ISO 5600:2017

Rubber — Determination of adhesion to rigid materials using conical shaped parts

ISO 5600:2017 specifies a method for the determination of the static vulcanized adhesion strength of rubber compounds to rigid materials. The test piece is composed of two conical ends of the rigid material, joined by a cylinder of rubber. The adhesion is obtained by a bonding system which can include not only the rigid material and the rubber compound, but other elements such as thin alloy coatings or chemical treatments of rigid parts and either a single cement or both primer and cover cements. The bonding system for preparing the test pieces should be adequately specified by the user, but provision is made in this document for the evaluation of different types of failure related to a complex bonding system. The method is designed primarily for test pieces prepared in the laboratory under standard conditions in order to provide data for development and control of bonding systems and their components, such as cements or special rubber compounds, and of methods of manufacture. While intended to be applied where the rubber is bonded to rigid supporting pieces, it might not cover such cases where the support, although of high-modulus material, has a low rigidity due to small transverse dimensions, as in the case of rubber bonded to metal wires, cords or thin sheets.

Caoutchouc — Détermination de l'adhérence aux matériaux rigides au moyen de pièces coniques

General Information

• Status: Published
• Publication Date: 31-May-2017
• ICS: 83.060 - Rubber
• Technical Committee: ISO/TC 45/SC 2 - Testing and analysis
• Drafting Committee: ISO/TC 45/SC 2/WG 1 - Physical properties
• Current Stage: 9060 - Close of review
• Start Date: 02-Sep-2027

Relations

• Revises: ISO 5600:2011 - Rubber — Determination of adhesion to rigid materials using conical shaped parts
• Effective Date: 10-Dec-2016

Standards Content (Sample)

INTERNATIONAL ISO
STANDARD 5600
Fifth edition
2017-06
Rubber — Determination of adhesion
to rigid materials using conical
shaped parts
Caoutchouc — Détermination de l’adhérence aux matériaux rigides
au moyen de pièces coniques
Reference number
ISO 5600:2017(E)
ISO 2017
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ISO 5600:2017(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2017, Published in Switzerland

All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form

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ii © ISO 2017 – All rights reserved
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ISO 5600:2017(E)
Contents Page

Foreword ........................................................................................................................................................................................................................................iv

1 Scope ................................................................................................................................................................................................................................. 1

2 Normative references ...................................................................................................................................................................................... 1

3 Terms and definitions ..................................................................................................................................................................................... 1

4 Principle ........................................................................................................................................................................................................................ 2

5 Apparatus ..................................................................................................................................................................................................................... 2

6 Calibration .................................................................................................................................................................................................................. 2

7 Test piece ...................................................................................................................................................................................................................... 2

7.1 Form and dimensions ......... ............................................................................................................................................................... 2

7.2 Materials ....................................................................................................................................................................................................... 2

7.3 Preparation ................................................................................................................................................................................................ 3

7.4 Number of test pieces ....................................................................................................................................................................... 3

7.5 Conditioning of test pieces ........................................................................................................................................................... 3

8 Procedure..................................................................................................................................................................................................................... 4

9 Expression of results ........................................................................................................................................................................................ 4

9.1 Adhesion value ........................................................................................................................................................................................ 4

9.2 Type of adhesion failure .................................................................................................................................................................. 4

10 Salvaging of bonded metal parts .......................................................................................................................................................... 4

11 Test report ................................................................................................................................................................................................................... 5

Annex A (normative) Calibration schedule ................................................................................................................................................... 6

© ISO 2017 – All rights reserved iii
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ISO 5600:2017(E)
Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards

bodies (ISO member bodies). The work of preparing International Standards is normally carried out

through ISO technical committees. Each member body interested in a subject for which a technical

committee has been established has the right to be represented on that committee. International

organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.

ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of

electrotechnical standardization.

The procedures used to develop this document and those intended for its further maintenance are

described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the

different types of ISO documents should be noted. This document was drafted in accordance with the

editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of

any patent rights identified during the development of the document will be in the Introduction and/or

on the ISO list of patent declarations received (see www .iso .org/ patents).

Any trade name used in this document is information given for the convenience of users and does not

constitute an endorsement.

For an explanation on the voluntary nature of standards, the meaning of ISO specific terms and

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URL: w w w . i s o .org/ iso/ foreword .html

This document was prepared by Technical Committee ISO/TC 45, Rubber and rubber products,

Subcommittee SC 2, Testing and analysis.

This fifth edition cancels and replaces the fourth edition (ISO 5600:2011), of which it constitutes a

minor revision to update the normative references in Clause 2.
iv © ISO 2017 – All rights reserved
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INTERNATIONAL STANDARD ISO 5600:2017(E)
Rubber — Determination of adhesion to rigid materials
using conical shaped parts

WARNING 1 — Persons using this document should be familiar with normal laboratory practice.

This document does not purport to address all of the safety problems, if any, associated with its

use. It is the responsibility of the user to establish appropriate safety and health practices and to

ensure compliance with any national regulatory conditions.

WARNING 2 — Certain procedures specified in this document might involve the use or generation

of substances, or the generation of waste, that could constitute a local environmental hazard.

Reference should be made to appropriate documentation on safe handling and disposal after use.

1 Scope

This document specifies a method for the determination of the static vulcanized adhesion strength

of rubber compounds to rigid materials. The test piece is composed of two conical ends of the rigid

material, joined by a cylinder of rubber.

The adhesion is obtained by a bonding system which can include not only the rigid material and the

rubber compound, but other elements such as thin alloy coatings or chemical treatments of rigid parts

and either a single cement or both primer and cover cements. The bonding system for preparing the

test pieces should be adequately specified by the user, but provision is made in this document for the

evaluation of different types of failure related to a complex bonding system.

The method is designed primarily for test pieces prepared in the laboratory under standard conditions

in order to provide data for development and control of bonding systems and their components, such

as cements or special rubber compounds, and of methods of manufacture. While intended to be applied

where the rubber is bonded to rigid supporting pieces, it might not cover such cases where the support,

although of high-modulus material, has a low rigidity due to small transverse dimensions, as in the case

of rubber bonded to metal wires, cords or thin sheets.
2 Normative references

The following documents are referred to in the text in such a way that some or all of their content

constitutes requirements of this document. For dated references, only the edition cited applies. For

undated references, the latest edition of the referenced document (including any amendments) applies.

ISO 5893:2002, Rubber and plastics test equipment — Tensile, flexural and compression types (constant

rate of traverse) — Specification
ISO 18899:2013, Rubber — Guide to the calibration of test equipment

ISO 23529, Rubber — General procedures for preparing and conditioning test pieces for physical test methods

3 Terms and definitions
No terms and definitions are listed in this document.

ISO and IEC maintain terminological databases for use in standardization at the following addresses:

— IEC Electropedia: available at http:// www .electropedia .org/
— ISO Online browsing platform: available at http:// www .iso .org/ obp
© ISO 2017 – All rights reserved 1
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ISO 5600:2017(E)
4 Principle
The test consists in mea
...