ISO 15470:2017

Surface chemical analysis — X-ray photoelectron spectroscopy — Description of selected instrumental performance parameters

ISO 15470:2017 describes the way in which specific aspects of the performance of an X-ray photoelectron spectrometer are described.

Analyse chimique des surfaces — Spectroscopie de photoélectrons X — Description de certains paramètres relatifs à la performance instrumentale

General Information

• Status: Published
• Publication Date: 01-Mar-2017
• ICS: 71.040.40 - Chemical analysis
• Technical Committee: ISO/TC 201/SC 7 - Electron spectroscopies
• Drafting Committee: ISO/TC 201/SC 7 - Electron spectroscopies
• Current Stage: 9093 - International Standard confirmed
• Completion Date: 16-Jul-2022

Relations

• Revises: ISO 15470:2004 - Surface chemical analysis — X-ray photoelectron spectroscopy — Description of selected instrumental performance parameters
• Effective Date: 16-Jul-2016

Standards Content (Sample)

INTERNATIONAL ISO
STANDARD 15470
Second edition
2017-03
Surface chemical analysis — X-ray
photoelectron spectroscopy —
Description of selected instrumental
performance parameters
Analyse chimique des surfaces — Spectroscopie de photoélectrons
X — Description de certains paramètres relatifs à la performance
instrumentale
Reference number
ISO 15470:2017(E)
©
ISO 2017

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ISO 15470:2017(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2017, Published in Switzerland
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
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ii © ISO 2017 – All rights reserved

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ISO 15470:2017(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Abbreviated terms . 1
5 Description of selected instrumental performance parameters . 1
5.1 Method of analysis . 1
5.2 Samples . 1
5.3 System configuration . 2
5.4 X-ray source . 2
5.4.1 Anode type . 2
5.4.2 Anode power . 2
5.4.3 Expected anode lifetime . 2
5.5 Spectrometer intensity performance and energy resolution . 2
5.6 Spectrometer energy scale . 2
5.7 Spectrometer intensity linearity. 3
5.8 Spectrometer response function . 3
5.9 Imaging and selected area resolution . 3
5.9.1 General. 3
5.9.2 Method 1 . 3
5.9.3 Method 2 . 3
5.9.4 Method 3 . 4
5.10 Charge neutralization . 4
5.11 Angle-resolved XPS . 4
5.12 Vacuum environment . 4
Bibliography . 5
© ISO 2017 – All rights reserved iii

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ISO 15470:2017(E)

Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/ patents).
Any trade name used in this document is information given for the convenience of users and does not
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For an explanation on the voluntary nature of standards, the meaning of ISO specific terms and
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URL: w w w . i s o .org/ iso/ foreword .html.
This document was prepared by Technical Committee ISO/TC 201, Surface chemical analysis,
Subcommittee SC 7, X-ray photoelectron spectroscopy.
This second edition cancels and replaces the first edition (ISO 15470:2004), of which it constitutes a
minor revision.
The changes compared to the previous edition are as follows:
— a typo has been corrected in 5.10;
— a Bibliography has been added;
— the text has been editorially revised to comply with the most recent drafting rules.
iv © ISO 2017 – All rights reserved

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ISO 15470:2017(E)

Introduction
X-ray photoelectron spectrometers are produced by many manufacturers throughout the world. While
the basic principle of the XPS analytical method in each instrument is the same, the specific designs of
the instruments and the way that performance specifications are provided differ widely. As a result,
it is often difficult to compare the performance of instruments from one manufacturer with those
from another. This document provides a basic list of items devised to enable all X-ray photoelectron
spectrometers to be described in a common manner. This document is not intended to replace the
manufacturer’s specification, which may extend to 30 or more pages. It is intended that, where certain
items are defined in that specification, there is an agreed and defined meaning to that item.
© ISO 2017 – All rights reserved v

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INTERNATIONAL STANDARD ISO 15470:2017(E)
Surface chemical analysis — X-ray photoelectron
spectroscopy — Description of selected instrumental
performance parameters
1 Scope
This document describes the way in which specific aspects of the performance of an X-ray photoelectron
spectrometer are described.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes
...