Plastiques alvéolaires -- Détermination des caractéristiques de combustion de petites éprouvettes en position horizontale, soumises à une petite flamme

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ISO/DIS 9772 - Cellular plastics -- Determination of horizontal burning characteristics of small specimens subjected to a small flame
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DRAFT INTERNATIONAL STANDARD
ISO/DIS 9772
ISO/TC 61/SC 4 Secretariat: BSI
Voting begins on: Voting terminates on:
2020-03-17 2020-06-09
Cellular plastics — Determination of horizontal burning
characteristics of small specimens subjected to a small
flame

Plastiques alvéolaires — Détermination des caractéristiques de combustion de petites éprouvettes en

position horizontale, soumises à une petite flamme
ICS: 83.100; 13.220.40
THIS DOCUMENT IS A DRAFT CIRCULATED
FOR COMMENT AND APPROVAL. IT IS
THEREFORE SUBJECT TO CHANGE AND MAY
NOT BE REFERRED TO AS AN INTERNATIONAL
STANDARD UNTIL PUBLISHED AS SUCH.
IN ADDITION TO THEIR EVALUATION AS
BEING ACCEPTABLE FOR INDUSTRIAL,
This document is circulated as received from the committee secretariat.
TECHNOLOGICAL, COMMERCIAL AND
USER PURPOSES, DRAFT INTERNATIONAL
STANDARDS MAY ON OCCASION HAVE TO
BE CONSIDERED IN THE LIGHT OF THEIR
POTENTIAL TO BECOME STANDARDS TO
WHICH REFERENCE MAY BE MADE IN
Reference number
NATIONAL REGULATIONS.
ISO/DIS 9772:2020(E)
RECIPIENTS OF THIS DRAFT ARE INVITED
TO SUBMIT, WITH THEIR COMMENTS,
NOTIFICATION OF ANY RELEVANT PATENT
RIGHTS OF WHICH THEY ARE AWARE AND TO
PROVIDE SUPPORTING DOCUMENTATION. ISO 2020
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ISO/DIS 9772:2020(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2020

All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may

be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting

on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address

below or ISO’s member body in the country of the requester.
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Published in Switzerland
ii © ISO 2020 – All rights reserved
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ISO/DIS 9772:2020(E)
Contents Page

Foreword ........................................................................................................................................................................................................................................iv

Introduction ..................................................................................................................................................................................................................................v

1 Scope ................................................................................................................................................................................................................................. 1

2 Normative references ...................................................................................................................................................................................... 1

3 Terms and definitions ..................................................................................................................................................................................... 1

4 Significance of test .............................................................................................................................................................................................. 2

5 Apparatus ..................................................................................................................................................................................................................... 2

6 Specimens .................................................................................................................................................................................................................... 7

6.1 Extended application of test results ..................................................................................................................................... 7

6.2 Preparation of specimens .............................................................................................................................................................. 8

7 Conditioning .............................................................................................................................................................................................................. 8

7.1 Specimens ................................................................................................................................................................................................... 8

7.2 Cotton indicator ..................................................................................................................................................................................... 9

8 Test procedure ........................................................................................................................................................................................................ 9

8.1 Adjustment of the flame .................................................................................................................................................................. 9

8.2 Adjustment of specimen support .........................................................................................................................................10

8.3 Positioning of cotton indicator ...............................................................................................................................................11

8.4 Positioning of specimen ...............................................................................................................................................................11

8.5 Burning procedure ...........................................................................................................................................................................11

8.6 Measurements ......................................................................................................................................................................................11

8.7 Preparation for the next test ....................................................................................................................................................12

9 Calculations.............................................................................................................................................................................................................12

10 Precision ....................................................................................................................................................................................................................12

11 Test report ................................................................................................................................................................................................................13

Annex A (informative) Classification system ............................................................................................................................................14

Bibliography .............................................................................................................................................................................................................................16

© ISO 2020 – All rights reserved iii
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ISO/DIS 9772:2020(E)
Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards

bodies (ISO member bodies). The work of preparing International Standards is normally carried out

through ISO technical committees. Each member body interested in a subject for which a technical

committee has been established has the right to be represented on that committee. International

organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.

ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of

electrotechnical standardization.

International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.

The main task of technical committees is to prepare International Standards. Draft International

Standards adopted by the technical committees are circulated to the member bodies for voting.

Publication as an International Standard requires approval by at least 75 % of the member bodies

casting a vote.

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. ISO shall not be held responsible for identifying any or all such patent rights.

ISO 9772 was prepared by Technical Committee ISO/TC 61, Plastics, Subcommittee SC 4, Burning

behaviour.

This fourth edition cancels and replaces the third edition (ISO 9772:2012), which has been technically

revised.
iv © ISO 2020 – All rights reserved
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ISO/DIS 9772:2020(E)
Introduction

Cellular plastics are widely used in products for packaging, building, housing, industry and transport,

in various applications. The burning behaviour of cellular plastics is a concern for the fire safety of these

products. This International Standard gives a method for the determination of the burning behaviour of

cellular plastics using a small flame source.

The burning behaviour of cellular plastics is influenced by the test specimen orientation (vertical or

horizontal). This method of test evaluates specimens which are oriented horizontally.

The method described is also intended as a pre-selection test for materials used for components of

devices and appliances. The final acceptance of the material will be dependent upon its use in complete

equipment that conforms with the standards applicable to such equipment.

It should be noted that the test results obtained by the test specified in this International Standard

alone cannot represent all the aspects of the fire hazard of cellular plastics in end-use conditions.

© ISO 2020 – All rights reserved v
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DRAFT INTERNATIONAL STANDARD ISO/DIS 9772:2020(E)
Cellular plastics — Determination of horizontal burning
characteristics of small specimens subjected to a small
flame
1 Scope

1.1 This International Standard specifies a small-scale laboratory screening procedure for comparing

the relative burning characteristics of horizontally oriented, small cellular plastic specimens having a

density less than 250 kg⋅m determined in accordance with ISO 845, when exposed to a small-flame

ignition source.

NOTE Another International Standard exists covering flexible cellular plastic and cellular rubber:

[2]
ISO 3582 .

1.2 This method of test is intended for quality assurance and limited product evaluation of cellular

plastic materials under controlled laboratory conditions, and is not intended to assess the fire behaviour

of e.g. building materials or furnishings under actual fire conditions.

1.3 The optional classification system described in Annex A is intended for the pre-selection of cellular

plastic materials for products, including the determination of the ranges of material parameters that give

the same classification (see 6.1).
2 Normative references

The following referenced documents are indispensable for the application of this document. For dated

references, only the edition cited applies. For undated references, the latest edition of the referenced

document (including any amendments) applies.
ISO 845, Cellular plastics and rubbers — Determination of apparent density
ISO 1923, Cellular plastics and rubbers — Determination of linear dimensions
ISO 10093, Plastics — Fire tests — Standard ignition sources
ISO 13943, Fire safety — Vocabulary
ASTM E2016, Standard Specification for Industrial Woven Wire Cloth
3 Terms and definitions

For the purposes of this International Standard, the terms and definitions given in ISO 13943 and the

following apply.
3.1
afterflame
flame that persists after the ignition source has been removed
[SOURCE: ISO 13943]
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ISO/DIS 9772:2020(E)
3.2
afterflame time
length of time for which an afterflame persists under specified conditions
[SOURCE: ISO 13943]
3.3
afterglow

persistence of glowing combustion after both removal of the ignition source and the cessation of any

flaming combustion
[SOURCE: ISO 13943]
3.4
afterglow time
length of time for which an afterglow persists under specified conditions
[SOURCE: ISO 13943]
3.5
extended application of test results

process of predicting a test result, on the basis of one or more existing test results obtained by the

same test, for a product for which a property and/or the intended end-use application(s) are subject to

variation
3.6
draught-free environment

space in which the results of experiments are not significantly affected by the local air speed

4 Significance of test

4.1 Tests conducted on a material under the conditions specified can be of considerable value when

comparing the horizontal burning characteristics of different materials, controlling manufacturing

processes or assessing any changes in formulation or treatment prior to use.

4.2 Assessment of fire hazard requires consideration of factors such as fuel contribution, intensity

of burning (rate of heat release) and products of combustion, as well as environmental factors such as

intensity of source, orientation of exposed material and ventilation conditions.

4.3 Horizontal burning characteristics, as measured by this test procedure, might be affected by

factors such as density, any anisotropy of the cellular material, its melting characteristics, its colour and

its thickness.

4.4 Certain materials might shrink from the applied flame without igniting. In this event, the test

results are not valid, and additional test specimens will be required to obtain 10 valid test results. If

this proves impossible due to non-ignition of all the specimens, then this test is not suitable for these

materials.

4.5 The horizontal burning characteristics of some cellular plastic materials might change with time,

and tests are therefore conducted before and after heat ageing.
5 Apparatus

5.1 A laboratory fume hood, having an inside volume of at least 0,5 m is used. The chamber shall permit

observation of tests in progress and shall provide a draught free environment whilst allowing normal

thermal circulation of air past the test specimen during burning. The inside surfaces of the chamber shall

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ISO/DIS 9772:2020(E)

be of a dark colour. When a light meter, facing towards the rear of the chamber, is positioned in place of

the test specimen, the recorded light level shall be less than 20 lux.

For safety and convenience, this enclosure (which can be completely closed) shall be fitted with an

extraction device, such as an exhaust fan, to remove products of combustion that might be toxic. The

extraction device shall be turned off during the test and turned on again immediately after the test to

remove the fire effluents. A positive closing damper might be needed.

NOTE The amount of oxygen available to support combustion is naturally important for the conduct of these

flame tests. For tests conducted by this method when burning times are protracted, chamber sizes greater than

0,5 m might be needed to provide reproducible results.

5.2 P/PF2 laboratory burner, as specified in IEC 60695-11-3, having a barrel length of (100 ± 10) mm

and an internal diameter of (9,5 ± 0,3) mm. The barrel shall not be equipped with an end attachment,

such as a stabilizer.

5.3 The burner shall be fitted with a Burner wing top, having an opening of internal length

(48 ± 1) mm and internal width (1,3 ± 0,05) mm (see Figure 1).

To ensure the wing top opening is uniform in width, one option is to slide a (1,3 ± 0,05) mm steel wire

or spacer along its length.

5.4 The Support gauze shall be a wire cloth of plain weave, approximately 215 mm long by 75 mm

wide, as shown in Figure 2. It shall consist of (6,4 ± 0,5) mm mesh gauze constructed of (0,9 ± 0,1) mm

diameter stainless steel, plain or low carbon steel wire. The cloth-mesh and wire diameter are to be

determined as described in the Standard Specification for Industrial Woven Wire Cloth, ASTM E2016.

5.5 The gauge-support holder shall consist of two laboratory ring stands with clamps adjustable to

the desired angles and heights. The gauze-support holder shall be constructed from aluminium or steel

and shall satisfy the following conditions:
— the long axis of the gauze shall be maintained to within 1° of the horizontal;

— the nearest end of the specimen shall be (13 ± 1) mm above the burner wing top (see Figure 2);

— the space both above and below the specimen shall not be obstructed;

— a means shall be provided for positioning the burner in the correct location relative to the specimen,

preferably with a sliding mechanism and a stop to allow fast movement of the burner flame towards

and away from the specimen;

— the gauze shall be equidistant from the front and back, and from both sides, of the test chamber, and

shall be (175 ± 25) mm above the cotton indicator base-board (see Figure 2).

5.6 There shall be two timing devices, each of which reads to within 1 s or less.

5.7 A Measuring scale graduated in millimetres, shall be used to measure the length, width and

thickness of the test specimen.

5.8 A Gas supply shall, supply technical-grade methane gas with a purity of at least 98 % and having a

heat content of (37 ± 1) MJ⋅m , with regulator and meter to ensure uniform gas flow.

Other gas mixtures having a heat content of approximately (37 ± 1) MJ⋅m or propane having a heat

content of (94 ± 2) MJ⋅m have been shown to provide similar results when using the procedure of

Clause 8. In cases of dispute,
...

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