ASTM D801-02(2017)
(Test Method)Standard Test Methods for Sampling and Testing Dipentene
Standard Test Methods for Sampling and Testing Dipentene
SIGNIFICANCE AND USE
3.1 The testing procedures described in these test methods have been in use for many years and emphasize the physical properties rather than the chemical composition of dipentene. These procedures were sufficient when dipentene was used primarily as a solvent. Currently, however, dipentene finds application as a chemical raw material and a knowledge of its chemical composition is therefore important. Test Methods D6387 describe a capillary gas chromatography method which is suitable for determining both the major and minor components found in dipentene.
SCOPE
1.1 These test methods cover procedures for sampling and testing dipentene and related terpene solvents, consisting chiefly of monocyclic terpene hydrocarbons distilling above the range for turpentine.
1.2 The procedures given in these test methods appear in the following order:
Section
Sampling
4
Detection and Removal of Separated Water
5
Appearance
6
Color
7
Odor
8
Specific Gravity
9
Refractive Index
10
Composition
11
Flash Point
12
Moisture
13
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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Designation: D801 − 02 (Reapproved 2017)
Standard Test Methods for
1
Sampling and Testing Dipentene
This standard is issued under the fixed designation D801; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D268 Guide for Sampling and Testing Volatile Solvents and
Chemical Intermediates for Use in Paint and Related
1.1 These test methods cover procedures for sampling and
Coatings and Material
testing dipentene and related terpene solvents, consisting
D890 Test Method for Water in Liquid Pine Chemicals
chiefly of monocyclic terpene hydrocarbons distilling above
D1209 Test Method for Color of Clear Liquids (Platinum-
the range for turpentine.
Cobalt Scale)
1.2 Theproceduresgiveninthesetestmethodsappearinthe
D6166 Test Method for Color of Pine Chemicals and Re-
following order:
lated Products (Instrumental Determination of Gardner
Section
Color)
Sampling 4
D6387 Test Methods for Composition of Turpentine and
Detection and Removal of Separated Water 5
Related Terpene Products by Capillary Gas Chromatogra-
Appearance 6
Color 7
phy
Odor 8
E300 Practice for Sampling Industrial Chemicals
Specific Gravity 9
Refractive Index 10
Composition 11 3. Significance and Use
Flash Point 12
3.1 The testing procedures described in these test methods
Moisture 13
have been in use for many years and emphasize the physical
1.3 The values stated in SI units are to be regarded as
properties rather than the chemical composition of dipentene.
standard. No other units of measurement are included in this
These procedures were sufficient when dipentene was used
standard.
primarily as a solvent. Currently, however, dipentene finds
1.4 This standard does not purport to address all of the
application as a chemical raw material and a knowledge of its
safety concerns, if any, associated with its use. It is the
chemical composition is therefore important. Test Methods
responsibility of the user of this standard to establish appro-
D6387 describe a capillary gas chromatography method which
priate safety, health, and environmental practices and deter-
is suitable for determining both the major and minor compo-
mine the applicability of regulatory limitations prior to use.
nents found in dipentene.
1.5 This international standard was developed in accor-
dance with internationally recognized principles on standard-
4. Sampling
ization established in the Decision on Principles for the
4.1 Sample the material in accordance with the procedure
Development of International Standards, Guides and Recom-
described in Guide D268 and Practice E300. If a sample from
mendations issued by the World Trade Organization Technical
close to the bottom of a tank shows a decided difference in
Barriers to Trade (TBT) Committee.
colororappearancefromsamplestakenatotherdepths,takean
extra bottom sample and examine it separately from the
2. Referenced Documents
composite sample. In such case the composite sample shall not
2
2.1 ASTM Standards:
include any portion of such bottom sample.
1 5. Detection and Removal of Separated Water
These test methods are under the jurisdiction of ASTM Committee D01 on
Paint and Related Coatings, Materials, and Applications and are the direct
5.1 Draw a portion of the dipentene by means of a glass or
responsibility of Subcommittee D01.34 on Pine Chemicals and Hydrocarbon
3
metal container with a removable stopper or top, or with a
Resins.
Current edition approved Dec. 1, 2017. Published December 2017. Originally
thief, from the lowest part of the container, or by opening the
approved in 1944. Last previous edition approved in 2013 as D801 – 02 (2013).
bottom valve of the level tank car. If water is found to be
DOI: 10.1520/D0801-02R17.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on Detailed description of equipment suitable for such sampling is given in
the ASTM website. Practice E300.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D801 − 02 (2017)
present, draw it all out, record the quantity, and deduct it from temperature at which the determination was made is respec-
the total volume of liquid delivered. tively above or below 20°C.
6. Appearance
11. Composition
6.1 Examine a portion of the sample after agitation to
11.1 Determine the component concentration of dipentene
determine its clarity and freedom from foreign m
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D801 − 02 (Reapproved 2013) D801 − 02 (Reapproved 2017)
Standard Test Methods for
1
Sampling and Testing Dipentene
This standard is issued under the fixed designation D801; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 These test methods cover procedures for sampling and testing dipentene and related terpene solvents, consisting chiefly of
monocyclic terpene hydrocarbons distilling above the range for turpentine.
1.2 The procedures given in these test methods appear in the following order:
Section
Sampling 4
Detection and Removal of Separated Water 5
Appearance 6
Color 7
Odor 8
Specific Gravity 9
Refractive Index 10
Composition 11
Flash Point 12
Moisture 13
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D268 Guide for Sampling and Testing Volatile Solvents and Chemical Intermediates for Use in Paint and Related Coatings and
Material
D890 Test Method for Water in Liquid Pine Chemicals
D1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
D6166 Test Method for Color of Pine Chemicals and Related Products (Instrumental Determination of Gardner Color)
D6387 Test Methods for Composition of Turpentine and Related Terpene Products by Capillary Gas Chromatography
E300 Practice for Sampling Industrial Chemicals
3. Significance and Use
3.1 The testing procedures described in these test methods have been in use for many years and emphasize the physical
properties rather than the chemical composition of dipentene. These procedures were sufficient when dipentene was used primarily
as a solvent. Currently, however, dipentene finds application as a chemical raw material and a knowledge of its chemical
composition is therefore important. Test Methods D6387 describe a capillary gas chromatography method which is suitable for
determining both the major and minor components found in dipentene.
1
These test methods are under the jurisdiction of ASTM Committee D01 on Paint and Related Coatings, Materials, and Applications and are the direct responsibility of
Subcommittee D01.34 on Pine Chemicals and Hydrocarbon Resins.
Current edition approved June 1, 2013Dec. 1, 2017. Published June 2013December 2017. Originally approved in 1944. Last previous edition approved in 20092013 as
D801 – 02 (2009).(2013). DOI: 10.1520/D0801-02R13.10.1520/D0801-02R17.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’sstandard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D801 − 02 (2017)
4. Sampling
4.1 Sample the material in accordance with the procedure described in Guide D268 and Practice E300. If a sample from close
to the bottom of a tank shows a decided difference in color or appearance from samples taken at other depths, take an extra bottom
sample and examine it separately from the composite sample. In such case the composite sample shall not include any portion of
such bottom sample.
5. Detection and Removal of Separated Water
3
5.1 Draw a portion of the dipentene by means of a glass or metal container with a removable stopper or top, or with a thief,
from the lowest part of the container, or by opening the bottom valve of the level tank car. If water is found to be present, draw
it all out, record the quantity, and deduct it from the total volume of
...
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