Standard Test Method for Tack-Free Time of Caulking Compounds and Sealants

ABSTRACT
This test method describes the determination of the tack-free time property of caulking compounds and sealants. The method is applicable to both gun and knife grades. Requirements for the apparatus including the cabinet or room, brass sheet, template, steel sheets, plastic strips (polyethylene strips), spatula, and knife blade are given. Methyl ethyl ketone, ethylene dichloride, or similar solvent shall be used. The test specimen shall be sampled from a previously unopened container and shall be thoroughly mixed before using. The method of preparation and conditioning of the test specimen, and the test procedure are detailed. No caulking compound or sealant shall adhere to the polyethylene strip in the test specimen.
SCOPE
1.1 This test method describes the determination of the tack-free time property of caulking compounds and sealants. This test method is applicable to both gun and knife grades.  
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 The committee with jurisdiction over this standard is not aware of any comparable standard published by other organizations.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Status
Published
Publication Date
30-Apr-2019
Current Stage
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ASTM D2377-14(2019) - Standard Test Method for Tack-Free Time of Caulking Compounds and Sealants
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D2377 − 14 (Reapproved 2019)
Standard Test Method for
Tack-Free Time of Caulking Compounds and Sealants
This standard is issued under the fixed designation D2377; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
3 1
1. Scope 4.2 Brass Sheet, ⁄4 by 1 ⁄2 in. (19 by 38 mm), approximately
⁄4 in. (6.4 mm) thick.
1.1 This test method describes the determination of the
tack-free time property of caulking compounds and sealants. 4.3 Template—A rectangular template of steel or brass, ⁄8
This test method is applicable to both gun and knife grades. in. (3.2 mm) thick, 1 by 3 ⁄4 in. (25.4 by 95.1 mm) inside, and
approximately 2 by 4 ⁄4 in. (51 by 121 mm) outside.
1.2 The values stated in inch-pound units are to be regarded
as the standard. The values given in parentheses are for 4.4 Steel Sheets—Two rectangular tin-plated steel sheets,
information only. approximately 3 by 5 in. (76 by 127 mm), and of a convenient
thickness.
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
4.5 Plastic Strips—Two, clear, low-density polyethylene
responsibility of the user of this standard to establish appro-
strips, 1 by 5 in. (25.4 by 127 mm) by 0.004 6 0.001 in.
priate safety, health, and environmental practices and deter-
(0.1016 6 0.0254 mm) thick.
mine the applicability of regulatory limitations prior to use.
4.6 Spatula, steel, havinga4to 5-in. (102 to 127-mm) long
1.4 The committee with jurisdiction over this standard is not
narrow blade.
aware of any comparable standard published by other organi-
4.7 Thin Knife Blade.
zations.
1.5 This international standard was developed in accor-
5. Solvent
dance with internationally recognized principles on standard-
5.1 Methyl Ethyl Ketone, Ethylene Dichloride, or similar
ization established in the Decision on Principles for the
solvent.
Development of International Standards, Guides and Recom-
mendations issued by the World Trade Organization Technical 6. Conditioning
Barriers to Trade (TBT) Committee.
6.1 Condition the sample in the original closed container for
at least 5 h at Standard Conditions as defined in Terminology
2. Referenced Documents
C717.
2.1 ASTM Standards:
C717 Terminology of Building Seals and Sealants 7. Sampling
7.1 Take the sealant from a previously unopened container
3. Terminology
and thoroughly mix before using.
3.1 Definitions—Refer to Terminology C717 for definitions
8. Test Specimens
of the following terms: caulking compound, compound, seal-
ant.
8.1 Prepare two test specimens as follows:
8.1.1 Thoroughly mix the conditioned compound and com-
4. Apparatus
pletely clean the template and steel sheets with solvent.
4.1 Cabinet or Room, capable of maintaining Standard
8.1.2 Center the template on the tin panel and carefully fill
Conditions as defined in Terminology C717.
it, avoiding air pockets. Strike off the surface of the compound
flat to a uniform ⁄8-in. (3.2-mm) thickness. With a thin knife
Thistestmethodisunderthejuri
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