EN ISO 5842:2023
(Main)Powder metallurgy - Hot isostatic pressing - Argon detection using gas chromatography and mass spectrometry techniques (ISO 5842:2022)
Powder metallurgy - Hot isostatic pressing - Argon detection using gas chromatography and mass spectrometry techniques (ISO 5842:2022)
This document specifies a gas chromatography and a mass spectrometry method of detecting the presence of argon in metal powder produced components, consolidated by hot isostatic pressing.
This document specifies the calibration and functionality test for the equipment covered. It also specifies methods for sampling, sample preparation and sample test procedure of PM HIP components to detect argon presence.
Components produced by additive manufacturing are not covered in this document.
Pulvermetallurgie - Heißisostatisches Pressen - Nachweis von Argon mittels Gaschromatographie und massenspektrometrischer Techniken (ISO 5842:2022)
In diesem Dokument wird ein gaschromatographisches und massenspektrometrisches Verfahren zum Nachweis
von Argon in aus Metallpulver hergestellten Bauteilen, die durch heißisostatisches Pressen verfestigt wurden,
festgelegt.
In diesem Dokument werden die Kalibrierung und die Funktionsprüfung für die behandelte Ausrüstung festgelegt.
Außerdem werden Verfahren für die Probenahme, die Probenvorbereitung und die Probenprüfung von
PM-HIP-Bauteilen zum Nachweis von Argon festgelegt.
Durch additive Fertigung hergestellte Bauteile werden in diesem Dokument nicht behandelt.
WICHTIG — Es liegt in der Verantwortung des Erwerbers der PM-HIP-Dienstleistung, in der Bestellung
festzulegen, ob eine Argon-Erkennungsprüfung erforderlich ist. Ist dies der Fall, muss der vereinbarte
Grenzwert für Argon angegeben werden.
Métallurgie des poudres - Pressage isostatique à chaud - Détection de l’argon par des techniques de chromatographie en phase gazeuse et de spectrométrie de masse (ISO 5842:2022)
Le présent document spécifie une méthode de chromatographie en phase gazeuse et une méthode de spectrométrie de masse pour détecter la présence d’argon dans les constituants produits à partir de poudres de métal, consolidés par compression isostatique à chaud.
Le présent document spécifie l’étalonnage et l’essai de fonctionnalité applicables aux équipements couverts. Il spécifie également les méthodes d’échantillonnage, la préparation des échantillons et la procédure d’essai des constituants PM HIP pour détecter la présence d’argon.
Les constituants produits par fabrication additive ne sont pas couverts par le présent document.
Metalurgija prahov - Vroče izostatično stiskanje - Zaznavanje argona s tehnikami plinske kromatografije in masne spektrometrije (ISO 5842:2022)
Ta dokument določa metodo plinske kromatografije in masne spektrometrije za zaznavanje prisotnosti argona v komponentah, izdelanih iz kovinskega praška in utrjenih z vročim izostatičnim stiskanjem.
Ta dokument določa kalibracijo in preskus funkcionalnosti za obravnavano opremo. Določa tudi metode za vzorčenje, pripravo vzorcev in postopek preskušanja vzorcev komponent PM HIP za zaznavanje prisotnosti argona.
Komponente, izdelane z aditivno proizvodnjo, niso obravnavane v tem dokumentu.
General Information
Standards Content (Sample)
SLOVENSKI STANDARD
01-september-2023
Metalurgija prahov - Vroče izostatično stiskanje - Zaznavanje argona s tehnikami
plinske kromatografije in masne spektrometrije (ISO 5842:2022)
Powder metallurgy - Hot isostatic pressing - Argon detection using gas chromatography
and mass spectrometry techniques (ISO 5842:2022)
Pulvermetallurgie - Heißisostatisches Pressen - Nachweis von Argon mittels
Gaschromatographie und massenspektrometrischer Techniken (ISO 5842:2022)
Métallurgie des poudres - Pressage isostatique à chaud - Détection de l’argon par des
techniques de chromatographie en phase gazeuse et de spectrométrie de masse (ISO
5842:2022)
Ta slovenski standard je istoveten z: EN ISO 5842:2023
ICS:
77.160 Metalurgija prahov Powder metallurgy
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
EN ISO 5842
EUROPEAN STANDARD
NORME EUROPÉENNE
June 2023
EUROPÄISCHE NORM
ICS 77.160
English Version
Powder metallurgy - Hot isostatic pressing - Argon
detection using gas chromatography and mass
spectrometry techniques (ISO 5842:2022)
Métallurgie des poudres - Pressage isostatique à chaud Pulvermetallurgie - Heißisostatisches Pressen -
- Détection de l'argon par des techniques de Nachweis von Argon mittels Gaschromatographie und
chromatographie en phase gazeuse et de spectrométrie massenspektrometrischer Techniken (ISO 5842:2022)
de masse (ISO 5842:2022)
This European Standard was approved by CEN on 26 June 2023.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2023 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 5842:2023 E
worldwide for CEN national Members.
Contents Page
European foreword . 3
European foreword
The text of ISO 5842:2022 has been prepared by Technical Committee ISO/TC 119 "Powder metallurgy”
of the International Organization for Standardization (ISO) and has been taken over as
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by December 2023, and conflicting national standards
shall be withdrawn at the latest by December 2023.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
Any feedback and questions on this document should be directed to the users’ national standards body.
A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the
United Kingdom.
Endorsement notice
The text of ISO 5842:2022 has been approved by CEN as EN ISO 5842:2023 without any modification.
INTERNATIONAL ISO
STANDARD 5842
First edition
2022-10
Powder metallurgy — Hot isostatic
pressing — Argon detection using
gas chromatography and mass
spectrometry techniques
Reference number
ISO 5842:2022(E)
ISO 5842:2022(E)
© ISO 2022
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
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Published in Switzerland
ii
ISO 5842:2022(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Equipment for argon detection . 3
4.1 Gas chromatography . 3
4.1.1 Principle . 3
4.1.2 Apparatus and reagents . 3
4.1.3 Equipment detection limit . 4
4.2 Mass spectrometry . 4
4.2.1 Principle . 4
4.2.2 Apparatus and reagents . 4
4.2.3 Equipment detection limit . 4
5 Calibration and functionality test . 5
5.1 General . 5
5.2 Gas chromatograph . 5
5.2.1 Calibration . . . 5
5.2.2 Functionality test. 5
5.3 Mass spectrometer . 5
5.3.1 Calibration . . . 5
5.3.2 Functionality test. 6
6 Sample preparation for argon detection . 6
7 Test procedure for argon detection .6
7.1 General . 6
7.2 Test procedure using gas chromatography . 6
7.3 Test procedure using mass spectrometry . 7
8 Test report . 7
Annex A (informative) Precision . 8
Bibliography .10
iii
ISO 5842:2022(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
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ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www.iso.org/patents).
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expressions related to conformity assessment, as well as information about ISO's adherence to
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www.iso.org/iso/foreword.html.
This document was prepared by Technical Committee ISO/TC 119 Powder metallurgy, Subcommittee
SC 3, Sampling and testing methods for sintered metal materials (excluding hardmetals).
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www.iso.org/members.html.
iv
ISO 5842:2022(E)
Introduction
It is essential to detect argon in powder metallurgy hot isostatic pressing (PM HIP) material in order to
ensure the desired performance of the PM HIP component. Argon from the production of powder can
...
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