ISO/PRF 11009
(Main)Petroleum products and lubricants -- Determination of water washout characteristics of lubricating greases
Petroleum products and lubricants -- Determination of water washout characteristics of lubricating greases
Produits pétroliers et lubrifiants -- Détermination de la résistance au délavage à l'eau des graisses lubrifiantes
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Standards Content (sample)
INTERNATIONAL ISO
STANDARD 11009
Second edition
Petroleum products and lubricants —
Determination of water washout
characteristics of lubricating greases
Produits pétroliers et lubrifiants — Détermination de la résistance au
délavage à l'eau des graisses lubrifiantes
PROOF/ÉPREUVE
Reference number
ISO 11009:2021(E)
ISO 2021
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ISO 11009:2021(E)
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ISO 11009:2021(E)
Contents Page
Foreword ........................................................................................................................................................................................................................................iv
Introduction ..................................................................................................................................................................................................................................v
1 Scope ................................................................................................................................................................................................................................. 1
2 Normative references ...................................................................................................................................................................................... 1
3 Terms and definitions ..................................................................................................................................................................................... 1
4 Principle ........................................................................................................................................................................................................................ 1
5 Sampling ........................................................................................................................................................................................................................ 2
6 Apparatus ..................................................................................................................................................................................................................... 2
7 Materials ....................................................................................................................................................................................................................... 2
8 Preparation of the apparatus .................................................................................................................................................................. 2
9 Operating procedure ........................................................................................................................................................................................ 3
10 Calculations................................................................................................................................................................................................................ 3
11 Expression of results ........................................................................................................................................................................................ 4
12 Precision ....................................................................................................................................................................................................................... 5
12.1 General ........................................................................................................................................................................................................... 5
12.2 Repeatability, r ....................................................................................................................................................................................... 5
12.3 Reproducibility, R ................................................................................................................................................................................ 5
13 Test report ................................................................................................................................................................................................................... 5
Annex A (informative) Set-up of apparatus ................................................................................................................................................... 6
Bibliography ................................................................................................................................................................................................................................ 8
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ISO 11009:2021(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/ patents).Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO's adherence to the
World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see www .iso .org/
iso/ foreword .html.This document was prepared by Technical Committee ISO/TC 28, Petroleum and related products, fuels
and lubricants from natural or synthetic sources.This second edition cancels and replaces the first edition (ISO 11009:2000), which has been technically
revised.The main changes compared to the previous edition are as follows:
— addition of a rating of the appearance of the grease and of the water after test;
— addition of a note concerning the application of the test results to determine the symbol 3 “water
contamination and rust protection“ of ISO 12924 grease specifications.Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www .iso .org/ members .html.iv PROOF/ÉPREUVE © ISO 2021 – All rights reserved
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ISO 11009:2021(E)
Introduction
[1]
ISO 6743-9 classifies greases according to their conditions of use. The complete designation of a
grease comprises of the ISO sign, the letter L (lubricant, industrial oils and related products), the letter
X for the grease family, four symbols related to the conditions of use, and the NLGI consistency number.
The third symbol is related to the ability of the grease to ensure satisfactory lubrication in presence of
water and provide an adequate corrosion protection level.[2]
The symbol 3 is a combination of the rust protection level evaluated using ISO 11007 and the level of
resistance to water contamination using this document.[3]
Greases are specified in ISO 12924 .
A rolling bearing grease may be not suitable to lubricate plain bearings or gears.
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INTERNATIONAL STANDARD ISO 11009:2021(E)
Petroleum products and lubricants — Determination of
water washout characteristics of lubricating greases
WARNING — The use of this document can involve hazardous materials, operations and
equipment. This document does not purport to address all of the safety problems associated
with its use. It is the responsibility of users of this document to take appropriate measures
to ensure the safety and health of personnel prior to the application of the document, and to
determine the applicability of any other restrictions for this purpose.1 Scope
This document specifies a method for evaluating the resistance of a lubricating grease to washout by
water from a bearing, when tested at 38 °C or 79 °C under specified laboratory test conditions.
This test method estimates the resistance of greases to washout from ball bearings under specified
conditions. No formal correlation with field service has been established so far.
This document is used for development and specification purposes.NOTE For the purposes of this document, the term “% (m/m)” is used to represent the mass fraction.
2 Normative referencesThe following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 15, Rolling bearings — Radial bearings — Boundary dimensions, general planISO 1998-1, Petroleum industry — Terminology — Part 1: Raw materials and products
ISO 3696, Water for analytical laboratory use — Specification and test methodsISO 23572, Petroleum products — Lubricating greases — Sampling of greases
3 Terms and definitions
For the purposes of this document, the terms and definitions given in ISO 1998-1 apply.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
— ISO Online browsing platform: available at https:// www .iso .org/ obp— IEC Electropedia: available at http:// www .electropedia .org/
4 Principle
A test portion of grease is packed in a ball bearing inserted in a housing with specified clearances.
−1 −1The bearing is rotated at 63 rad/s ± 3 rad/s (600 min ± 30 min ). Water, controlled at a specified
test temperature, impinges on the bearing housing from a nozzle with a diameter of 1 mm, at a rate of
5 ml/s ± 0,5 ml/s. The distance between the end of the nozzle and the shield of the housing is 57 mm.
The water jet is set to strike the bearing 6 m...
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