO THEIR EVALUATION AS
Reference number
BEING ACCEPTABLE FOR INDUSTRIAL, TECHNO-
ISO/FDIS 6350:2023(E)
LOGICAL, COMMERCIAL AND USER PURPOSES,
DRAFT INTERNATIONAL STANDARDS MAY ON
OCCASION HAVE TO BE CONSIDERED IN THE
LIGHT OF THEIR POTENTIAL TO BECOME STAN-
DARDS TO WHICH REFERENCE MAY BE MADE IN
NATIONAL REGULATIONS. © ISO 2023

---------------------- Page: 1 ----------------------
ISO/FDIS 6350:2023(E)
FINAL
INTERNATIONAL ISO/FDIS
DRAFT
STANDARD 6350
ISO/TC 6
Lignins — Determination of dry
Secretariat: SCC
matter content — Oven-drying and
Voting begins on:
freeze-drying methods
Voting terminates on:
Lignines — Détermination de la teneur en matières sèches —
Méthodes par séchage à l'étuve et lyophilisation
COPYRIGHT PROTECTED DOCUMENT
© ISO 2023
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
RECIPIENTS OF THIS DRAFT ARE INVITED TO
ISO copyright office
SUBMIT, WITH THEIR COMMENTS, NOTIFICATION
OF ANY RELEVANT PATENT RIGHTS OF WHICH
CP 401 • Ch. de Blandonnet 8
THEY ARE AWARE AND TO PROVIDE SUPPOR TING
CH-1214 Vernier, Geneva
DOCUMENTATION.
Phone: +41 22 749 01 11
IN ADDITION TO THEIR EVALUATION AS
Reference number
Email: copyright@iso.org
BEING ACCEPTABLE FOR INDUSTRIAL, TECHNO­
ISO/FDIS 6350:2023(E)
Website: www.iso.org
LOGICAL, COMMERCIAL AND USER PURPOSES,
DRAFT INTERNATIONAL STANDARDS MAY ON
Published in Switzerland
OCCASION HAVE TO BE CONSIDERED IN THE
LIGHT OF THEIR POTENTIAL TO BECOME STAN­
DARDS TO WHICH REFERENCE MAY BE MADE IN
ii
  © ISO 2023 – All rights reserved
NATIONAL REGULATIONS. © ISO 2023

---------------------- Page: 2 ----------------------
ISO/FDIS 6350:2023(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 2
5 Apparatus . 2
6 Sampling . 2
7 Determination of dry matter content .3
7.1 General . 3
7.2 Oven-drying .
...

ISO/DISFDIS 6350:20222023(E)
Date: 2022-11-302023-09-21
ISO TC 6/WG 16
Secretariat: SCC
Secretariat: CA
Lignins — Determination of dry matter content — Oven-drying and freeze-drying
methods

---------------------- Page: 1 ----------------------
ISO/DISFDIS 6350:20222023(E)
© ISO 20222023
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part
of this publication may be reproduced or utilized otherwise in any form or by any means, electronic or
mechanical, including photocopying, or posting on the internet or an intranet, without prior written
permission. Permission can be requested from either ISO at the address below or ISO’s member body
in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii © ISO 20222023 – All rights reserved

---------------------- Page: 2 ----------------------
ISO/DISFDIS 6350:20222023(E)
Contents
Foreword . iv
Introduction . v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 2
5
. Apparatus…………………………………………………………………………………………………………………
……2
6
. Sampling……………………………………………………………………………………………………………………
……3
7 Determination of dry matter
content………………………………………………………………………………3
7.1 Oven-drying……………………………………………………………………………………………………………………3
7.2 Lyophilization (freeze-drying)………………………………………………………………………………………4
8
. Calculation…………………………………………………………………………………………………………………
…….4
9
Report…………………………………………………………………………………………………………………………
……5
Annex A (informative)
Precision……………………………………………………………………………………………6
Bibliography…………………………………………………………………………………………………………………………
7
Foreword . iv
Introduction . v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 2
5 Apparatus . 2
6 Sampling . 3
7 Determination of dry matter content . 3
7.1 General . 3
7.2 Oven-drying . 3
7.3 Lyophilization (Freeze-drying) . 4
8 Calculation . 5
© ISO 20222023 – All rights reserved iii

---------------------- Page: 3 ----------------------
ISO/DISFDIS 6350:20222023(E)
9 Precision . 5
10 Report .
...

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