EN ISO 13160:2015

Water quality - Strontium 90 and strontium 89 - Test methods using liquid scintillation counting or proportional counting (ISO 13160:2012)

ISO 13160:2012 specifies the test methods and their associated principles for the measurement of the activity of 90Sr in equilibrium with 90Y, and 89Sr, pure beta-emitting radionuclides, in water samples. Different chemical separation methods are presented to produce strontium and yttrium sources, the activity of which is determined using a proportional counter (PC) or liquid scintillation counter (LSC). The selection of the test method depends on the origin of the contamination, the characteristics of the water to be analysed, the required accuracy of test results and the available resources of the laboratories.
These test methods are used for water monitoring following, past or present, accidental or routine, liquid or gaseous discharges. It also covers the monitoring of contamination caused by global fallout.
When fallout occurs immediately following a nuclear accident, the contribution of 89Sr to the total amount of strontium activity is not negligible. ISO 13160:2012 provides the test methods to determine the activity concentration of 90Sr in presence of 89Sr.

Wasserbeschaffenheit - Strontium 90 und Strontium 89 - Verfahren mittels Flüssigszintillationszählung oder Proportionalzählung (ISO 13160:2012)

Qualité de l'eau - Strontium 90 et strontium 89 - Méthodes d'essai par comptage des scintillations en milieu liquide ou par comptage proportionnel (ISO 13160:2012)

L'ISO 13160:2012 spécifie les méthodes d'essai et leurs principes associés de mesurage de l'activité du strontium 90Sr en équilibre avec 90Y, et du strontium 89Sr, qui sont des radionucléides émetteurs bêta purs, dans des échantillons d'eau. Différentes méthodes de séparation chimique sont présentées afin de produire des sources de strontium et d'yttrium dont les activités sont déterminées au moyen d'un compteur proportionnel (CP) ou d'un compteur à scintillations en milieu liquide (CSL). Le choix de la méthode d'essai dépend de l'origine de la contamination, des caractéristiques de l'eau à analyser, de l'exactitude requise des résultats d'essai et des ressources dont disposent les laboratoires.
Ces méthodes servent au contrôle de l'eau suite à des rejets liquides ou gazeux, qu'ils soient passés ou présents, accidentels ou de routine. Ces méthodes couvrent également le contrôle de la contamination due aux retombées mondiales.
Dans le cas de retombées récentes se produisant immédiatement après un accident nucléaire, la contribution du 89Sr au total de l'activité du strontium n'est pas négligeable. L'ISO 13160:2012 fournit les méthodes d'essai permettant de déterminer l'activité volumique du 90Sr en présence de 89Sr.

Kakovost vode - Stroncij Sr-90 in stroncij Sr-89 - Preskusne metode s štetjem s tekočinskim scintilatorjem ali proporcionalnim štetjem (ISO 13160:2012)

Ta mednarodni standard določa preskusne metode in z njimi povezana načela za merjenje aktivnosti stroncija Sr-90 v ravnovesju z itrijem Y-90 in stroncijem Sr-89, čistimi beta oddajnimi radionuklidami, v vzorcih vode. Predstavljene so različne metode kemičnega ločevanja za izdelavo virov stroncija in itrija, pri čemer se njihova aktivnost določi s proporcionalnim štetjem (PC) ali štetjem s tekočinskim scintilatorjem (LSC). Izbira preskusne metode je odvisna od izvora onesnaženosti, značilnosti vode, za katero se izvaja analiza, zahtevane
natančnosti rezultatov preskusa in virov, ki so na voljo v laboratorijih. Te preskusne metode se uporabljajo za spremljanje stanja vode v preteklosti ali sedanjosti, naključno ali rutinsko in za tekoče ali plinaste izpuste. Zajemajo tudi spremljanje onesnaženja, ki je posledica globalnega usedanja. Ko pride do usedanja neposredno po jedrski nesreči, prispevek stroncija Sr-89 k skupni količini aktivnosti stroncija ni zanemarljiv. Ta mednarodni standard določa preskusne metode za določanje koncentracije aktivnosti stroncija Sr-90 ob prisotnosti stroncija Sr-89.

General Information

• Status: Withdrawn
• Publication Date: 13-Oct-2015
• Withdrawal Date: 27-Jul-2021
• ICS: 13.060.60 - Examination of physical properties of water
• ICS: 17.240 - Radiation measurements
• Technical Committee: CEN/TC 230 - Water analysis
• Drafting Committee: CEN/TC 230 - Water analysis
• Current Stage: 9960 - Withdrawal effective - Withdrawal
• Completion Date: 28-Jul-2021
• Ref Project: SIST EN ISO 13160:2016 - Water quality - Strontium 90 and strontium 89 - Test methods using liquid scintillation counting or proportional counting (ISO 13160:2012)

Relations

• Replaced By: EN ISO 13160:2021 - Water quality - Strontium 90 and strontium 89 - Test methods using liquid scintillation counting or proportional counting (ISO 13160:2021)
• Effective Date: 17-Apr-2019

Standards Content (Sample)

SLOVENSKI STANDARD
01-februar-2016
.DNRYRVWYRGH6WURQFLM6ULQVWURQFLM6U3UHVNXVQHPHWRGHVãWHWMHPV
WHNRþLQVNLPVFLQWLODWRUMHPDOLSURSRUFLRQDOQLPãWHWMHP,62
Water quality - Strontium 90 and strontium 89 - Test methods using liquid scintillation
counting or proportional counting (ISO 13160:2012)
Wasserbeschaffenheit - Strontium 90 und Strontium 89 - Verfahren mittels
Flüssigszintillationszählung oder Proportionalzählung (ISO 13160:2012)
Qualité de l'eau - Strontium 90 et strontium 89 - Méthodes d'essai par comptage des
scintillations en milieu liquide ou par comptage proportionnel (ISO 13160:2012)
Ta slovenski standard je istoveten z: EN ISO 13160:2015
ICS:
13.060.60 Preiskava fizikalnih lastnosti Examination of physical
vode properties of water
17.240 Merjenje sevanja Radiation measurements
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 13160
EUROPEAN STANDARD
NORME EUROPÉENNE
October 2015
EUROPÄISCHE NORM
ICS 13.060.60; 17.240
English Version
Water quality - Strontium 90 and strontium 89 - Test
methods using liquid scintillation counting or proportional
counting (ISO 13160:2012)
Qualité de l'eau - Strontium 90 et strontium 89 - Wasserbeschaffenheit - Strontium 90 und Strontium
Méthodes d'essai par comptage des scintillations en 89 - Verfahren mittels Flüssigszintillationszählung
milieu liquide ou par comptage proportionnel (ISO oder Proportionalzählung (ISO 13160:2012)
13160:2012)
This European Standard was approved by CEN on 27 September 2015.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2015 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 13160:2015 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
The text of ISO 13160:2012 has been prepared by Technical Committee ISO/TC 147 “Water quality” of
the International Organization for Standardization (ISO) and has been taken over as EN ISO 13160:2015
by Technical Committee CEN/TC 230 “Water analysis” the secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by April 2016, and conflicting national standards shall be
withdrawn at the latest by April 2016.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent
rights.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 13160:2012 has been approved by CEN as EN ISO 13160:2015 without any modification.
INTERNATIONAL ISO
STANDARD 13160
First edition
2012-07-15
Water quality — Strontium 90 and strontium
89 — Test methods using liquid scintillation
counting or proportional counting
Qualité de l’eau — Strontium 90 et strontium 89 — Méthodes d’essai
par comptage des scintillations en milieu liquide ou par comptage
proportionnel
Reference number
ISO 13160:2012(E)
©
ISO 2012
ISO 13160:2012(E)
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means,
electronic or mechanical, including photocopying and microfilm, without permission in writing from either ISO at the address below or ISO’s
member body in the country of the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail [e-mail]
Web www.iso.org
Published in Switzerland
ii © ISO 2012 – All rights reserved

ISO 13160:2012(E)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Symbols, definitions, and units . 1
4 Principle . 2
4.1 General . 2
4.2 Chemical separation . 2
4.3 Detection . 3
5 Chemical reagents and equipment . 3
6 Procedure . 3
6.1 Test sample preparation . 3
6.2 Chemical separation . 3
6.3 Preparation of the source for test . 5
6.4 Measurement . 6
7 Expression of results . 8
90 90
7.1 Determination of Sr in equilibrium with Y . 8
90 90
7.2 Determination of Sr by ingrowth of Y . 9
90 89 90 90
7.3 Determination of Sr in presence of Sr when Sr is in equilibrium with Y . 11
7.4 Confidence limits .14
8 Quality control .14
9 Test report .15
89 90
Annex A (informative) Determination of Sr and Sr by precipitation and proportional counting .16
89 90
Annex B (informative) Determination of Sr and Sr by precipitation and liquid scintillation counting 20
90 90
Annex C (informative) Determination of Sr from its daughter product Y at equilibrium by organic
extraction and liquid scintillation counting.24
Annex D (informative) Determination of Sr after ionic exchange separation by proportional counting 26
Annex E (informative) Determination of Sr after separation on a crown ether specific resin and liquid
scintillation counting .29
90 90
Annex F (informative) Determination of Sr from its daughter product Y at equilibrium by organic
extraction by proportional counting .31
Annex G (informative) Correction factor for purity control using proportional counting .35
Bibliography .38
ISO 13160:2012(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies
(ISO member bodies). The work of preparing International Standards is normally carried out through ISO
technical committees. Each member body interested in a subject for which a technical committee has been
established has the right to be represented on that committee. International organizations, governmental and
non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International
Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International Standards
adopted by the technical committees are circulated to the member bodies for voting. Publication as an
International Standard requires approval by at least 75 % of the member bodies casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. ISO shall not be held responsible for identifying any or all such patent rights.
ISO 13160 was prepared by Technical Committee ISO/TC 147, Water quality, Subcommittee SC 3,
Radiological methods.
iv © ISO 2012 – All rights reserved

INTERNATIONAL STANDARD ISO 13160:2012(E)
Water quality — Strontium 90 and strontium 89 — Test methods
using liquid scintillation counting or proportional counting
WARNING — Persons using this International Standard should be familiar with normal laboratory
practice. This document does not purport to address all of the safety problems, if any, associated with
its use. It is the responsibility of the user to establish appropriate safety and health practices and to
ensure compliance with any national regulatory conditions.
IMPORTANT — It is absolutely essential that tests conducted in accordance with this International
Standard be carried out by suitably qualified staff.
1 Scope
This International Standard specifies the test methods and their associated principles for the measurement
90 90 89
of the activity of Sr in equilibrium with Y, and Sr, pure beta-emitting radionuclides, in water samples.
Different chemical separation methods are presented to produce strontium and yttrium sources, the activity of
which is determined using a proportional counter (PC) or liquid scintillation counter (LSC). The selection of the
test method depends on the origin of the contamination, the characteristics of the water to be analysed, the
required accuracy of test results and the available resources of the laboratories.
These test methods are used for water monitoring following, past or present, accidental or routine, liquid or
gaseous discharges. It also covers the monitoring of contamination caused by global fallout.
When fallout occurs immediately following a nuclear accident, the contribution of Sr to the total amount of
strontium activity is not negligible. This International Standard provides the test methods to determine the
90 89
activity concentration of Sr in presence of Sr.
2 Normative references
The following referenced documents are indispensable for the application of this document. For dated
references, only the edition cited applies. For undated references, the latest edition of the referenced document
(including any amendments) applies.
ISO 11929, Determination of the characteristic limi
...