Automotive fuels - Automotive B10 diesel fuel - Requirements and test methods

This European Standard specifies requirements and test methods for marketed and delivered automotive B10 diesel fuel, i.e. diesel fuel containing up to 10,0 %(V/V) Fatty Acid Methyl Ester. It is applicable to fuel for use in diesel engine vehicles compatible with automotive B10 diesel fuel.
NOTE 1   This product is allowed in Europe [4], but national legislation can set additional requirements or rules concerning, or even prohibiting, marketing or delivering of the product.
NOTE 2   In this European Standard, A-deviations apply (see Annex B).
NOTE 3   For the purposes of this European Standard, the terms "% (m/m)" and "% (V/V)" are used to represent respectively the mass fraction and the volume fraction.

Kraftstoffe für Kraftfahrzeuge - B10 Dieselkraftstoff - Anforderungen und Prüfverfahren

Carburants pour automobiles - Carburant B10 pour moteur automobile diesel - Exigences et méthodes d'essai

Goriva za motorna vozila - Dizelsko gorivo za motorna vozila B10 - Zahteve in preskusne metode

General Information

Status
Not Published
Public Enquiry End Date
30-Jun-2021
Current Stage
4020 - Public enquire (PE) (Adopted Project)
Start Date
07-Apr-2021
Due Date
25-Aug-2021
Completion Date
28-Jun-2021

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SLOVENSKI STANDARD
oSIST prEN 16734:2021
01-junij-2021
Goriva za motorna vozila - Dizelsko gorivo za motorna vozila B10 - Zahteve in
preskusne metode
Automotive fuels - Automotive B10 diesel fuel - Requirements and test methods

Kraftstoffe für Kraftfahrzeuge - B10 Dieselkraftstoff - Anforderungen und Prüfverfahren

Carburants pour automobiles - Carburant B10 pour moteur automobile diesel -
Exigences et méthodes d'essai
Ta slovenski standard je istoveten z: prEN 16734
ICS:
75.160.20 Tekoča goriva Liquid fuels
oSIST prEN 16734:2021 en

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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oSIST prEN 16734:2021
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oSIST prEN 16734:2021
DRAFT
EUROPEAN STANDARD
prEN 16734
NORME EUROPÉENNE
EUROPÄISCHE NORM
May 2021
ICS 75.160.20 Will supersede EN 16734:2016+A1:2018
English Version
Automotive fuels - Automotive B10 diesel fuel -
Requirements and test methods

Carburants pour automobiles - Carburant B10 pour Kraftstoffe für Kraftfahrzeuge - B10 Dieselkraftstoff -

moteur automobile diesel - Exigences et méthodes Anforderungen und Prüfverfahren
d'essai

This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee

CEN/TC 19.

If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations

which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.

This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other

language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC

Management Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,

Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and

United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are

aware and to provide supporting documentation.

Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without

notice and shall not be referred to as a European Standard.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels

© 2021 CEN All rights of exploitation in any form and by any means reserved Ref. No. prEN 16734:2021 E

worldwide for CEN national Members.
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oSIST prEN 16734:2021
prEN 16734:2021 (E)
Contents Page

European foreword ...................................................................................................................................................... 3

1 Scope .................................................................................................................................................................... 5

2 Normative references .................................................................................................................................... 5

3 Terms and definitions ................................................................................................................................... 7

4 Sampling ............................................................................................................................................................. 7

5 Pump marking.................................................................................................................................................. 7

6 Requirements and test methods ............................................................................................................... 7

6.1 Dyes and markers ........................................................................................................................................... 7

6.2 Additives ............................................................................................................................................................ 8

6.2.1 General ................................................................................................................................................................ 8

6.2.2 Methylcyclopentadienyl manganese tricarbonyl (MMT) ................................................................. 8

6.3 Fatty acid methyl ester (FAME) .................................................................................................................. 8

6.4 Other (bio-) components .............................................................................................................................. 9

6.5 Generally applicable requirements and related test methods ...................................................... 9

6.6 Climate dependent requirements and related test methods ........................................................ 13

6.7 Precision and dispute .................................................................................................................................. 15

Annex A (informative) A-deviations .................................................................................................................... 16

Bibliography.................................................................................................................................................................. 17

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oSIST prEN 16734:2021
prEN 16734:2021 (E)
European foreword

This document (prEN 16734:2021) has been prepared by Technical Committee CEN/TC 19 “Gaseous

and liquid fuels, lubricants and related products of petroleum, synthetic and biological origin”, the

secretariat of which is held by NEN.
This document is currently submitted to the CEN Enquiry.
This document will supersede EN 16734:2016+A1:2018.

This document has originally been prepared under a mandate [1] given to CEN by the European

Commission and the European Free Trade Association. It has been developed in coordination with

representatives of those institutions.

This document describes a specification for diesel fuel containing up to 10,0 % (V/V) Fatty Acid Methyl

Ester. This product is not suitable for all vehicles, so consumers and providers should consult vehicle

manufacturers or manuals before use.

Requirements following amendment 2003/17/EC [3], 2009/30/EC [4], 2011/63/EU [5] and

2014/77/EU [6] to the European Fuels Quality Directive 98/70/EC [2], are taken into account. Dates

are included with all normative test method references in order to comply with the requirements of the

European Commission; with the accompanying assurance by CEN/TC 19 that any referenced updated

versions will always give at least the same accuracy and at least the same level of precision (see [4]).

The marking at the pump of this product is in line with the requirements of the Fuels Quality Directive

and the Alternative Fuels Infrastructure Directive [7].

Significant technical changes between this document and the previous edition are:

— Inclusion of the amended EN 14214 FAME specification.

— Update to the normative references towards undated versions where they don't concern

requirements originating from European Directives (in line with decisions by CEN/TC 19 in

coordination with the European Commission), and updating the effective publication dates were

required.

— Deletion of the Fuel Ignition Tester (EN 16144) as an alternative test method for cetane number

determination due to its absence of use in the market. Whereas the BASF engine (EN 16906) and

the ICN technique (EN 17155) have now been included as alternative methods for cetane number

determination,

— Addition of micro-distillation (EN 17306) as an alternative test method to distillation by

EN ISO 3405 and EN ISO 3924.

— Addition of automated method (EN ISO 22995) as an alternative test method to cloud point by

EN ISO 3015.

— Addition of the Stabinger viscometer (ISO 23581) as an alternative test method to viscosity by

EN ISO 3104.

— Addition of oxidation stability by rapid small scale oxidation method (EN 16091) as an alternative

test method to oxidation stability by EN 15751 for diesel fuel containing FAME above 2,0 % (V/V).

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— Deletion of Annex A on precision data and introduction of a NOTE under 6.5.1 in relation to test

method precision data for diesel fuel containing FAME.

— Update to the 'workmanship clause' in 6.5.3 to address the issue of abrasive wear of fuel injection

equipment by hard particles in diesel fuel.

— Introduction of further clarification around the lubricity requirement in Table 1.

— Reduction of the minimum density limit for Grades D, E and F, moving the property from Table 1

to Table 2.
— Clarification of the dispute requirement concerning sulfur content in 6.7.3.
— Deletion of the allowance for cetane alternative methods in 6.7.4.

— Addition of 6.7.11 to address situations in which the test method includes a bias-correction to the

dispute method.

— Deletion of the A-deviation for Belgium following change of national legislation.

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oSIST prEN 16734:2021
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1 Scope

This document specifies requirements and test methods for marketed and delivered automotive B10

diesel fuel, i.e. diesel fuel containing up to 10,0 %(V/V) Fatty Acid Methyl Ester. It is applicable to fuel

for use in diesel engine vehicles compatible with automotive B10 diesel fuel.

NOTE 1 This product is allowed in Europe [4], but national legislation can set additional requirements or rules

concerning, or even prohibiting, marketing or delivering of the product.
NOTE 2 In this document, A-deviations apply (see Annex A).

NOTE 3 For the purposes of this document, the terms “% (m/m)” and “% (V/V)” are used to represent

respectively the mass fraction and the volume fraction.
2 Normative references

The following documents are referred to in the text in such a way that some or all of their content

constitutes requirements of this document. For dated references, only the edition cited applies. For

undated references, the latest edition of the referenced document (including any amendments) applies.

EN 116, Diesel and domestic heating fuels - Determination of cold filter plugging point - Stepwise cooling

bath method

EN 12662, Liquid petroleum products - Determination of total contamination in middle distillates, diesel

fuels and fatty acid methyl esters

EN 12916:2019, Petroleum products - Determination of aromatic hydrocarbon types in middle distillates -

High performance liquid chromatography method with refractive index detection

EN 14078:2014, Liquid petroleum products - Determination of fatty acid methyl ester (FAME) content in

middle distillates - Infrared spectrometry method

EN 14214:2012+A2:2019, Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel

engines and heating applications - Requirements and test methods

EN 15195:2014, Liquid petroleum products - Determination of ignition delay and derived cetane number

(DCN) of middle distillate fuels by combustion in a constant volume chamber

EN 15751, Automotive fuels - Fatty acid methyl ester (FAME) fuel and blends with diesel fuel -

Determination of oxidation stability by accelerated oxidation method

EN 16329, Diesel and domestic heating fuels - Determination of cold filter plugging point - Linear cooling

bath method

EN 16576:2014, Automotive fuels - Determination of manganese and iron content in diesel - Inductively

coupled plasma optical emission spectrometry (ICP OES) method

EN 16715:2015, Liquid petroleum products - Determination of ignition delay and derived cetane number

(DCN) of middle distillate fuels - Ignition delay and combustion delay determination using a constant

volume combustion chamber with direct fuel injection

Liquid petroleum products — Determination of the ignition quality of diesel fuels —

EN 16906:2017,
BASF engine method
standard under revision
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prEN 16734:2021 (E)

EN 16942, Fuels - Identification of vehicle compatibility - Graphical expression for consumer information

EN 17155:2018, Liquid petroleum products - Determination of indicated cetane number (ICN) of middle

distillate fuels - Primary reference fuels calibration method using a constant volume combustion chamber

EN 17306:2019, Liquid petroleum products - Determination of distillation characteristics at atmospheric

pressure - Micro-distillation

EN ISO 3015, Petroleum and related products from natural or synthetic sources - Determination of cloud

point (ISO 3015)

EN ISO 2160, Petroleum products - Corrosiveness to copper - Copper strip test (ISO 2160)

EN ISO 2719, Determination of flash point - Pensky-Martens closed cup method (ISO 2719)

EN ISO 3104, Petroleum products - Transparent and opaque liquids - Determination of kinematic viscosity

and calculation of dynamic viscosity (ISO 3104)
EN ISO 3170, Petroleum liquids - Manual sampling (ISO 3170)
EN ISO 3171, Petroleum liquids - Automatic pipeline sampling (ISO 3171)

EN ISO 3405:2019, Petroleum and related products from natural or synthetic sources - Determination of

distillation characteristics at atmospheric pressure (ISO 3405:2019)

EN ISO 3675:1998, Crude petroleum and liquid petroleum products - Laboratory determination of density

- Hydrometer method (ISO 3675:1998)

EN ISO 3924:2019, Petroleum products - Determination of boiling range distribution - Gas

chromatography method (ISO 3924:2019)

EN ISO 4259-2, Petroleum and related products - Precision of measurement methods and results - Part 2:

Interpretation and application of precision data in relation to methods of test (ISO 4259-2)

EN ISO 4264, Petroleum products - Calculation of cetane index of middle-distillate fuels by the four

variable equation (ISO 4264:2018)

EN ISO 5165:2020, Petroleum products - Determination of the ignition quality of diesel fuels - Cetane

engine method (ISO 5165:2020)
EN ISO 6245, Petroleum products - Determination of ash (ISO 6245:2001)

EN ISO 10370, Petroleum products - Determination of carbon residue - Micro method (ISO 10370)

EN ISO 12185:1996 , Crude petroleum and petroleum products — Determination of density — Oscillating

U-tube method (ISO 12185:1996)

EN ISO 12205, Petroleum products - Determination of the oxidation stability of middle-distillate fuels (ISO

12205)

EN ISO 12937, Petroleum products - Determination of water - Coulometric Karl Fischer titration method

(ISO 12937)

EN ISO 13032:2012, Petroleum products - Determination of low concentration of sulfur in automotive

fuels - Energy-dispersive X-ray fluorescence spectrometric method (ISO 13032:2012)

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EN ISO 13759, Petroleum products - Determination of alkyl nitrate in diesel fuels - Spectrometric method

(ISO 13759)

EN ISO 20846:2019, Petroleum products - Determination of sulfur content of automotive fuels -

Ultraviolet fluorescence method (ISO 20846:2019)

EN ISO 20884:2019, Petroleum products - Determination of sulfur content of automotive fuels -

Wavelength-dispersive X-ray fluorescence spectrometry (ISO 20884:2019)

EN ISO 22995, Petroleum products - Determination of cloud point - Automated step-wise cooling method

(ISO 22995)

ISO 23581, Petroleum products and related products — Determination of kinematic viscosity — Method

by Stabinger type viscometer
3 Terms and definitions
No terms and definitions are listed in this document.
4 Sampling

Samples shall be taken as described in EN ISO 3170 or EN ISO 3171 and/or in accordance with the

requirements of national standards or regulations for the sampling of automotive diesel fuel. The

national requirements shall be set out in detail or shall be referred to by reference in a National Annex

to this document.

In view of the sensitivity of some of the test methods referred to in this document, particular attention

shall be paid to compliance with any guidance on sampling containers which is included in the test

method standard.
5 Pump marking

Information to be marked on dispensing pumps and nozzles used for delivering automotive B10 diesel

fuel, and the dimensions of the mark shall be in accordance with EN 16942.

Labelling shall be clearly visible, easily legible and displayed at any point where diesel with metallic

additives is made available to consumers. The label shall contain: “Contains metallic additives” in the

national language(s) and shall be laid down in the National Annex to this document.

Further indication on dispensing pumps in the national language of “Not suitable for all vehicles;

consult vehicle manufacturer or manual before use” is also strongly recommended.
6 Requirements and test methods
6.1 Dyes and markers
The use of dyes or markers is allowed.
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prEN 16734:2021 (E)
6.2 Additives
6.2.1 General

In order to improve the quality, the use of additives is allowed. Suitable fuel additives without known

harmful side-effects are recommended in the appropriate amount, to help to avoid deterioration of

driveability and emissions control durability. Other technical means with equivalent effect may also be

used.

NOTE Deposit forming tendency test methods suitable for routine control purposes have not yet been

identified and developed.
6.2.2 Methylcyclopentadienyl manganese tricarbonyl (MMT)
When methylcyclopentadieny
...

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